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Loaded silicon nitride tips (Thermomicroscopes, triangular, spring constant 0.06 N/m) were prepared by immersion in a 10 μM ethanolic solution of dendrimer (Aldrich, U.K.) for 5 s and then left to air-dry for 5 min prior to use. Si(100) wafers were used as supplied from Compart Technology, U.K.
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Loaded silicon nitride tips (Thermomicroscopes, triangular, spring constant 0.06 N/m) were prepared by immersion in a 10 μM ethanolic solution of dendrimer (Aldrich, U.K.) for 5 s and then left to air-dry for 5 min prior to use. Si(100) wafers were used as supplied from Compart Technology, U.K.
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Experiments were conducted using an Eastcoast Scientific AFM, with a quadrant photodetector allowing simultaneous topographic and friction force measurements. Contact mode AFM was performed in air at 19.5 ± 0.5 °C and relative humidity of 52 ± 2%.
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Experiments were conducted using an Eastcoast Scientific AFM, with a quadrant photodetector allowing simultaneous topographic and friction force measurements. Contact mode AFM was performed in air at 19.5 ± 0.5 °C and relative humidity of 52 ± 2%.
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