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16
-
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0342570550
-
-
note
-
3, Z = 4, 4588 observed reflections (I > 2.0σ(I)), R = 0.0508, Rw = 0.129. The structure was solved by direct methods using Siemens SHELXTL PLUS (PC version).
-
-
-
-
17
-
-
0343876158
-
-
note
-
This average, or range, was obtained from a search of the Cambridge crystallographic database.
-
-
-
-
18
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0000883590
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0001454688
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21
-
-
37049096497
-
-
τ is defined as (α - β)/60°, where α = largest angle, β = second largest angle (τ = 1.0 for ideal trigonal bipyramidal; τ = 0.0 for ideal square pyramidal). Addison, A. W.; Rao, T. N.; Reedijk, J.; Van Rijn, J.; Verschoor, G. C. J. Chem. Soc., Dalton Trans. 1984, 1349-1356.
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-
22
-
-
0342570532
-
-
note
-
3, Z = 8; 13 388 observed reflections, R = 0.0658, Rw = 0.1298, GOF = 1.04. The structure was solved by direct methods (SIR92) and refined with SHELX97.
-
-
-
-
24
-
-
0024394199
-
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Kumar, M.; Colpas, G. J.; Day, R. O.; Maroney, M. J. J. Am. Chem. Soc. 1989, 111, 8323-8325.
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-
25
-
-
0343004871
-
-
note
-
3, Z = 4; 6622 observed reflections, R = 0.0564, Rw = 0.1308, GOF = 0.950. The structure was solved by direct methods (SIR92) and refined with SHELX97.
-
-
-
-
26
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0000491610
-
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Cornman, C. R.; Stautler, T. C.; Boyle, P. D. J. Am. Chem. Soc. 1997, 119, 5986-5987.
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