Metal complexes with 2,3-bis(diphenylphosphino)-1,4-diazadiene ligands: Synthesis, structures, and an intramolecular metal-mediated [4 + 2] cycloaddition employing a benzene ring as a dienophile

Inorganic Chemistry

Volumn 42, Issue 2, 2003, Pages 625-632

  Walther, Dirk ^a   Liesicke, Stefan ^a   Böttcher, Lars ^a   Fischer, Reinald ^a   Görls, Helmar ^a   Vaughan, Gavin ^b  

^a FRIEDRICH SCHILLER UNIVERSITY JENA   (Germany)

^b EUROPEAN SYNCHROTRON RADIATION FACILITY   (France)

Author keywords

[No Author keywords available]

Indexed keywords

2,3 BIS(DIPHENYLPHOSPHINO) 1,4 DIAZADIENE DERIVATIVE; ALKADIENE; METAL COMPLEX; UNCLASSIFIED DRUG;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; COMPLEX FORMATION; CRYSTAL STRUCTURE; LIGAND BINDING; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE; PROTON NUCLEAR MAGNETIC RESONANCE; SYNTHESIS;

EID: 0037467738     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic020534w     Document Type: Article

References (41)

1. Togni, A.; Venanzi, L. M. Angew. Chem. 1994, 106, 517; Angew. Chem., Int. Ed. Engl. 1994, 33, 497.
2. Togni, A.; Venanzi, L. M. Angew. Chem. 1994, 106, 517; Angew. Chem., Int. Ed. Engl. 1994, 33, 497.
3. Britovsek, G. J. P.; Gibson, V. C.; Wass, D. F. Angew. Chem. 1999, 111, 448-468; Angew. Chem., Int. Ed. 1999, 38, 429.
4. Britovsek, G. J. P.; Gibson, V. C.; Wass, D. F. Angew. Chem. 1999, 111, 448-468; Angew. Chem., Int. Ed. 1999, 38, 429.
5. Killian, C. M.; Johnson, L. K.; Brookhart, M. Organometallics 1997, 16, 2005 and references therein.
6. Knowles, W. S. Angew. Chem. 2002, 114, 2096; Angew. Chem., Int. Ed. 2002, 41, 1998 and references therein.
7. Knowles, W. S. Angew. Chem. 2002, 114, 2096; Angew. Chem., Int. Ed. 2002, 41, 1998 and references therein.
8. Chen, Y.; Kiattansakul, R.; Ma, B.; Synder, J. K. J. Org. Chem. 2001, 66, 6932.
9. Tanaka, K.; Fu, G. C. Angew. Chem. 2002, 114, 1677; Angew. Chem., Int. Ed. 2002, 41, 1603.
10. Tanaka, K.; Fu, G. C. Angew. Chem. 2002, 114, 1677; Angew. Chem., Int. Ed. 2002, 41, 1603.
11. Shultz, C. S.; DeSimone, J. M.; Brookhart, M. Organometallics 2001, 20, 16.
12. Shultz, C. S.; DeSimone, J. M.; Brookhart, M. J. Am. Chem. Soc. 2001, 123, 9172.
13. Rigaut, S.; Maury, O.; Touchard, D.; Dixneuf, P. H. Chem. Commun. 2001, 373.
14. Rigaut, S.; Monnier, F.; Mousset, F.; Touchard, D.; Dixneuf, P. H. Organometallics 2002, 21, 2654.
15. Garcia, M. H.; Robalo, M. P.; Dias, A. R.; Duarte, M. T.; Wenseelers, W.; Aerts, G.; Goovaerts, E.; Cifuntes, M. P.; Hurst, S.; Humphrey, M. G.; Samoc, M.; Luther-Davies, B. Organometallics 2002, 21, 2107.
16. Garcia, M. H.; Robalo, M. P.; Dias, A. R.; Piedade, M. F. M.; Galvao, A.; Wenseelers, W.; Goovaerts, E. J. Organomet. Chem. 2001, 619, 252.
17. Heyn, R. H.; Görbitz, C. H. Organometallics 2002, 21, 2781.
18. Melenkivitz, R.; Mindiola, D. J.; Hillhouse, G. L. J. Am. Chem. Soc. 2002, 124, 3846.
19. Mindiola, D. J.; Hillhouse, G. L. J. Am. Chem. Soc. 2001, 123, 4623.
20. Sjoevall, S.; Andersson, C.; Wendt, O. F. Organometallics 2001, 20, 4119.
21. King, R. B. In Organometallic Synthesis; Academic: New York 1965; Vol. 1, p 124.
22. Lindauer, D.; Becker, R.; Döring, M.; Fehling; P.; Goerls, H. J. Prakt. Chem. 1995, 337, 143.
23. Issleib, K.; Tzschach, A. Chem. Ber. 1959, 92, 1118.
24. Jardine, F. H.; Rule, L.; Vohra, A. G. J. Chem. Soc. A 1970, 238.
25. MOLEN, An Interactive Structure Solution Procedure; Enraf-Nonius: Delft, The Netherlands, 1990.
26. Otwinowski, Z.; Minor, W. Processing of X-Ray Diffraction Data Collected in Oscillation Mode. In Methods in Enzymology, Vol. 276, Macromolecular Crystallography, Part A; Carter, C. W., Sweet, R. M., Eds.; Academic Press: New York, 1997; pp 307-326.
27. SMART. Software for the CCD Detektor System, version 5.05: Bruker AXS: Madison, WI, 1998.
28. Sheldrick, G. M. Acta Crystallogr. 1990, A46, 467.
29. Sheldrick, G. M. SHELXTL97-2; University of Göttingen: Göttingen, Germany, 1997.
30. Saito, K.; Omura Y.; Maekawa, E. Tetrahedron Lett. 1984, 25, 2573.
31. Saito, K.; Omura Y.; Maekawa, E.; Gassmann, P. G. Bull. Chem Soc. Jpn. 1990, 63, 395.
32. Grimme, W.; Gommes, T.; Roth, W. R.; Breukmann, R. Angew. Chem. 1992, 104, 867-869; Angew. Chem., Int. Ed. Engl. 1992, 31, 872.
33. Grimme, W.; Gommes, T.; Roth, W. R.; Breukmann, R. Angew. Chem. 1992, 104, 867-869; Angew. Chem., Int. Ed. Engl. 1992, 31, 872.
34. Capuano, L.; Moersdorf, P. Liebigs Ann. Chem. 1982, 2178.
35. Ilge, H. D.; Langbein, H.; Reichenbächer, M.; Pätzold, R. J. Prakt. Chem. 1981, 323, 367.
36. Lenoble, C.; Becker, R. S. J. Phys. Chem. 1986, 90, 2651 and references therein.
37. Santiago, A.; Becker, R. S. J. Am. Chem. Soc. 1968, 90, 3654.
38. Hart, R. J.; Heller, H. G. J. Chem. Soc., Perkin Trans. 1 1972, 1321.
39. Heller, H. G.; Szewczyk, E. D. J. Chem. Soc., Perkin Trans. 1 1974, 1487.
40. Wismonski-Knittel, T.; Fischer, G.; Fischer, E. J. Chem. Soc., Perkin Trans. 2 1974, 1930.
41. Compton, R. G.; Fischer, A. C.; Wellington, R. G.; Winkler, J. J. Phys. Chem. 1992, 96, 8153.