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Volumn 4, Issue 15, 2002, Pages 2477-2480

Complete π-facial diastereoselectivity in Diels-Alder reactions of dissymmetric 2,4-cyclohexadienones

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EID: 0037825690     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol020087o     Document Type: Article
Times cited : (26)

References (35)
  • 4
    • 0002746686 scopus 로고
    • Curran, D. P., Ed.; JAI Press: Greenwich, CT, Chapter 1
    • (b) Fallis, A. G.; Lu, Y.-F. In Advances in Cycloaddition; Curran, D. P., Ed.; JAI Press: Greenwich, CT, 1993; Vol. 3, Chapter 1.
    • (1993) Advances in Cycloaddition , vol.3
    • Fallis, A.G.1    Lu, Y.-F.2
  • 5
    • 0001448958 scopus 로고    scopus 로고
    • (c) Ohwada, T. Chem. Rev. 1999, 99, 1337-1375.
    • (1999) Chem. Rev. , vol.99 , pp. 1337-1375
    • Ohwada, T.1
  • 16
    • 0001677413 scopus 로고    scopus 로고
    • For the Diels-Alder reactions with a spirolactone-cyclohexadienone, see: Drutu, I.; Njardarson, J. T.; Wood, J. L. Org. Lett. 2002, 4, 493-496.
    • (2002) Org. Lett. , vol.4 , pp. 493-496
    • Drutu, I.1    Njardarson, J.T.2    Wood, J.L.3
  • 27
    • 0042593991 scopus 로고    scopus 로고
    • note
    • General Procedure for Diels-Alder Reactions of 1. A mixture | of 2,3-cyclohexadienone 1 (0.5 mmol) and a dienophile (10 mmol. 20 equiv) was kept in a sealed tube at 100 or 150 °C for a period of time (see Tables 1-3). The reaction mixture was then cooled to room temperature and subjected to column chromatography (silica gel, ethyl acetate/hexanes) to afford pure cycloadducts.
  • 28
    • 0043094935 scopus 로고    scopus 로고
    • note
    • 13C NMR (100 or 150 MHz), DEPT, and low- and high-resolution MS analyses.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.