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note
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-3 was observed at the center of the porphyrin cavity. This result was repeated for several different crystals and was interpreted therefore as a partial zinc atom, present in ca. 8% of the porphyrin molecules, probably as a result of incomplete demetalation during acidic workup in this particular sample. It should be noted that the structure of m-Fb-1 differs dramatically from that of m-Zn-1 (reported herein), and we conclude therefore that the gross structure is that of the free-base form. Literal interpretation of the X-ray results would suggest that the crystals analyzed actually comprise solid solutions of ca. 8% m-Zn-1 in a lattice of m-Fb-1.
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Sanders, J.K.M.3
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