Halide-Bridged Palladium(II) Dimers of Orthometalated (S)-(+)-N,N-Dimethyl-α-methylbenzylamine and (S)-(+)-N,N-Dimethyl[1-(2-naphthyl)ethyl]amine: Solution and Solid-State Structures and Reactions with 3,4-Dimethyl-1-phenylphosphole and Allyldiphenylphosphine

Organometallics

Volumn 19, Issue 1, 2000, Pages 91-104

  Gül, Nizamettin ^a   Nelson, John H ^a  

^a UNIVERSITY OF NEVADA   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0038486450     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om990681a     Document Type: Article

References (52)

1. Wild, S. E. Coord. Chem. Rev. 1997, 166, 291.
2. (a) Kyba, E. P.; Rines, S. P. J. Org. Chem. 1982, 47, 4800.
3. (b) Nelson, J. H. Coord. Chem. Rev. 1995, 139, 245.
4. (a) Leung, P.-H.; Loh, S. K.; Mok, K. F.; White, A. J. P.; Williams, D. J. J. Chem. Soc., Chem. Commun. 1996, 591.
5. (b) Aw, B. H.; Leung, P.-H.; White, A. J. P.; Williams, D. J. Orgonometallics, 1996, 15, 3640.
6. (c) Selvaratnam, S.; Mok, K. F.; Leung, P.-H.; White, A. J. P.; Williams, D. J. Inorg. Chem, 1996, 35, 4798.
7. (d) Leung, P.-H.; Loh, S. K.; Mok, K. F.; White, A. J. P.; Williams, D. J. J. Chem. Soc., Dalton Trans. 1996, 4443.
8. (e) Aw, B. H.; Hor, T. S. A.; Selvaratnam, S.; White, A. J. P.; Williams, D. J.; Rees, N. H.; McFarlane, W.; Leung, P.-H. Inorg. Chem. 1997, 36, 2138.
9. (f) Leung, P.-H.; Selvaratnam, S.; Cheng, C. R.; Mok, K. F.; Rees, N. H.; McFarlane, W. J. Chem. Soc., Chem. Commun. 1997, 751.
10. (g) Liu, A. M.; Mok, K. F.; Leung, P.-H. J. Chem. Soc., Chem. Commun. 1997, 239.
11. (h) Leung, P.-H.; Siah, S. Y.; White, A. J. P.; Williams, D. J. Chem. Soc., Dalton Trans. 1998, 893.
12. (i) Song, Y.; Vittal, J. J.; Chan, S.-H.; Leung, P.-H. Organometallics 1999, 18, 650.
13. (j) Gül, N.; Nelson, J. H. Tetrahedron, in press.
14. (k) Lang, H.; Vittal, J. J.; Leung, P.-H. J. Chem. Soc., Dalton Trans. 1998, 2109.
15. (l) Leung, P.-H.; Liu, A.; Mok, K. F. Tetrahedron: Asymmetry, 1999, 10, 1309.
16. Hockless, D. C. R.; Gugger, P. A.; Leung, P.-H.; Mayadunne, R. C.; Pabel, M.; Wild, S. B. Tetrahedron, 1997, 53, 4083.
17. (a) Turner, E. E.; Harris, M. M. Q. Rev. 1947, 1, 299.
18. (b) Jacques, J.; Collet, A.; Wilen, S. H. Enantiomers, Racemates and Resolutions; Wiley-Interscience: New York, 1981; pp 371-377.
19. Hockless, D. C. R.; Gugger, P. A.; Wild, S. B. Unpublished work cited in ref 1.
20. Tani, K.; Brown, L. D.; Ahmed, J.; Ibers, J. A.; Yokota, M.; Nakamura, A.; Otsuka, S. J. Am. Chem. Soc. 1997, 99, 77876.
21. Gül, N.; Nelson, J. H. J. Mol. Struct. 1999, 475, 121.
22. Gül, N.; Nelson, J. H. Organometallics 1999, 18, 709.
23. Gül, N.; Nelson, J. H. Polyhedron 1999, 18, 1835.
24. (a) Attar, S.; Catalano, V. J.; Nelson, J. H. Organometallics 1996, 15, 2932.
25. (b) Attar, S.; Nelson, J. H.; Fischer, J.; De Cian, A.; Sutter, J.-P.; Pfeffer, M. Organometallics 1995, 14, 4559.
26. (c) Hansen, H. D.; Maitra, K.; Nelson, J. H. Inorg. Chem. 1999, 38, 2150.
27. (a) Van der Schaaf, P. A.; Boersma, J.; Kooijman, H.; Speck, A. L.; Van Koten, G. Organometallics 1993, 12, 4334.
28. (b) Alcock, N. W.; Hulmes, D. I.; Brown, J. M. J. Chem. Soc., Chem. Commun. 1995, 395.
29. (c) Jiang, Q.; Rüegger, H.; Venanzi, L. M. J. Organomet. Chem. 1995, 488, 233. The first two citations claim that equatorial carbon-methyl groups are rarely found in complexes of these types of ligands, whereas the third claims that they are found approximately 50% of the time for such rings.
30. (a) Appleton, T. G.; Clark, H. C.; Manzer, L. E. Coord. Chem. Rev. 1973, 10, 335.
31. (b) Gofman, M. M.; Nefedov, V. I. Inorg. Chim. Acta 1978, 28, 1.
32. Sandstorm, J. Dynamic NMR Spectroscopy; Academic: New York, 1982.
33. Gutmann, V. The Donor-Acceptor Approach to Molecular Interactions; Plenum: New York, 1978.
34. Redwine, K. D.; Wilson, W. L.; Moses, D. G.; Catalano, V. J.; Nelson, J. H. Inorg. Chem., submitted for publication.
35. Wilson, W. L.; Fischer, J.; Wasylishen, R. E.; Eichele, K.; Catalano, V. J.; Frederick, J. H.; Nelson, J. H. Inorg. Chem. 1996, 35, 1486.
36. (a) Kojima, T.; Saeki, K.; Ono, K.; Ohba, M.; Matsuda, Y. J. Chem. Soc., Chem. Commun. 1997, 1679.
37. (b) Gouygou, M.; Tissot, D.; Daran, J.-C.; Balavoine, C. G. A. Organometallics 1997, 16, 1008.
38. Wilson, W. L.; Rahn, J. A.; Alcock, N. W.; Fischer, J.; Frederick, J. H.; Nelson, J. H. Inorg. Chem. 1994, 33, 109.
39. (a) Mathey, F. Chem. Rev. 1988, 88, 429, and references therein.
40. (b) Holland, S.; Jeanjean, M.; Mathey, F. Angew. Chem., Int. Ed. Engl. 1997, 36, 98.
41. Maitra, K.; Catalano, V. J.; Nelson, J. H. J. Am. Chem. Soc. 1997, 119, 12560.
42. (a) Mathey, F.; Muller, G. Tetrahedron 1972, 27, 5645.
43. (b) Horner, L.; Ertel, I.; Ruprecht, H.-D.; Bélovský, O. Chem. Ber. 1970, 103, 1582.
44. Carly, A. J.; MacLaughlin, S. A.; Nucciarone, D. In Phosphorus-31 NMR Spectroscopy in Stereochemical Analysis; Quin, L. D., Verkade, J. G., Eds.; VCH: Deerfield Beach, FL, 1987; pp 559-619.
45. Garrou, P. E. Chem. Rev. 1981, 81, 229.
46. Sanger, A. R. J. Chem. Soc., Dalton Trans. 1977, 1971.
47. Morandini, F.; Consiglio, G.; Piccolo, O. Inorg. Chim. Acta 1982, 57, 15.
48. Steffan, W.-L.; Palenik, G. J. Inorg. Chem. 1976, 15, 2432.
49. Bregue, A.; Mathey, F.; Savignac, P. Synthesis 1981, 983.
50. Parkins, S.; Moezzi, B.; Hope, H. XABS2: An emperical absorption corrections program. J. Appl. Crystallogr. 1995, 53-56.
51. International Tables for X-ray Crystallography; D. Reidell Publishing Co.: Boston, 1992; Vol. C.
52. Flack, H. D. Acta Crystallogr. 1983, A39, 876.