메뉴 건너뛰기




Volumn 150, Issue 1, 2001, Pages 57-70

Inverse detection and heteronuclear editing in 1H-15N correlation and 1H-1H double-quantum NMR spectroscopy in the solid state under fast MAS

Author keywords

[No Author keywords available]

Indexed keywords

ARTICLE;

EID: 0035743160     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.2001.2312     Document Type: Article
Times cited : (63)

References (60)
  • 1
    • 85120190700 scopus 로고
    • M. Mehring Principles of High Resolution NMR in Solids 1983 Springer-Verlag Berlin
    • (1983)
    • Mehring, M.1
  • 2
    • 85120216353 scopus 로고
    • K. Schmidt-Rohr H.W. Spiess Multidimensional Solid-State NMR and Polymers 1994 Academic Press London
    • (1994)
    • Schmidt-Rohr, K.1    Spiess, H.W.2
  • 4
    • 85120217987 scopus 로고    scopus 로고
    • 1H NMR spectroscopy in the solid state: Very-fast sample spinning and multiple-quantum coherences, Adv. Opt. Magn. Reson, in press.
  • 6
    • 0032607798 scopus 로고    scopus 로고
    • Solid-state nuclear magnetic resonance spectra of dipolar-coupled multi-spin systems under fast magic angle spinning
    • C. Filip S. Hafner I. Schnell D.E. Demco H.W. Spiess Solid-state nuclear magnetic resonance spectra of dipolar-coupled multi-spin systems under fast magic angle spinning J. Chem. Phys. 110 1999 423 440
    • (1999) J. Chem. Phys. , vol.110 , pp. 423-440
    • Filip, C.1    Hafner, S.2    Schnell, I.3    Demco, D.E.4    Spiess, H.W.5
  • 9
    • 0346938543 scopus 로고    scopus 로고
    • High-field and high-speed CPMAS 13C NMR heteronuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee–Goldburg homonuclear decoupling
    • 13C NMR heteronuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee–Goldburg homonuclear decoupling J. Magn. Reson. 124 1997 516 519
    • (1997) J. Magn. Reson. , vol.124 , pp. 516-519
    • van Rossum, B.-J.1    Förster, H.2    de Groot, H.J.M.3
  • 10
    • 0032561821 scopus 로고    scopus 로고
    • Carbon-proton chemical shift correlation in solid-state NMR by through bond multiple-quantum spectroscopy
    • A. Lesage D. Sakellariou S. Steuernagel L. Emsley Carbon-proton chemical shift correlation in solid-state NMR by through bond multiple-quantum spectroscopy J. Am. Chem. Soc. 120 1998 13194 13201
    • (1998) J. Am. Chem. Soc. , vol.120 , pp. 13194-13201
    • Lesage, A.1    Sakellariou, D.2    Steuernagel, S.3    Emsley, L.4
  • 11
    • 0033208603 scopus 로고    scopus 로고
    • Recoupled polarization transfer heteronuclear 1H–13C multiple-quantum correlation in solids under ultra-fast MAS
    • 13C multiple-quantum correlation in solids under ultra-fast MAS J. Magn. Reson. 140 1999 471 476
    • (1999) J. Magn. Reson. , vol.140 , pp. 471-476
    • Saalwächter, K.1    Graf, R.2    Spiess, H.W.3
  • 12
    • 0035743912 scopus 로고    scopus 로고
    • Recoupled polarization-transfer methods for solid-state 1H–13C heteronuclear correlation in the limit of fast MAS
    • 13C heteronuclear correlation in the limit of fast MAS J. Magn. Reson. 148 2001 398 418
    • (2001) J. Magn. Reson. , vol.148 , pp. 398-418
    • Saalwächter, K.1    Graf, R.2    Spiess, H.W.3
  • 13
    • 0035307855 scopus 로고    scopus 로고
    • Heteronuclear 1H–13C multiple-spin correlation in solid-state NMR: Combining REDOR recoupling and multiple-quantum spectroscopy
    • 13C multiple-spin correlation in solid-state NMR: Combining REDOR recoupling and multiple-quantum spectroscopy J. Chem. Phys. 114 2001 5707 5728
    • (2001) J. Chem. Phys. , vol.114 , pp. 5707-5728
    • Saalwächter, K.1    Spiess, H.W.2
  • 14
    • 85120235612 scopus 로고    scopus 로고
    • Solid-state NMR in immobilized biomolecules: Correlation experiments for assignment and structure determination in fully labeled peptides and membrane-proteins
    • M. Baldus Solid-state NMR in immobilized biomolecules: Correlation experiments for assignment and structure determination in fully labeled peptides and membrane-proteins The Future of Solid State NMR in Biology 2000
    • (2000)
    • Baldus, M.1
  • 15
    • 0002377859 scopus 로고
    • Frequency-switched pulse sequences—Homonuclear decoupling and dilute spin NMR in solids
    • A. Bielecki A.C. Kolbert M.H. Levitt Frequency-switched pulse sequences—Homonuclear decoupling and dilute spin NMR in solids Chem. Phys. Lett. 155 1989 341 346
    • (1989) Chem. Phys. Lett. , vol.155 , pp. 341-346
    • Bielecki, A.1    Kolbert, A.C.2    Levitt, M.H.3
  • 17
    • 49449126641 scopus 로고
    • Cross-correlation of spin-decoupled NMR spectra by heteronuclear two-dimensional spectroscopy
    • A.A. Maudsley L. Müller R.R. Ernst Cross-correlation of spin-decoupled NMR spectra by heteronuclear two-dimensional spectroscopy J. Magn. Reson. 28 1977 463 469
    • (1977) J. Magn. Reson. , vol.28 , pp. 463-469
    • Maudsley, A.A.1    Müller, L.2    Ernst, R.R.3
  • 18
    • 0002616982 scopus 로고
    • Sensitivity enhanced detection of weak nuclei using heteronuclear multiple quantum coherence
    • L. Müller Sensitivity enhanced detection of weak nuclei using heteronuclear multiple quantum coherence J. Am. Chem. Soc. 101 1979 4481 4484
    • (1979) J. Am. Chem. Soc. , vol.101 , pp. 4481-4484
    • Müller, L.1
  • 19
    • 33644757144 scopus 로고
    • Correlation of proton and nitrogen-15 chemical shifts by multiple quantum NMR
    • A. Bax R.H. Griffey B.L. Hawkins Correlation of proton and nitrogen-15 chemical shifts by multiple quantum NMR J. Magn. Reson. 55 1983 301 315
    • (1983) J. Magn. Reson. , vol.55 , pp. 301-315
    • Bax, A.1    Griffey, R.H.2    Hawkins, B.L.3
  • 20
    • 0000195671 scopus 로고
    • Natural abundance nitrogen-15 NMR by enhanced heteronuclear spectroscopy
    • G. Bodenhausen D.J. Ruben Natural abundance nitrogen-15 NMR by enhanced heteronuclear spectroscopy Chem. Phys. Lett. 69 1980 185 189
    • (1980) Chem. Phys. Lett. , vol.69 , pp. 185-189
    • Bodenhausen, G.1    Ruben, D.J.2
  • 21
    • 0001173504 scopus 로고
    • Stimulated echo NMR spectra and their use for heteronuclear two-dimensional shift correlation
    • A.G. Redfield Stimulated echo NMR spectra and their use for heteronuclear two-dimensional shift correlation Chem. Phys. Lett. 96 1983 537
    • (1983) Chem. Phys. Lett. , vol.96 , pp. 537
    • Redfield, A.G.1
  • 22
    • 85120194657 scopus 로고
    • R.R. Ernst G. Bodenhausen A. Wokaun Principles of Nuclear Magnetic Resonance in One and Two Dimensions 1987 Oxford Univ. Press Oxford
    • (1987)
    • Ernst, R.R.1    Bodenhausen, G.2    Wokaun, A.3
  • 23
    • 45449123834 scopus 로고
    • Efficient purging scheme for proton-detected heteronuclear two-dimensional NMR
    • G. Otting K. Wüthrich Efficient purging scheme for proton-detected heteronuclear two-dimensional NMR J. Magn. Reson. 76 1988 569 574
    • (1988) J. Magn. Reson. , vol.76 , pp. 569-574
    • Otting, G.1    Wüthrich, K.2
  • 24
    • 36149026370 scopus 로고
    • Nuclear double resonance in the rotating frame
    • S.R. Hartmann E.L. Hahn Nuclear double resonance in the rotating frame Phys. Rev. 128 1962 2042 2053
    • (1962) Phys. Rev. , vol.128 , pp. 2042-2053
    • Hartmann, S.R.1    Hahn, E.L.2
  • 25
    • 0009650639 scopus 로고
    • Spin temperature in nuclear double resonance
    • F.M. Lurie C.P. Slichter Spin temperature in nuclear double resonance Phys. Rev. A 133 1964 1108 1122
    • (1964) Phys. Rev. A , vol.133 , pp. 1108-1122
    • Lurie, F.M.1    Slichter, C.P.2
  • 26
    • 0000854398 scopus 로고
    • Higher resolution NMR of rare spins in solids
    • H.E. Bleich A.G. Redfield Higher resolution NMR of rare spins in solids J. Chem. Phys. 55 1971 5405 5406
    • (1971) J. Chem. Phys. , vol.55 , pp. 5405-5406
    • Bleich, H.E.1    Redfield, A.G.2
  • 27
    • 36849102863 scopus 로고
    • High-resolution NMR in solids by intermolecular double resonance
    • C.S. Yannoni High-resolution NMR in solids by intermolecular double resonance J. Chem. Phys. 56 1972 1773 1774
    • (1972) J. Chem. Phys. , vol.56 , pp. 1773-1774
    • Yannoni, C.S.1
  • 29
    • 36849106840 scopus 로고
    • Proton-enhanced NMR of dilute spins in solids
    • A. Pines M.G. Gibby J.S. Waugh Proton-enhanced NMR of dilute spins in solids J. Chem. Phys. 59 1973 569 590
    • (1973) J. Chem. Phys. , vol.59 , pp. 569-590
    • Pines, A.1    Gibby, M.G.2    Waugh, J.S.3
  • 30
    • 0033629934 scopus 로고    scopus 로고
    • Sensitivity enhancement in solid state 15N NMR by indirect detection with high-speed magic angle spinning
    • 15N NMR by indirect detection with high-speed magic angle spinning J. Magn. Reson. 142 2000 199 204
    • (2000) J. Magn. Reson. , vol.142 , pp. 199-204
    • Ishii, Y.1    Tycko, R.2
  • 32
    • 0011667250 scopus 로고
    • Separation of the different orders of NMR multiple-quantum transitions by the use of pulsed-field gradients
    • A. Bax P.G. de Jong A.F. Mehlkopf J. Smidt Separation of the different orders of NMR multiple-quantum transitions by the use of pulsed-field gradients Chem. Phys. Lett. 69 1980 567 570
    • (1980) Chem. Phys. Lett. , vol.69 , pp. 567-570
    • Bax, A.1    de Jong, P.G.2    Mehlkopf, A.F.3    Smidt, J.4
  • 33
    • 0001138399 scopus 로고
    • Pulsed field gradients in NMR. An alternative to phase cycling
    • P. Barker R. Freeman Pulsed field gradients in NMR. An alternative to phase cycling J. Magn. Reson. 64 1985 334 338
    • (1985) J. Magn. Reson. , vol.64 , pp. 334-338
    • Barker, P.1    Freeman, R.2
  • 34
    • 0001594959 scopus 로고
    • Optimized recording of heteronuclear NMR spectra using pulsed-field gradients
    • A. Bax S.S. Pochaapsky Optimized recording of heteronuclear NMR spectra using pulsed-field gradients J. Magn. Reson. 99 1992 638 643
    • (1992) J. Magn. Reson. , vol.99 , pp. 638-643
    • Bax, A.1    Pochaapsky, S.S.2
  • 35
    • 0347722841 scopus 로고    scopus 로고
    • Heteronuclear multidimensional NMR experiments for the structure determination of proteins in solution employing pulsed field gradients
    • M. Sattler J. Schleucher C. Griesinger Heteronuclear multidimensional NMR experiments for the structure determination of proteins in solution employing pulsed field gradients Progr. NMR Spectrosc. 34 1999 93 158
    • (1999) Progr. NMR Spectrosc. , vol.34 , pp. 93-158
    • Sattler, M.1    Schleucher, J.2    Griesinger, C.3
  • 36
    • 85011817347 scopus 로고
    • Detection of weak heteronuclear dipolar couplings by rotational-echo double-resonance nuclear magnetic resonance
    • T. Gullion J. Schaefer Detection of weak heteronuclear dipolar couplings by rotational-echo double-resonance nuclear magnetic resonance Adv. Magn. Reson. 13 1989 57 83
    • (1989) Adv. Magn. Reson. , vol.13 , pp. 57-83
    • Gullion, T.1    Schaefer, J.2
  • 37
  • 38
    • 43949171911 scopus 로고
    • Measurement of heteronuclear dipolar coupling by transferred-echo double-resonance NMR
    • A.W. Hing S. Vega J. Schaefer Measurement of heteronuclear dipolar coupling by transferred-echo double-resonance NMR J. Magn. Reson. A 103 1993 151 162
    • (1993) J. Magn. Reson. A , vol.103 , pp. 151-162
    • Hing, A.W.1    Vega, S.2    Schaefer, J.3
  • 39
    • 0003166074 scopus 로고
    • Solid-state proton multiple-quantum NMR spectroscopy with fast magic-angle spinning
    • H. Geen J.J. Titman J. Gottwald H.W. Spiess Solid-state proton multiple-quantum NMR spectroscopy with fast magic-angle spinning Chem. Phys. Lett. 227 1994 79 86
    • (1994) Chem. Phys. Lett. , vol.227 , pp. 79-86
    • Geen, H.1    Titman, J.J.2    Gottwald, J.3    Spiess, H.W.4
  • 40
    • 0000611231 scopus 로고
    • High-resolution double-quantum NMR spectroscopy of homonuclear spin pairs and proton connectivities in solids
    • J. Gottwald D.E. Demco R. Graf H.W. Spiess High-resolution double-quantum NMR spectroscopy of homonuclear spin pairs and proton connectivities in solids Chem. Phys. Lett. 243 1995 314 323
    • (1995) Chem. Phys. Lett. , vol.243 , pp. 314-323
    • Gottwald, J.1    Demco, D.E.2    Graf, R.3    Spiess, H.W.4
  • 41
    • 0002960267 scopus 로고
    • Recoupling of homo- and heteronuclear dipolar interaction in rotating solids
    • A.E. Bennett R.G. Griffin S. Vega Recoupling of homo- and heteronuclear dipolar interaction in rotating solids P. Diehl E. Fluck H. Günter R. Kosfeld J. Seelig NMR Basic Principles and Progress 1994 Springer-Verlag Berlin 1 77
    • (1994) , pp. 1-77
    • Bennett, A.E.1    Griffin, R.G.2    Vega, S.3
  • 42
    • 0021114895 scopus 로고
    • Application of phase-sensitive two-dimensional correlated spectroscopy (COSY) for measurements of 1H–1H spin–spin coupling constants in proteins
    • 1H spin–spin coupling constants in proteins Biochem. Biophys. Res. Commun. 113 1983 967 974
    • (1983) Biochem. Biophys. Res. Commun. , vol.113 , pp. 967-974
    • Marion, D.1    Wüthrich, K.2
  • 44
    • 0030834723 scopus 로고    scopus 로고
    • Dipolar couplings and internuclear distances by double-quantum nuclear magnetic resonance spectroscopy of solids
    • R. Graf D.E. Demco J. Gottwald S. Hafner H.W. Spiess Dipolar couplings and internuclear distances by double-quantum nuclear magnetic resonance spectroscopy of solids J. Chem. Phys. 106 1997 885 895
    • (1997) J. Chem. Phys. , vol.106 , pp. 885-895
    • Graf, R.1    Demco, D.E.2    Gottwald, J.3    Hafner, S.4    Spiess, H.W.5
  • 45
    • 0141803269 scopus 로고    scopus 로고
    • Highly ordered columnar structures from hexa-peri-hexabenzocoronenes—Synthesis, X-ray diffraction, and solid-state hetero nuclear multiple-quantum NMR investigations
    • A. Fechtenkötter K. Saalwächter M.A. Harbison K. Müllen H.W. Spiess Highly ordered columnar structures from hexa- peri -hexabenzocoronenes—Synthesis, X-ray diffraction, and solid-state hetero nuclear multiple-quantum NMR investigations Angew. Chem. Int. Ed. Engl. 38 1999 3039 3042
    • (1999) Angew. Chem. Int. Ed. Engl. , vol.38 , pp. 3039-3042
    • Fechtenkötter, A.1    Saalwächter, K.2    Harbison, M.A.3    Müllen, K.4    Spiess, H.W.5
  • 46
    • 0031578999 scopus 로고    scopus 로고
    • Pulsed field gradient multiple-quantum MAS NMR spectroscopy of half-integer spin quadrupolar nuclei
    • C.A. Fyfe J. Skibsted H. Grondey H.M.zu Altenschildesche Pulsed field gradient multiple-quantum MAS NMR spectroscopy of half-integer spin quadrupolar nuclei Chem. Phys. Lett. 281 1997 44 48
    • (1997) Chem. Phys. Lett. , vol.281 , pp. 44-48
    • Fyfe, C.A.1    Skibsted, J.2    Grondey, H.3    Altenschildesche, H.M.zu4
  • 48
    • 0001048159 scopus 로고    scopus 로고
    • Pulsed field gradient selection in two-dimensional magic angle spinnig NMR spectroscopy of dipolar solids
    • T. Fritzhanns S. Hafner D.E. Demco H.W. Spiess F.H. Laukien Pulsed field gradient selection in two-dimensional magic angle spinnig NMR spectroscopy of dipolar solids J. Magn. Reson. 134 1998 355 359
    • (1998) J. Magn. Reson. , vol.134 , pp. 355-359
    • Fritzhanns, T.1    Hafner, S.2    Demco, D.E.3    Spiess, H.W.4    Laukien, F.H.5
  • 49
    • 0034724241 scopus 로고    scopus 로고
    • A 1H double-quantum magic-angle spinning solid-state NMR investigation of packing and dynamics in triphenylene and hexabenzocoronene derivatives
    • 1H double-quantum magic-angle spinning solid-state NMR investigation of packing and dynamics in triphenylene and hexabenzocoronene derivatives J. Mol. Struct. 521 2000 179 195
    • (2000) J. Mol. Struct. , vol.521 , pp. 179-195
    • Brown, S.P.1    Schnell, I.2    Brand, J.D.3    Müllen, K.4    Spiess, H.W.5
  • 51
    • 85120237245 scopus 로고
    • J.-M. Lehn Supramolecular Chemistry 1995 VCH New York
    • (1995)
    • Lehn, J.-M.1
  • 52
    • 85120214084 scopus 로고    scopus 로고
    • F. H. Beijer, Ph.D. thesis, Eindhoven University of Technology, The Netherlands, 1998.
  • 58
    • 85120217389 scopus 로고    scopus 로고
    • 2, scale.
  • 59
    • 0028501497 scopus 로고
    • Multiple-quantum nuclear magnetic resonance spectroscopy of coupled spin 1/2 in solids: Combination with cross polarization and magic-angle spinning
    • Y. Ba S. Veeman Multiple-quantum nuclear magnetic resonance spectroscopy of coupled spin 1/2 in solids: Combination with cross polarization and magic-angle spinning Solid State NMR 3 1994 249
    • (1994) Solid State NMR , vol.3 , pp. 249
    • Ba, Y.1    Veeman, S.2
  • 60
    • 85120235944 scopus 로고    scopus 로고
    • 1H-related MAS correlations in deuterated peptides, 22nd Discussion Meeting, Gesellschaft Deutscher Chemiker—Fachgruppe Magnetische Resonanzspektroskopie, Regensburg, Germany, 2000.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.