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Volumn 124, Issue 50, 2002, Pages 14983-14992

Total synthesis of (-)-gambierol

Author keywords

[No Author keywords available]

Indexed keywords

ETHERS; TOXIC MATERIALS;

EID: 0037132628     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja028167a     Document Type: Article
Times cited : (174)

References (81)
  • 1
    • 1542502091 scopus 로고
    • For reviews on marine polycyclic ether toxins, see (a) Yasumoto, T.; Murata, M. Chem. Rev. 1993, 93, 1897.
    • (1993) Chem. Rev. , vol.93 , pp. 1897
    • Yasumoto, T.1    Murata, M.2
  • 32
    • 2042507954 scopus 로고
    • For reviews on Suzuki-Miyaura cross-coupling reaction, see: (a) Suzuki, A.; Miyaura, N. Chem. Rev. 1995, 95, 2457.
    • (1995) Chem. Rev. , vol.95 , pp. 2457
    • Suzuki, A.1    Miyaura, N.2
  • 33
    • 0001786881 scopus 로고    scopus 로고
    • Diederich, F., Stang, P. J., Eds.; Wiley-VCH: Weinheim, Germany
    • (b) Suzuki, A. In Metal-catalyzed Cross-coupling Reactions; Diederich, F., Stang, P. J., Eds.; Wiley-VCH: Weinheim, Germany, 1998; pp 49-97.
    • (1998) Metal-catalyzed Cross-coupling Reactions , pp. 49-97
    • Suzuki, A.1
  • 44
    • 0000802361 scopus 로고    scopus 로고
    • Paquette, L. A., Ed.; John Wiley and Sons, New York
    • (b) For a comprehensive review, see Farina, V.; Krishnamurthy, V.; Scott, W. J. In Organic Reactions; Paquette, L. A., Ed.; John Wiley and Sons: New York, 1997; Vol. 50, pp 1-652.
    • (1997) Organic Reactions , vol.50 , pp. 1-652
    • Farina, V.1    Krishnamurthy, V.2    Scott, W.J.3
  • 54
    • 0346318578 scopus 로고    scopus 로고
    • note
    • The numbering of carbon atoms of all compounds in this paper corresponds to that of gambierol.
  • 60
    • 0348209168 scopus 로고    scopus 로고
    • note
    • 1H NMR spectrum of epimeric ketone 47β was different from that of ketone 47α, indicating that we can rule out the possibility of epimerization during the oxidation with TPAP/NMO.
  • 70
    • 0346318579 scopus 로고    scopus 로고
    • note
    • The corresponding iodide was too unstable to be used.
  • 71
    • 0346948546 scopus 로고    scopus 로고
    • note
    • A mixed solvent system of 1:1 DMSO/THF was used in the present study due to the low solubility of -vinyl stannane 3 in DMSO.
  • 76
    • 0348209167 scopus 로고    scopus 로고
    • note
    • TMS and TES protective groups could not survive the next reductive debenzylation with LiDBB.
  • 79
    • 0347579335 scopus 로고    scopus 로고
    • note
    • 1H NMR analysis of the purified mixture.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.