Synthesis and x-ray crystal structure of [(THF)Zn(O2(OH)SiR)]4 (R = (2,6-i-Pr2C6H3)N(SiMe3)): Enroute to larger aggregates

Inorganic Chemistry

Volumn 42, Issue 4, 2003, Pages 970-973

  Anantharaman, Ganapathi ^a   Roesky, Herbert W ^a   Schmidt, Hans Georg ^a   Noltemeyer, Mathias ^a   Pinkas, Jiri ^b  

^a UNIVERSITY OF GÖTTINGEN   (Germany)

^b MASARYK UNIVERSITY   (Czech Republic)

Author keywords

[No Author keywords available]

Indexed keywords

DIMETHYLZINC; HYDROXYL GROUP; LITHIUM DERIVATIVE; METHYLLITHIUM; SILANE DERIVATIVE; SILICON; UNCLASSIFIED DRUG; ZINC;

ARTICLE; CHEMICAL BOND; CHEMICAL REACTION; CRYSTAL STRUCTURE; ROOM TEMPERATURE; STOICHIOMETRY; SYNTHESIS; X RAY DIFFRACTION;

EID: 0037463660     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic020514u     Document Type: Article

References (49)

1. (a) Cotton, F. A.; Wilkinson, G.; Murillo, C. A.; Bochmann, M. Advanced Inorganic Chemistry, 5th ed.; John Wiley and Sons: New York, 1999.
2. (b) Wells, A. F. Structural Inorganic Chemistry, 5th ed.; Clarendon Press: Oxford, U.K., 1984.
3. (c) Baerlocher, C.; Meier, W. M.; Olson, D. H. Atlas of Zeolite Framework Types, 5th ed.; Elsevier: Amsterdam, 2001.
4. (a) Yermanov, Y. I.; Kuznetsov, B. N.; Zakharov, V. A. Catalysis by Supported Complexes; Elsevier: Amsterdam, 1981.
5. (b) Seiyama, T.; Tanabe, K. New Horizons in Catalysis; Elsevier: Amsterdam, 1980.
6. (c) Harley, F. R. Supported Metal Complexes; Reidel: Boston, MA, 1985.
7. (d) Cornils, B.; Hermann, W. A. Applied Homogeneous Catalysis with Organometallic Compounds; VCH: Weinheim, Germany, 1996.
8. (a) Frash, M. V.; van Santen, R. A. Phys. Chem. Chem. Phys. 2000, 2, 1085.
9. (b) Kumar N.; Linfors, L.-E. Catal. Lett. 1996, 38, 239.
10. (c) Bhaumik, A.; Kumar, R. J. Chem. Soc., Chem. Commun. 1995, 869.
11. (d) Zhao, D.; Goldfarb, D. J. Chem. Soc., Chem. Commun. 1995, 875.
12. (e) Gao, H.; Suo, J.; Li, S. J. Chem. Soc., Chem. Commun. 1995, 835.
13. (f) Serano, D. P.; Li, H.-X.; Davis, M. E. J. Chem. Soc., Chem. Commun. 1992, 745.
14. (g) Ono, Y. Catal. Rev. - Sci. Eng. 1992, 34, 179.
15. (h) Cauqui, J. J.; Calvino, G.; Cifredo. L.; Esquivias, J. M.; Rodríguez-Izquierdo, J. J. Non-Cryst. Solids 1992, 147/148, 758.
16. (i) Reddy, J. S.; Kumar, R. J. Catal. 1991, 130, 440.
17. (j) Reddy, J. S.; Kumar, R.; Ratnasamy, P. Appl. Catal. 1990, 58, LI.
18. (a) Perego, G.; Ballassi, G.; Corno, C.; Tamarasso, M.; Buonuomo, F.; Esposito, A. In Studies in Surface Science and Catalysis, New Developments in Zeolite Science and Technology; Muratami, Y., Iijima, A., Word, J. W., Eds.; Elsevier: Amsterdam, 1986.
19. (b) Boccuti, M. R.; Rao, K. M.; Zecchina, A.; Leofanti, G.; Petrini, G. In Structure and Reactivity of Surfaces; Morterra, C., Zecchina, A., Costa, G., Eds.; Elsevier: Amsterdam, 1989; p 133.
20. (a) Biscardi, J. A.; Meitzner, G. D.; Iglesia, E. J. Catal. 1998, 179, 192.
21. (b) Circolo, M. F.; Norby, P.; Hanson, J. C.; Corbin, D. R.; Grey, C. P. J. Phys. Chem. B 1999, 103, 346.
22. (c) Murray, D. K.; Howard, T.; Goguen, P. W.; Krawietz, T. R.; Haw, J. F. J. Am. Chem. Soc. 1994, 116, 6354.
23. (d) Murray, D. K.; Chang, J. W.; Haw, J. F. J. Am. Chem. Soc. 1993, 115, 4732.
24. (e) Isao, M.; Czarny, Y. Z.; Oszczudlowski, J. J. Appl. Chem. 1991, 3, 187.
25. (a) Murugavel, R.; Voigt, A.; Walawalkar, M. G.; Roesky, H. W. Chem. Rev. 1996, 96, 2205.
26. (b) Voronkov, M. G.; Maletina, E. A.; Roman, V. K. Heterosiloxanes (Soviet Scientific Review Supplement, Series Chemistry, Vol. 1); Academic Press: London, 1988.
27. (c) Feher, F. J.; Budzichowski, T. A. Polyhedron 1995, 14, 3239.
28. (a) Murugavel, R.; Chandrasekhar, V.; Roesky, H. W. Acc. Chem. Res. 1996, 29, 183.
29. (b) Murugavel, R.; Bhattacharjee, M.; Roesky, H. W. Appl. Organomet. Chem. 1999, 13, 227 and further references therein.
30. (a) Walawalkar, M. G.; Roesky, H. W.; Murugavel, R. Acc. Chem. Res. 1999, 32, 117 and further references therein.
31. (b) Chakraborthy, D.; Horchler, S.; Roesky, H. W.; Noltemeyer, M.; Schmidt. H.-G. Inorg. Chem. 2000, 39, 3995.
32. (c) Roesky, H. W. Solid State Sci. 2001, 3, 777.
33. (a) Schindler, F.; Schmidbaur, H. Angew. Chem. 1967, 79, 697; Angew. Chem., Int. Ed. Engl. 1967, 6, 683.
34. (a) Schindler, F.; Schmidbaur, H. Angew. Chem. 1967, 79, 697; Angew. Chem., Int. Ed. Engl. 1967, 6, 683.
35. (b) Schindler, F.; Schmidbaur, H. Angew. Chem. 1965, 77, 865; Angew. Chem., Int. Ed. Engl. 1965, 4, 876.
36. (b) Schindler, F.; Schmidbaur, H. Angew. Chem. 1965, 77, 865; Angew. Chem., Int. Ed. Engl. 1965, 4, 876.
37. (c) Driess, M.; Merz, K.; Rell, S. Eur. J. Inorg. Chem. 2000. 2517.
38. (d) Su, K.; Tilley, T. D.; Sailor, M. J. J. Am. Chem. Soc. 1996, 118, 3459.
39. Anantharaman, G.; Reddy, N. D.; Roesky, H. W.; Magull, J. Organometallics 2001, 20, 5777.
40. Anantharaman, G.; Roesky, H. W.; Magull, J. Angew. Chem. 2002, 114, 1274; Angew. Chem., Int. Ed. 2002, 41, 1226.
41. Anantharaman, G.; Roesky, H. W.; Magull, J. Angew. Chem. 2002, 114, 1274; Angew. Chem., Int. Ed. 2002, 41, 1226.
42. Winkhofer, N.; Voigt, A.; Dorn, H.; Roesky, H. W.; Steiner, A.; Stalke, D.; Reller, A. Angew. Chem. 1994, 106, 1414; Angew. Chem., Int. Ed. Engl. 1994, 33, 1352.
43. Winkhofer, N.; Voigt, A.; Dorn, H.; Roesky, H. W.; Steiner, A.; Stalke, D.; Reller, A. Angew. Chem. 1994, 106, 1414; Angew. Chem., Int. Ed. Engl. 1994, 33, 1352.
44. Sheldrick, G. M. Acta Crystallogr., Sect. A 1990, 46, 467.
45. Sheldrick, G. M. SHELX-97, Program for Crystal Structure Refinement; University of Göttingen: Göttingen, Germany, 1997.
46. (a) Murugavel, R.; Chandrasekhar, V.; Voigt, A.; Noltemeyer, M.; Schmidt, H.-G.; Roesky, H. W. Organometallics 1995, 14, 5298.
47. (b) Klemp, A.; Haptop, H.; Roesky, H. W.; Noltemeyer, M.; Schmidt, H.-G. Inorg. Chem. 1999, 38, 5832.
48. For compounds having Zn···Zn interactions, see the following: (a) Elias, A. J.; Schmidt, H.-G.; Noltemeyer, M.; Roesky, H. W. Organometallics 1992, 11, 462. (b) Li, H.; Eddaoudi, M.; Groy, T. L.; Yaghi, O. M. J. Am. Chem. Soc. 1998, 120, 8571.
49. For compounds having Zn···Zn interactions, see the following: (a) Elias, A. J.; Schmidt, H.-G.; Noltemeyer, M.; Roesky, H. W. Organometallics 1992, 11, 462. (b) Li, H.; Eddaoudi, M.; Groy, T. L.; Yaghi, O. M. J. Am. Chem. Soc. 1998, 120, 8571.