Comparison of sulfuric acid treatment and multi-layer silica gel column chromatography in cleanup methods for determination of PCDDs, PCDFs and dioxin-like PCBs in foods

Journal of the Food Hygienic Society of Japan

Volumn 43, Issue 5, 2002, Pages 312-321

  Amakura, Yoshiaki ^a   Tsutsumi, Tomoaki ^a   Sasaki, Kumiko ^a   Toyoda, Masatake ^a,b   Maitani, Tamio ^a  

^a NATIONAL INSTITUTE OF HEALTH SCIENCES   (Japan)

^b JISSEN WOMEN'S UNIVERSITY   (Japan)

Author keywords

Dioxin; Dioxin like PCB; Multi layer silica gel column chromatography; PCDD; PCDF; Sulfuric acid treatment

Indexed keywords

ACETONE; DIOXIN; FAT; FISH OIL; HEXANE; OIL; POLYCHLORINATED BIPHENYL DERIVATIVE; POLYCHLORINATED DIBENZODIOXIN; POLYCHLORINATED DIBENZOFURAN; SILICA GEL; SULFURIC ACID;

ARTICLE; CEREAL; COLUMN CHROMATOGRAPHY; DAIRY PRODUCT; EXTRACTION; FISH; FOOD ANALYSIS; FOOD COMPOSITION; FRUIT; ISOMER; MEAT; PURIFICATION; SAMPLING; VEGETABLE;

EID: 0036443738     PISSN: 00156426     EISSN: None     Source Type: Journal    
DOI: 10.3358/shokueishi.43.312     Document Type: Article

References (14)

1. Asplund, L., Jansson, B., de Wit, C., Bergek, S., Hlelt, M., Rappe, C., Odsjö, T., Olsson, M., Polychlorinated dibenzo-p-dioxins (PCDD) and dibenzofurans (PCDF) compared to other organohalogen pollutants in biological samples from Swedish ecosystems. Organohalogen Compounds, 1, 405-408 (1990).
2. Ballschmiter, K., Bacher, R. "Dioxin - Chemistry, Analysis and Toxicity -", Shimizu, T. ed., Tokyo, NTN, 1999, p. 281-369. (ISBN 900830-43-7)
3. WHO, Executive Summary for Assessment of the Health Risk of Dioxins, Reevaluation of the Tolerable Daily Intake (TDI), 1998.
4. Bock, K. W., Aryl hydrocarbon or dioxin receptor: Biologic and toxic responses. Rev. Physiol. Biochem. Pharmacol., 125, 1-42 (1994).
5. Silbergeld, E. K., Gasiewicz, T. A., Dioxins and the Ah receptor. Am. J. Ind. Med., 16, 455-474 (1989).
6. Mimura, J., Fujii-Kuriyama, Y., Transcriptional regulation by Ah (Dioxin) receptor. Tanpakushitsu Kakusan Koso (Protein, Nucleic Acid and Enzyme), 45, 1,526-1,533 (2000).
7. Toyoda, M., Iida, T., Hori, T., Yanagi, T., Kono, Y., Uchibe, H., Concentrations of PCDDs, PCDFs and Coplanar PCBs in Japanese retail foods. Shokuhin Eiseigaku Zasshi (J. Food Hyg. Soc. Japan), 40, 111-121 (1999).
8. Yoshida, K., Ikeda, S., Nakanishi, J., Assessment of human risk of dioxins in Japan. Chemosphere, 40, 177-195 (2000).
9. Shokuhinchu No Daiokishinrui Oyobi Kopurana PCB No Sokuteiho Zantei Gaidorain (Provisional guidelines for analysis of polychlorinated dibenzo-p-dioxins, dibenzofurans and coplanar PCBs in Foods) (Sep., 1999), Environmental Health Bureau, Ministry of Health and Welfare, Japan.
10. Tsutsumi, T., Yanagi, T., Nakamura, M., Kono, Y., Uchibe, H., Iida, T., Hori, T., Nakagawa, R., Tobiishi, K., Matsuda, R., Sasaki, K., Toyoda, M., Update of daily intake PCDDs, PCDFs, and dioxin-like PCBs from food in Japan. Chemosphere, 45, 1,129-1,137 (2001).
11. Takayama,K.,Miyata,H.,Aozasa,O.,Mimura,M.,Kashimoto, T., Dietary intake of dioxin-related compounds through food in Japan. Shokuhin Eiseigaku Zasshi (J. Food Hyg. Soc. Japan), 32, 525-532 (1991).
12. Hori, S., Daiokishinrui (PCDDs, PCDFs, Co-PCBs) No Bunseki No Zissai. Japan Fudo Saiensu (Japan Food Science), 38, 58-73 (1999).
13. Takasuga, T., Inoue, T., Ohi, E., Evaluation of high-resolution gas chromatography/high-resolution mass spectrometry method for the determination of dioxin and related compounds. Kankyo Kagaku (J. Environ. Chem.), 2, 599-613 (1992).
14. Van den Berg, M., Birnbaum, L., Bosveld, A. T. C., Brunstrom, B., Cook, P., Feeley, M., Giesy, J. P., Hanberg, A., Hasegawa, R., Kennedy, S. W., Kubiak, T., Larsen, J. C., van Leeuwen, F. X. R., Liem, A. K. D., Nolt, C., Peterson, R. E., Poellinger, L., Safe, S., Schrenk, D., Tillitt, D., Tysklind, M., Younes, M., Warn, F., Zacharewski, T., Toxic equivalency factors (TEFs) for PCBs, PCDDs, PCDFs for humans and wildlife. Environmental Health Perspectives, 106, 775-792 (1998).