Speciation of sulphur in soils and soil particles by X-ray spectromicroscopy

European Journal of Soil Science

Volumn 54, Issue 2, 2003, Pages 423-433

  Prietzel, J ^a   Thieme, J ^b   Neuhausler U ^c   Susini, J ^c   Kogel Knabner I ^a  

^a TECHNICAL UNIVERSITY OF MUNICH   (Germany)

^b UNIVERSITY OF GÖTTINGEN   (Germany)

^c EUROPEAN SYNCHROTRON RADIATION FACILITY   (France)

Author keywords

[No Author keywords available]

Indexed keywords

COLLOID; FOREST SOIL; SOIL AGGREGATE; SOIL ANALYSIS; SPECIATION (CHEMISTRY); SULFUR; X-RAY SPECTROSCOPY;

EID: 0038725646     PISSN: 13510754     EISSN: None     Source Type: Journal    
DOI: 10.1046/j.1365-2389.2003.00543.x     Document Type: Article

References (27)

1. Barrett, R., Kaulich, B., Salomé, M. & Susini, J. 2000. Current status of the Scanning X-ray microscope at the ESRF. In: X-Ray Microscopy: 6th International Conference, August 2-6, 1999, Berkeley, CA (eds W. Meyer-Ilse, T. Warwick & D. Attwood), p. 458. American Institute of Physics, Melville, NY.
2. David, C., Kaulich, B., Barrett, R., Salomé, M. & Susini, J. 2000. High-resolution lenses for sub-100 nm X-ray fluorescence microscopy. Applied Physics Letters, 77, 3851-3853.
3. DeLong, W.A. & Lowe, L.E. 1961. Note on carbon-bonded sulphur in soil. Canadian Journal of Soil Science, 42, 233.
4. Dick, W.A. & Tabatabai, M.A. 1979. Ion chromatographic determination of sulfate and nitrate in soils. Soil Science Society of America Journal, 43, 899-904.
5. Fitzgerald, J.W. 1976. Sulfate ester formation and hydrolysis: a potentially important, yet often ignored aspect of the sulfur cycle of aerobic soils. Bacteriological Reviews, 40, 689-721.
6. Freney, J.R. 1961. Some observations on the nature of organic sulphur compounds in soil. Australian Journal of Agriculture Research, 12, 424-432.
7. Freney, J.R., Melville, G.E. & Williams, C.H. 1970. The determination of carbon-bonded sulfur in soil. Soil Science, 109, 310-318.
8. Howarth, R.W., Stewart, J.W.B. & Ivanov, M.V. 1992. Sulphur Cycling on the Continents. Scientific Committee on Problems of the Environment, SCOPE 48. John Wiley & Sons, Chichester.
9. Morra, M.J., Fendorf, S.E. & Brown, P.D. 1997. Speciation of sulfur in humic and fulvic acids using X-ray absorption near-edge structure (XANES) spectroscopy. Geochimica et Cosmochimica Acta, 61, 683-688.
10. Pickering, I.J., Prince, R.C., Divers, T. & George, G.N. 1998. Sulfur K-edge X-ray absorption for determining the chemical speciation of sulfur in biological systems. Federation of European Biochemical Societies Letters, 441, 11-14.
11. Prange, A., Arzberger, I., Engemann, C., Modrow, H., Schumann, O., Trüper, H.G., Steudel, R., Dahl, C. & Hormes, J. 1999. In situ analysis of sulfur in the sulfur globules of phototrophic sulfur bacteria by X-ray absorption near edge spectroscopy. Biochimica et Biophysica Acta, 1428, 446-454.
12. Prietzel, J. & Hirsch, C. 2000. Ammonium fluoride extraction for determining inorganic sulphur in acid forest soils. European Journal of Soil Science, 51, 323-333.
13. Pruden, G. & Bloomfield, C. 1968. The determination of Fe(II) sulphide in soils in the presence of Fe(III) oxide. Analyst, 93, 532-534.
14. Ressler, T. 1998. WinXAS: a program for X-ray absorption spectroscopy data analysis under MS-Windows. Journal of Synchrotron Radiation, 5, 112-118.
15. Rompel, A., Cinco, R.M., Latimer, M.J., McDermott, A.E., Guiles, R.D., Quintanilha, A. et al. 1998. Sulfur K-edge X-ray absorption spectroscopy: a spectroscopic tool to examine the redox state of S-containing metabolites in vivo. Proceedings of the National Academy of Sciences of the USA, 95, 6122-6127.
16. Sarret, G., Connan, J., Kasrai, M., Bancroft, G.M., Charrié-Duhaut, A., Lemoine, S. et al. 1999. Chemical forms of sulfur in geological and archaeological asphaltenes from Middle East, France, and Spain determined by sulfur K- and L-edge X-ray absorption near-edge structure spectroscopy. Geochimica et Cosmochimica Acta, 63, 3767-3779.
17. Spiro, C.L., Wong, J., Lytle, F.W., Gregor, R.B., Maylotte, D.H. & Lamson, S.H. 1984. X-ray absorption spectroscopic investigation of sulfur sites in coal: Organic sulfur identification. Science (Washington DC), 226, 48-50.
18. Strehl, C. & Prietzel, J. 1998. Method for the partitioning of organic sulphur in forest soil O layers. Soil Biology and Biochemistry, 30, 1725-1731.
19. Strehl, C. & Prietzel, J. 1999. Simple and rapid determination of thiol- and disulfide sulfur in foliage and humic soil horizons. Journal of Plant Nutrition and Soil Science, 162, 511-516.
20. 3. Journal of Chemistry and Physics, 74, 215-217.
21. Tabatabai, M.A. & Bremner, J.M. 1972. Forms of sulfur, and carbon, nitrogen and sulfur relationships in Iowa soils. Soil Science, 114, 380-386.
22. Vairavamurthy, A., Maletic, D., Wang, S., Manowitz, B., Eglinton, T. & Lyons, T. 1997. Characterization of sulfur-containing functional groups in sedimentary humic substances by X-ray absorption near-edge spectroscopy. Energy and Fuels, 11, 546-553.
23. Vairavamurthy, A., Zhou, W., Eglinton, T. & Manowitz, B. 1994. Sulfonates: a novel class of organic sulfur compounds in marine sediments. Geochimica et Cosmochimica Acta, 58, 4681-4687.
24. Waldo, G.S., Carlson, R.M.K., Moldovan, J.M., Peters, K.E. & Penner-Hahn, J.E. 1991. Sulfur speciation in heavy petroleums: information from x-ray absorption near-edge structure. Geochimica et Cosmochimica Acta, 55, 801-814.
25. Xia, K., Weesner, F., Bleam, W.F., Bloom, P.R., Skyllberg, U.L. & Helmke, P.A. 1998. XANES studies of oxidation states of sulfur in aquatic and soil humic substances. Soil Science Society of America Journal 62, 1240-1246.
26. Xia, K., Skyllberg, U.L., Bleam, W.F., Bloom, P.R., Nater, E.A. & Helmke, P.A. 1999. X-ray absorption spectroscopic evidence for the complexation of Hg(II) by reduced sulfur in soil humic substances. Environmental Science and Technology, 33, 257-261.
27. Zhabina, N.N. & Volkov, I.I. 1978. A method for determination of various sulfur compounds in sea sediments and rocks. In: Environmental Biogeochemistry and Geomicrobiology: Methods, Metals, and Assessment, Volume 3 (ed. W.E. Krumbein), pp. 735-746. Ann Arbor Science, Ann Arbor, MI.