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Crown-6=1,7,10,13,16-hexaoxacyclooctadecane.
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0343783424
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60 polyhedra suggest that, besides the main orientation, a much smaller population of a second molecule, which is rotated by 90° about the K3-K4 axis of the main species, is also present. The molecule with this secondary orientation breaks the mirror plane. A refinement of two further fullerene molecules as well as the main species is not possible because of the correlation between the parameters. A twinned model fitting the data in an analogous manner does not lead to any improvement in the refinement. Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-138621. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: (+44) 1223-336-033; e-mail: deposit@ccdc.cam. ac.uk).
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