The first [4+2]-coordinated tetraorganolead compound: Synthesis, structure and conversion into a triorganolead cation, a benzoxaphosphaplumbole, and diorganolead dihalides

Zeitschrift fur Anorganische und Allgemeine Chemie

Volumn 628, Issue 11, 2002, Pages 2435-2442

  Peveling, Katja ^a   Schürmann, Markus ^a   Jurkschat, Klaus ^a  

^a TU DORTMUND UNIVERSITY   (Germany)

Author keywords

Crystal structure; Intramolecular coordination; Lead; NMR spectroscopy (207Pb); Phosphorus

Indexed keywords

BENZOXAPHOSPHAPLUMBOLE; CATION; CHEMICAL COMPOUND; CHLORIDE; HALIDE; LEAD; TRIPHENYLLEAD CHLORIDE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL PARAMETERS; CHEMICAL REACTION; CHEMICAL STRUCTURE; CRYSTAL; STRUCTURE ANALYSIS; X RAY DIFFRACTION;

EID: 0036032322     PISSN: 00442313     EISSN: None     Source Type: Journal    
DOI: 10.1002/1521-3749(200211)628:11<2435::AID-ZAAC2435>3.0.CO;2-S     Document Type: Article

References (87)

1. M. Albrecht, G. van Koten, Angew. Chem. 2001, 113, 3866; Angew. Chem. Int. Ed. Engl. 2001, 40, 3750.
2. M. Albrecht, G. van Koten, Angew. Chem. 2001, 113, 3866; Angew. Chem. Int. Ed. Engl. 2001, 40, 3750.
3. J. T. B. H. Jastrzebski, P. A. van der Schaaf, J. Boersma, G. van Koten, M. C. Zoutberg, D. Heijdenrijk, Organometallics 1989, 8, 1373.
4. G. van Koten Pure Appl. Chem. 1989, 61, 1681.
5. G. van Koten Pure Appl. Chem. 1990, 62, 1155.
6. G. van Koten, J. Terheijden, J. A. M. van Beek, I. C. M. Wehman-Ooyevaar, F. Muller, C. H. Stam, Organometallics 1990, 9, 903.
7. H. C. L. Abbenhuis, N. Feiken, D. M. Grove, J. T. B. H. Jastrzebski, H. Kooijman, P. van der Sluis, W. J. J. Smeets, A. L. Spek, G. van Koten, J. Am. Chem. Soc. 1992, 114, 9773.
8. C. Chuit, R. J. P. Corriu, A. Mehdi, C. Reyé, Angew. Chem. 1993, 105, 1372; Angew. Chem. Int. Ed. Engl. 1993, 32, 1311.
9. C. Chuit, R. J. P. Corriu, A. Mehdi, C. Reyé, Angew. Chem. 1993, 105, 1372; Angew. Chem. Int. Ed. Engl. 1993, 32, 1311.
10. F. Carré, C. Chuit, R. J. P. Corriu, A. Mehdi, C. Reyé, Angew. Chem. 1994, 106, 1152; Angew. Chem. Int. Ed. Engl. 1994, 33, 1097.
11. F. Carré, C. Chuit, R. J. P. Corriu, A. Mehdi, C. Reyé, Angew. Chem. 1994, 106, 1152; Angew. Chem. Int. Ed. Engl. 1994, 33, 1097.
12. F. Carré, C. Chuit, R. J. P. Corriu, A. Mehdi, C. Reyé, Organometallics 1995, 14, 2754.
13. F. Carré, C. Chuit, R. J. P. Corriu, A. Fanta, A. Mehdi, C. Reyé, Organometallics 1995, 14, 194.
14. M. Chauhan, C. Chuit, R. J. P. Corriu, A. Mehdi, C. Reyé, Organometallics 1996, 15, 4326.
15. M. Chauhan, C. Chuit, R. J. P. Corriu, C. Reyé, Tetrahedron Letters 1996, 37, 845.
16. J.-P. Sutter, S. L. James, P. Steenwinkel, T. Karlen, D. M. Grove, N. Veldman, W. J. J. Smeets, A. L. Spek, G. van Koten, Organometallics 1996, 15, 941.
17. R. Schlengermann, J. Sieler, S. Jelonek, E. Hey-Hawkins, Chem. Commun. 1997, 197.
18. F. Carré, M. Chauhan, C. Chuit, R. J. P. Corriu, C. Reyé, J. Organomet. Chem. 1997, 540, 175.
19. J. A. M. Brandts, R. A. Gossage, J. Boersma, A. L. Spek, G. van Koten, Organometallics 1999, 18, 2642.
20. M. R. Meneghetti, M. Grellier, M. Pfeffer, A. De Cian, J. Fischer, Eur. J. Inorg. Chem. 2000, 1539.
21. M. Albrecht, S. L. James, N. Veldman, A. L. Spek, G. van Koten, Can. J. Chem. 2001, 79, 709.
22. M. Albrecht, B. M. Kocks, A. L. Spek, G. van Koten, J. Organomet. Chem. 2001, 624, 271.
23. G. Rodríguez, M. Lutz, A. L. Spek, G. van Koten, Chem. Eur. J. 2002, 8, 46.
24. C. J. Moulton, B. L. Shaw, J. Chem. Soc., Dalton Trans. 1976, 1020.
25. F. Gorla, L. M. Venanzi, A. Albinati, Organometallics 1994, 13, 43.
26. A. Pape, M. Lutz, G. Müller, Angew. Chem. 1994, 106, 2375; Angew. Chem. Int. Ed. Engl. 1994, 33, 2281.
27. A. Pape, M. Lutz, G. Müller, Angew. Chem. 1994, 106, 2375; Angew. Chem. Int. Ed. Engl. 1994, 33, 2281.
28. T. Karlen, P. Dani, D. M. Grove, P. Steenwinkel, G. van Koten, Organometallics 1996, 15, 5687.
29. M. Gupta, C. Hagen, R. J. Flesher, W. C. Kaska, C. M. Jensen, Chem. Commun. 1996, 2083.
30. G. Müller, M. Waldkircher, A. Pape, "Phosphine Coordination to Silicon Revisited" in Organosilicon Chemistry III; Auner, N., Weis, J. (eds), Wiley-VCH, 1998, p. 452.
31. J. C. Grimm, C. Nachtigal, H.-G. Mack, W. C. Kaska, H. A. Mayer, Inorg. Chem. Commun. 2000, 3, 511.
32. P. Dani, M. A. M. Toorneman, G. P. M. van Klink, G. van Koten, Organometallics 2000, 19, 5287.
33. R. P. Hughes, A. Williamson, C. D. Incarvito, A. L. Rheingold, Organometallics 2001, 20, 4741.
34. D. G. Gusev, F. M. Dolgushin, M. Y. Antipin, Organometallics 2001, 20, 1001.
35. E. J. Farrington, E. M. Viviente, B. S. Williams, G. van Koten, J. M. Brown, Chem. Commun. 2002, 308.
36. J. Errington, W. S. McDonald, B. L. Shaw, J. Chem. Soc., Dalton Trans. 1980, 2312.
37. J. Dupont, N. Beydoun, M. Pfeffer, J. Chem. Soc., Dalton Trans. 1989, 1715.
38. W. T. S. Huck, L. J. Prins, R. H. Fokkens, N. M. M. Nibbering, F. C. J. M. van Veggel, D. N. Reinhoudt, J. Am. Chem. Soc. 1998, 120, 6240.
39. M. Mehring, M. Schürmann, K. Jurkschat, Organometallics 1998, 17, 1227.
40. J. Vicente, A. Arcas, M.-A. Blasco, J. Lozano, M. C. R. de Arellano, Organometallics 1998, 17, 5374.
41. M. Mehring, K. Jurkschat, M. Schürmann, Main Group Met. Chem. 1998, 21, 635.
42. M. Mehring, C. Löw, M. Schürmann, K. Jurkschat, Eur. J. Inorg. Chem. 1999, 887.
43. J. Vicente, M.-T. Chicote, M.-D. Abrisqueta, P. G. Jones, Organometallics 2000, 19, 2629.
44. M. Mehring, C. Löw, M. Schürmann, F. Uhlig, K. Jurkschat, Organometallics 2000, 19, 4613.
45. M. Mehring, I. Vrasidas, D. Horn, M. Schürmann, K. Jurkschat, Organometallics 2001, 20, 4647.
46. K. Peveling, M. Schürmann, K. Jurkschat, Main Group Met. Chem. 2001, 24, 251.
47. K. Peveling, M. Schürmann, R. Ludwig, K. Jurkschat, Organometallics 2001, 20, 4654.
48. M. Henn, Jurkschat, K.; Löw, C.; Mehring, M.; Peveling, K.; Schürmann, M. unpublished results.
49. C. Löwig, J. Pract Chem. 1853, 60, 304.
50. C. Löwig, Liebigs Ann. Chem. 1853, 88, 318.
51. G. Calingaert, Chem. Rev. 1925, 2, 43.
52. J. Sarapuk, K. Bielecki, H. Kleszczynska, A. Dziamska, S. Przestalski, Appl. Organomet. Chem. 2001, 15, 56.
53. D. M. X. Donnelly, J.-P. Finet, B. A. Rattigan, J. Chem. Soc., Perkin Trans. 1 1995, 1679.
54. J. T. Pinley, Pure Appl. Chem. 1996, 68, 819.
55. M. G. Moloney, R. M. Thompson, E. Wright, Main Group Met. Chem. 1996, 19, 133.
56. S.-K. Kang, U. Shivkumar, C. Ahn, S.-C. Choi, J.-S. Kim, Synth. Commun. 1997, 27, 1893.
57. S.-K. Kang, H.-C. Ryu, S.-C. Choi, Chem. Commun. 1998, 1317.
58. S.-K. Kang, H.-C. Ryu, H.-J. Son, Synlett 1998, 771.
59. M. G. Moloney, D. R. Paul, R. M. Thompson, E. Wright, J. Organomet. Chem. 1998, 560, 77.
60. J. E. H. Buston, H. J. Howell, M. G. Moloney, V. C. Manson, R. M. Thompson, Main Group Met. Chem. 1998, 21, 51.
61. J. E. H. Buston, R. G. Compton, M. A. Leech, M. G. Moloney, J. Organomet. Chem. 1999, 585, 326.
62. G. I. Elliott, J. P. Konopelski, Tetrahedron 2001, 57, 5683.
63. th International Conference on the Coordination and Organometallic Chemistry of Germanium, Tin and Lead, ICCOC-GTL-10, July 8 to 12, 2001, Bordeaux, France, Book of Abstracts IL5.
64. A.-F. Shihada, F. Weller, Z. Anorg. Allg. Chem. 2001, 627, 638.
65. A. Silvestru, C. Silvestru, I. Haiduc, J. E. Drake, J. Yang, F. Caruso, Polyhedron 1997, 16, 949.
66. R. A. Varga, C. Silvestru, I. Haiduc, Synth. React. Inorg. Met.-Org. Chem. 2000, 30, 485.
67. S. N. Ólafsson, C. Flensburg, P. Andersen, J. Chem. Soc., Dalton Trans. 2000, 4360.
68. H. Gilman, D. S. Melstrom, J. Am. Chem. Soc. 1950, 2953.
69. H. O. van der Kooi, J. Wolters, A. van der Gen, Recueil, J. R. Neth. Chem. Soc. 1979, 98, 353.
70. J. Huheey, E. A. Keiter, R. L. Keiter, Anorganische Chemie: Prinzipien von Struktur und Reaktivität, 2nd ed., de Gruyter, New York-Berlin, 1995.
71. L. Pauling, The Nature of the Chemical Bond, 3rd ed., Cornell University Press: Ithaca, New York, 1960.
72. J. D. Dunitz, X-Ray Analysis and the Structure of Organic Molecules, Cornell University Press: Ithaca, New York, 1979.
73. H. Preut, F. Huber, Acta Cryst. 1993, C49, 1372.
74. M. Henn, K. Jurkschat, R. Ludwig, M. Mehring, K. Peveling, M. Schürmann, Organometallics 2002, submitted.
75. E. Capek, K. E. Schwarzhans, Monatsh. Chem. 1987, 118, 419.
76. D. S. Melstrom, Iowa State Coll. J. Sci. 1943, 18, 65.
77. U. Kolb, M. Beuter, M. Gerner, M. Dräger, Organometallics 1994, 13, 4413.
78. U. Kolb, M. Beuter, M. Dräger, Inorg. Chem. 1994, 33, 4522.
79. U. Kolb, M. Dräger, Jousseaume, B. Organometallics 1991, 10, 2737.
80. C. Glidewell, D. C. Liles, Acta Crystallogr. 1978, B34, 129.
81. H. Preut, F. Huber, Z. Anorg. Allg. Chem. 1977, 435, 234.
82. H. J. Eppley, J. L. Ealy, C. H. Yoder, J. N. Spencer, A. L. Rheingold, J. Organomet. Chem. 1992, 431, 133.
83. D. Dakternieks, T. S. Basu Baul, S. Dutta, E. R. T. Tiekink, Organometallics 1998, 17, 3058.
84. G. M. Sheldrick, Acta Cryst. 1990, A46, 467.
85. G. M. Sheldrick, University of Göttingen, 1997.
86. International Tables for Crystallography, Kluwer Academic: Dortrecht 1992, Vol C.
87. G. M. Sheldrick, SHELXTL, Release 5.1 Software Reference Manual, Bruker AXS, Inc.: Madison, Wisconsin, USA, 1997.