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The pyridine ligand is deprotonated in aqueous environments and probably forms a (hyperbranched) polymer by coordinating to the activated Pd centers. The addition of pyridine causes the polymers to break down. See for similar hyperbranched polymers: Huck, W. T. S.; van Veggel, F. C. J. M.; Kropman, B. L.; Blank, D. H. A.; Keim, E. G.; Smithers, M. M. A.; Reinhoudt, D. N. J Am. Chem. Soc. 1995, 117, 8293-8294. Huck, W. T. S.; Snellink-Ruël, B. A.; van Veggel, F. C. J. M.; Lichtenbelt, J. W. Th.; Reinhoudt, D. N. Chem. Commun. 1997, 9-10.
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0010472493
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The pyridine ligand is deprotonated in aqueous environments and probably forms a (hyperbranched) polymer by coordinating to the activated Pd centers. The addition of pyridine causes the polymers to break down. See for similar hyperbranched polymers: Huck, W. T. S.; van Veggel, F. C. J. M.; Kropman, B. L.; Blank, D. H. A.; Keim, E. G.; Smithers, M. M. A.; Reinhoudt, D. N. J Am. Chem. Soc. 1995, 117, 8293-8294. Huck, W. T. S.; Snellink-Ruël, B. A.; van Veggel, F. C. J. M.; Lichtenbelt, J. W. Th.; Reinhoudt, D. N. Chem. Commun. 1997, 9-10.
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2642714467
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note
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+. However, also weak signals at higher mlz ratios are observed. This might be an effect of the matrix and/or applied technique, which is currently under investigation.
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44
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2642701230
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note
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Due to a too low resolution the isotope pattern was not observed. However, the calculated isotope pattern with the experimental resolution was in good agreement with the measured signals.
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