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Chloroform solutions of 1 and 2a (molar ratio in the range 0.5-2.0) were mixed in a vial at room temperature. The open vial was closed in a cylindrical bottle containing vaseline oil; the volatile solvent was allowed to diffuse at room temperature and after 1 day the white crystals of 3a were filtered and washed with n-pentane. The co-crystal 3b was prepared by a similar procedure starting from an acetone solution of 1 and 2b.
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Chloroform solutions of 1 and 2a (molar ratio in the range 0.5-2.0) were mixed in a vial at room temperature. The open vial was closed in a cylindrical bottle containing vaseline oil; the volatile solvent was allowed to diffuse at room temperature and after 1 day the white crystals of 3a were filtered and washed with n-pentane. The co-crystal 3b was prepared by a similar procedure starting from an acetone solution of 1 and 2b.
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26
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0012933267
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note
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-3. Detailed crystallographic data were deposited as CCDC 194241 (3a) and CCDC 194242 (3b) with the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK.
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