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0043226771
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1H NMR and MS.
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22
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0041724251
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note
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1H NMR (300 MHz). When sodium tert-butoxide and ligand were mixed under similar conditions, a black precipitate resulted. Further studies to establish the structure of the active catalyst in this case will be reported elsewhere.
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0043226770
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2 (0.9 mg, 0.004 mmol), and N,N-bis(2,6-diisopropyl)dihydroimidazolium chloride (1.2 mg, 0.004 mmol) diluted in THF (5 mL). Stirring continued and the reaction was worked up at the indicated time. The product was isolated and characterized as before.
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