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0442265999
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note
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2 provided a mixture of olefins with a Z/E ratio of 5:1 in 85% yield.
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For an elimination reaction of α-nonactivated cyclic sulfate, see: (a) Winkler, J. D.; Kim, S.; Harrison, S.; Lewin, N. E.; Blumberg, P. M. J. Am. Chem. Soc. 1999, 121, 296. (b) Kim, C. U.; Lew, W.; Williams, M. A. Wu, H.; Zhang, L.; Chen, X.; Escarpe, P. A.; Mendel, D. B.; Laver, W. G. Stevens, R. C. J. Med. Chem. 1998, 41, 2451. (c) Schaub, C.; Müller, B.; Schmidt, R. R. Eur. J. Org. Chem. 2000, 1745.
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26
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15444353753
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For an elimination reaction of α-nonactivated cyclic sulfate, see: (a) Winkler, J. D.; Kim, S.; Harrison, S.; Lewin, N. E.; Blumberg, P. M. J. Am. Chem. Soc. 1999, 121, 296. (b) Kim, C. U.; Lew, W.; Williams, M. A. Wu, H.; Zhang, L.; Chen, X.; Escarpe, P. A.; Mendel, D. B.; Laver, W. G. Stevens, R. C. J. Med. Chem. 1998, 41, 2451. (c) Schaub, C.; Müller, B.; Schmidt, R. R. Eur. J. Org. Chem. 2000, 1745.
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27
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0041962511
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For an elimination reaction of α-nonactivated cyclic sulfate, see: (a) Winkler, J. D.; Kim, S.; Harrison, S.; Lewin, N. E.; Blumberg, P. M. J. Am. Chem. Soc. 1999, 121, 296. (b) Kim, C. U.; Lew, W.; Williams, M. A. Wu, H.; Zhang, L.; Chen, X.; Escarpe, P. A.; Mendel, D. B.; Laver, W. G. Stevens, R. C. J. Med. Chem. 1998, 41, 2451. (c) Schaub, C.; Müller, B.; Schmidt, R. R. Eur. J. Org. Chem. 2000, 1745.
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29
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0442264414
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note
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This reaction patterned after a similar step in the Magnus synthesis. 7
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