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3), 10.7 (s, 1H; Ru=CH). Other data are given in the Supporting Information.
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32
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0011414396
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note
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int = 0.000), 4542 observed (>2σ), final residuals R1 = 0.0601, wR2 = 0.1581 (I > 2σ(I)); R1 = 0.0869, wR2 = 0.1782 (all data).
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0011465651
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note
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-1 (CO). Other data are given in the Supporting Information.
-
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41
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0011504626
-
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note
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int = 0.000), 2155 observed (>2σ), final residuals R1 = 0.0498, wR2 = 0.1263 (I > 2σ(I)); R1 = 0.1777, wR2 = 0.1730 (all data).
-
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-
42
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0011465652
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note
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1H NMR measurement at -80 °C. Only 3a was observed as the organometallic product.
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45
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0000353313
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