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note
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2-derivatized silica. Disulfide terminated AQ-ODN on a support was deprotected by a usual procedure using conc. ammonium hydroxide and then purified by 20% DPAGE (Ref. 4b).
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16
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0042056416
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note
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A solution of disulfide terminated AQ-ODN and fully complementary DNA 15-mer in 10 mM sodium phosphate and 100 mM NaCl was annealed at 90°C for 5 min and then gradually cooled. The resulting solution was used for preparation of the ds AQ-ODN modified electrode.
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19
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0041555155
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note
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The electron transfer rate constant of surface confined redox molecules can be obtained from the following equation (Ref. 3b and 10).
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