-
3
-
-
0034712156
-
-
Wolfe, J. P.; Tomori, H.; Sadighi, J. P.; Yin, J.; Buchwald, S. L. J. Org. Chem. 2000, 65, 1158.
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J. Org. Chem.
, vol.65
, pp. 1158
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-
Wolfe, J.P.1
Tomori, H.2
Sadighi, J.P.3
Yin, J.4
Buchwald, S.L.5
-
4
-
-
0011411784
-
-
2 could offer a partial solution to this problem, this was both experimentally complicated and still had a fairly narrow substrate scope (e.g., no primary aliphatic amines, no acyclic secondary amines): Harris, M. C.; Huang, X.; Buchwald, S. L. Org. Lett. 2002, 4, 2885.
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Org. Lett.
, vol.4
, pp. 2885
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-
Harris, M.C.1
Huang, X.2
Buchwald, S.L.3
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5
-
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0032560932
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-
Old, D. W.; Wolfe, J. P.; Buchwald, S. L. J. Am. Chem. Soc. 1998, 120, 9722.
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(1998)
J. Am. Chem. Soc.
, vol.120
, pp. 9722
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Old, D.W.1
Wolfe, J.P.2
Buchwald, S.L.3
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6
-
-
0032578172
-
-
(a) Hamann, B. C.; Hartwig, J. F. J. Am. Chem. Soc. 1998, 120, 7369. (b) Hartwig, J. F.; Hamann, B. C. U.S. Patent 6,235,938, 2001. Ni-catalyzed coupling of sulfoximines with aryl tosylates: (c) Bolm, C.; Hildebrand, J. P.; Rudolph, J. Synthesis 2000, 911.
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J. Am. Chem. Soc.
, vol.120
, pp. 7369
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Hamann, B.C.1
Hartwig, J.F.2
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7
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0032578172
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U.S. Patent 6,235,938, 2001
-
(a) Hamann, B. C.; Hartwig, J. F. J. Am. Chem. Soc. 1998, 120, 7369. (b) Hartwig, J. F.; Hamann, B. C. U.S. Patent 6,235,938, 2001. Ni-catalyzed coupling of sulfoximines with aryl tosylates: (c) Bolm, C.; Hildebrand, J. P.; Rudolph, J. Synthesis 2000, 911.
-
-
-
Hartwig, J.F.1
Hamann, B.C.2
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8
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-
0032578172
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-
(a) Hamann, B. C.; Hartwig, J. F. J. Am. Chem. Soc. 1998, 120, 7369. (b) Hartwig, J. F.; Hamann, B. C. U.S. Patent 6,235,938, 2001. Ni-catalyzed coupling of sulfoximines with aryl tosylates: (c) Bolm, C.; Hildebrand, J. P.; Rudolph, J. Synthesis 2000, 911.
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Synthesis
, vol.911
-
-
Bolm, C.1
Hildebrand, J.P.2
Rudolph, J.3
-
9
-
-
0011720666
-
-
Ligand 1 is commercially available from Strem Chemical. (a) Kaye, S.; Fox, J. M.; Hicks, F. A.; Buchwald, S. L. Adv. Synth. Catal. 2001, 343, 789. (b) Tomori, M.; Fox, J. M.; Buchwald, S. L. J. Org. Chem. 2000, 65, 5334.
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Adv. Synth. Catal.
, vol.343
, pp. 789
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Kaye, S.1
Fox, J.M.2
Hicks, F.A.3
Buchwald, S.L.4
-
10
-
-
0034714545
-
-
Ligand 1 is commercially available from Strem Chemical. (a) Kaye, S.; Fox, J. M.; Hicks, F. A.; Buchwald, S. L. Adv. Synth. Catal. 2001, 343, 789. (b) Tomori, M.; Fox, J. M.; Buchwald, S. L. J. Org. Chem. 2000, 65, 5334.
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J. Org. Chem.
, vol.65
, pp. 5334
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Tomori, M.1
Fox, J.M.2
Buchwald, S.L.3
-
11
-
-
0033544422
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Wagaw, S.; Yang, B. H.; Buchwald, S. L. J. Am. Chem. Soc. 1999, 121, 10251.
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(1999)
J. Am. Chem. Soc.
, vol.121
, pp. 10251
-
-
Wagaw, S.1
Yang, B.H.2
Buchwald, S.L.3
-
12
-
-
0037140736
-
-
Only a few examples of the coupling of amides with aryl triflates have been disclosed, cf.: Yin, J.; Buchwald, S. L. J. Am. Chem. Soc. 2002, 124, 6043.
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J. Am. Chem. Soc.
, vol.124
, pp. 6043
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Yin, J.1
Buchwald, S.L.2
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13
-
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0038276940
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For a Pd-catalyzed oxidation reaction accelerated by t-BuOH as a cosolvent, see: Bagdanoff, J. T.; Ferreira, E. M.; Stolz, B. M. Org. Lett. 2003, 5, 835.
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Org. Lett.
, vol.5
, pp. 835
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Bagdanoff, J.T.1
Ferreira, E.M.2
Stolz, B.M.3
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14
-
-
0038332036
-
-
note
-
In preliminary experiments, primary and secondary alcohols provided poor results while tert-amyl alcohol was a suitable solvent.
-
-
-
-
15
-
-
0037178121
-
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Klapars, A.; Huang, X.; Buchwald, S. L. J. Am. Chem. Soc. 2002, 124, 7421.
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J. Am. Chem. Soc.
, vol.124
, pp. 7421
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Klapars, A.1
Huang, X.2
Buchwald, S.L.3
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16
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-
0034794463
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Klapars, A.; Antilla, J. C.; Huang, X.; Buchwald, S. L. J. Am. Chem. Soc. 2001, 123, 7727.
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(2001)
J. Am. Chem. Soc.
, vol.123
, pp. 7727
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Klapars, A.1
Antilla, J.C.2
Huang, X.3
Buchwald, S.L.4
-
18
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-
0037149057
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Kwong, F. Y.; Klapars, A.; Buchwald, S. L. Org. Lett. 2002, 4, 581.
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(2002)
Org. Lett.
, vol.4
, pp. 581
-
-
Kwong, F.Y.1
Klapars, A.2
Buchwald, S.L.3
-
19
-
-
0037031625
-
-
Aqueous hydroxide as a base for palladium-catalyzed amination has been reported; however, a phase transfer catalyst and toluene cosolvent were required: (a) Kuwano, R.; Utsunomiya, M.; Hartwig, J. F. J. Org. Chem. 2002, 67, 6479. For the use of solid NaOH in dioxane, see: (b) Grasa, G. A.; Viciu, M. S.; Huang, J.; Nolan, S. P. J. Org. Chem. 2001, 66, 7729.
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J. Org. Chem.
, vol.67
, pp. 6479
-
-
Kuwano, R.1
Utsunomiya, M.2
Hartwig, J.F.3
-
20
-
-
0035900483
-
-
Aqueous hydroxide as a base for palladium-catalyzed amination has been reported; however, a phase transfer catalyst and toluene cosolvent were required: (a) Kuwano, R.; Utsunomiya, M.; Hartwig, J. F. J. Org. Chem. 2002, 67, 6479. For the use of solid NaOH in dioxane, see: (b) Grasa, G. A.; Viciu, M. S.; Huang, J.; Nolan, S. P. J. Org. Chem. 2001, 66, 7729.
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(2001)
J. Org. Chem.
, vol.66
, pp. 7729
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Grasa, G.A.1
Viciu, M.S.2
Huang, J.3
Nolan, S.P.4
-
21
-
-
0032510005
-
-
- could be used instead of 1 with comparable results. (a) Nishiyama, M.; Yamamoto, T.; Koie, Y. Tetrahedron Lett. 1998, 39, 617. (b) Netherton, M. R.; Fu, G. C. Org. Lett. 2001, 3, 4295.
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(1998)
Tetrahedron Lett.
, vol.39
, pp. 617
-
-
Nishiyama, M.1
Yamamoto, T.2
Koie, Y.3
-
22
-
-
0035961019
-
-
- could be used instead of 1 with comparable results. (a) Nishiyama, M.; Yamamoto, T.; Koie, Y. Tetrahedron Lett. 1998, 39, 617. (b) Netherton, M. R.; Fu, G. C. Org. Lett. 2001, 3, 4295.
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(2001)
Org. Lett.
, vol.3
, pp. 4295
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Netherton, M.R.1
Fu, G.C.2
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23
-
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0037416262
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3/1 is more convenient and therefore recommended in the majority of cases. For studies on palladacycles of this type, see: Bedford, R. B.; Cazin, C. S. J.; Coles, S. J.; Gelbrich, T.; Horton, P. N.; Hursthouse, M. B.; Light, M. E. Organometallics 2003, 22, 987.
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(2003)
Organometallics
, vol.22
, pp. 987
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Bedford, R.B.1
Cazin, C.S.J.2
Coles, S.J.3
Gelbrich, T.4
Horton, P.N.5
Hursthouse, M.B.6
Light, M.E.7
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