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2 in this order. Bottles were under an argon atmosphere. The purified NO was bubbled through a previously degassed stirred stock solution at room temperature for an appropriate time
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2=0.112. The X-ray crystallographic structure of 2a is shown in Figure 1. The crystallographic data has been deposited at the Cambrigde Crystallographic Data Centre as Supplementary Publication No. CCDC-212523.
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