Automated headspace solid-phase microextraction and in-matrix derivatization for the determination of amphetamine-related drugs in human urine by gas chromatography-mass spectrometry

Journal of Chromatographic Science

Volumn 40, Issue 1, 2002, Pages 19-25

  Namera, Akira ^a   Yashiki, Mikio ^a   Kojima, Tohru ^a   Ueki, Makoto ^a  

^a LSI MEDIENCE CORPORATION   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

3,4 METHYLENEDIOXYAMPHETAMINE; AMPHETAMINE DERIVATIVE; CARBAMIC ACID DERIVATIVE; CHLOROFORMIC ACID ETHYL ESTER; FENFLURAMINE; HOMOVERATRYLAMINE; METHAMPHETAMINE; PHENETHYLAMINE; POTASSIUM CARBONATE; SODIUM CHLORIDE;

ANALYTIC METHOD; ARTICLE; AUTOMATION; DERIVATIZATION; DRUG DETERMINATION; DRUG URINE LEVEL; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; SOLID PHASE MICROEXTRACTION; URINALYSIS;

EID: 0036039339     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/40.1.19     Document Type: Article

References (18)

1. Determination of drugs of abuse in blood
2. Determination of amphetamine, methamphetamine and amphetamine-derived designer drugs or medicaments in blood and urine
3. Solid phase microextraction with fused silica optical fibers
4. Detection of amphetamines in urine using head space-solid phase microextraction and chemical ionization selected ion monitoring
5. Rapid analysis of amphetamines in blood using head space-solid phase microextraction and selected ion monitoring
6. Simple clean-up of methamphetamine and amphetamine in human urine by direct-immersion solid phase microextraction (DI-SPME)
7. Application of a solid-phase microextraction technique for the detection of urinary methamphetamine and amphetamine by gas chromatography
8. Quantitative and qualitative analysis of MDMA, MDEA, MA and amphetamine in urine by headspace/solid phase micro-extraction (SPME) and GC/MS
9. Method optimization for the analysis of amphetamines in urine by solid-phase microextraction
10. Aqueous alkylchloro-formate derivatisation and solid-phase microextraction: Determination of amphetamines in urine by capillary gas chromatography
11. Screening procedure for 21 amphetamine-related compounds in urine using solid-phase microextraction and gas chromatography-mass spectrometry
12. Determination of amphetamine and methamphetamine in human hair by headspace solid-phase microextraction and gas chromatography with nitrogen-phosphorus detection
13. Automated determination of "Ecstasy" and amphetamines in urine by SPME and capillary gas chromatography after propylchloroformate derivatization
14. Simple and simultaneous analysis of fenfluramine, amphetamine and methamphetamine in whole blood by gas chromatography-mass spectrometry after headspace-solid phase microextraction and derivatization
15. Highly sensitive analysis of methamphetamine and amphetamine in human whole blood using headspace solid-phase microextraction and gas chromatography-mass spectrometry
16. Rapid GC-MS confirmation of urinary amphetamine and methamphetamine as their propylchloroformate derivatives