Functionalization of the macropolyhedral borate anion cluster [B22H22]2-: Isolation and characterization of the OH and OEt derivatives

Journal of Organometallic Chemistry

Volumn 680, Issue 1-2, 2003, Pages 212-217

  Volkov, O ^a,b   Rath, N P ^b   Barton, L ^b  

^a NIKOLAEV INSTITUTE OF INORGANIC CHEMISTRY   (Russian Federation)

^b UNIVERSITY OF MISSOURI ST LOUIS   (United States)

Author keywords

Boranes; Boron hydrides; Macropolyhedral borane clusters; NMR spectroscopy; X ray diffraction

Indexed keywords

ALCOHOL; ANION; BORANE DERIVATIVE; BORIC ACID; HYDROXIDE;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL BOND; CHEMICAL REACTION; CLUSTER ANALYSIS; CONTROLLED STUDY; CRYSTAL STRUCTURE; ISOLATION PROCEDURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REPRODUCIBILITY; STRUCTURE ANALYSIS; THIN LAYER CHROMATOGRAPHY; X RAY DIFFRACTION;

EID: 0042389518     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(03)00350-4     Document Type: Article

References (42)

1. L. Barton, T.P. Onak, Species containing more than l2 boron atoms, in: Gmelin Handbuch der Anorganischen Chemie, Erg-Werk, Borverbindungen 20, Vol. 54, 1979, pp. 240-304.
2. Bould J. Clegg W. Teat S.J. Barton L. Rath N.P. Thornton-Pett M. Kennedy J.D. Inorg. Chim. Acta 289 1999 95
3. J. Bould, J.D. Kennedy, L. Barton, N.P. Rath, J. Chem. Soc. Chem. Commun. (1997) 2405.
4. Yao H.-J. Hu C.-H. Sun J. Jin R.-S. Zheng P.-J. Bould J. Greatrex R. Kennedy J.D. Ormsby D.L. Thornton-Pett M. Collect. Czech. Chem. Commun. 64 1999 927
5. M.F. Hawthorne, K. Shelly, F. Li, Chem. Commun. (2002) 547.
6. Hawthorne M.F. in: Siebert W. (Ed.), Advances in Boron Chemistry 1997 261 Royal Society of Chemistry London
7. Hawthorne M.F. in: Davidson M.G. Hughes A.K. Marder T.B. Wade K. (Eds.), Contemporary Boron Chemistry 2000 197 Royal Society of Chemistry London
8. Hawthorne M.F. Mol. Med. Today 4 1998 174
9. Soloway A.H. Tjarks W. Barnum B. Rong F.G. Barth R.F. Codogni I.M. Wilson J.G. Chem. Rev. 98 1998 1515
10. B. Larsson, J. Crawford, R. Weinreich (Eds.), Advances in Neutron Capture Therapy: Chemistry and Biology, Vol. 2, Elsevier, Amsterdam, 1997.
11. Hawthorne M.F. Maderna A. Chem. Rev. 99 1999 3421
12. M.F. Hawthorne, K. Shelly, R.J. Wiersema (Eds.), Proceedings of the Eighth International Symposium Frontiers in Neutron Capture Therapy, Vol. 1, 13-18 September 1998, Los Angeles, CA, 2001, 759 pp. and references therein.
13. Kaszynski P. ACS Symp. Ser. 798 2001 68
14. Pitochelli A.R. Hawthorne M.F. J. Am. Chem. Soc. 82 1960 3228
15. Pitochelli A.R. Hawthorne M.F. J. Am. Chem. Soc. 84 1962 3218
16. Hosmane N.S. Franken A. Zhang G. Srivastava R.R. Smith R.Y. Spielvogel B.F. Main Group Met. Chem. 21 1998 319
17. Volkov O. Dirk W. Englert U. Paetzold P. Z. Anorg. Allg. Chem. 625 1999 1193
18. T. Jelinek, J.D. Kennedy, B. Stibr, J. Chem. Soc. Chem. Commun. (1994) 1415.
19. J. Bould, W. Clegg, J.D. Kennedy, S.J. Teat, M. Thornton-Pett, J. Chem. Soc. Dalton. Trans. (1997) 2005.
20. Bould J. Barrett S.A. Barton L. Rath N.P. Kennedy J.D. Inorg. Chem. Commun. 1 1998 365
21. Sivaev I.B. Bregadze V.I. Sjoberg S. in: Davidson M.G. Hughes A.K. Marder T.B. Wade K. (Eds.), Contemporary Boron Chemistry 2000 135 Royal Society of Chemistry London
22. J. Bould, U. Doerfler, W. Clegg, S.J. Teat, M. Thornton-Pett, J.D. Kennedy, Chem. Commun. (2001) 1788.
23. Peymann T. Knobler C.B. Hawthorne M.F. J. Am. Chem. Soc. 121 1999 5601
24. Peymann T. Knobler C.B. Khan S.I. Hawthorne M.F. J. Am. Chem. Soc. 123 2001 2182
25. Peymann T. Knobler C.B. Khan S.I. Hawthorne M.F. Inorg. Chem. 40 2001 1291
26. Herzog A. Callahan R.P. Macdonald C.L.B. Lynch V.M. Hawthorne M.F. Lagow R.J. Angew. Chem. Int. Ed. Engl. 40 2001 2121
27. Maderna A. Knobler C.B. Hawthorne M.F. Angew. Chem. Int. Ed. Engl. 40 2001 1662
28. Peymann T. Knober C.B. Khan S.I. Hawthorne M.F. Angew. Chem. Int. Ed. Engl. 40 2001 1664
29. J. Thomas, M.F. Hawthorne, Chem. Commun. (2001) 1884.
30. Herzog A. Knobler C.B. Khan S.I. Hawthorne M.F. J. Am. Chem. Soc. 123 2001 12791
31. Wiersema R.J. Middaugh R.L. J. Am. Chem. Soc. 89 1967 5078
32. Wiersema R.J. Middaugh R.L. Inorg. Chem. 8 1969 2074
33. Wiersema R.J. Middaugh R.L. J. Am. Chem. Soc. 92 1970 223
34. Bechtold R. Kaczmarczyk A. J. Am. Chem. Soc. 96 1974 5953
35. Bruker Analytical X-ray, Madison, WI, 2001.
36. Blessing R.H. Acta Crystallogr. A 51 1995 33
37. G.M. Sheldrick, Bruker Analytical X-ray Division, Madison, WI, 2001.
38. Gaines D.F. Nelson C.K. Steehler G.A. J. Am. Chem. Soc. 106 1984 7266
39. Bould J. Greatrex R. Kennedy J.D. Ormsby D. Londesborough M. Callaghan K.L.F. Thornton-Pett M. Spalding T.R. Teat S.J. Clegg W. Fang H. Rath N.P. Barton L. J. Am. Chem. Soc. 124 2002 7229
40. Tippe A. Hamilton W.C. Inorg. Chem. 8 1969 464
41. Leonowicz M.E. Scholer F.R. Inorg. Chem. 19 1980 122
42. M.A. Fox, A.K. Hughes, J.M. Malget, J. Chem. Soc. Dalton Trans. (2002) 3505.