Enantioselective synthesis of the metabolites of vasopressin V2 receptor antagonist OPC-31260 via lipase-catalyzed transesterification

Tetrahedron

Volumn 56, Issue 27, 2000, Pages 4667-4682

  Matsubara, Jun ^a   Kitano, Kazuyoshi ^a   Otsubo, Kenji ^a   Kawano, Yoshikazu ^a   Ohtani, Tadaaki ^a   Bando, Masahiko ^a   Kido, Masaru ^a   Uchida, Minoru ^a   Tabusa, Fujio ^a  

^a OTSUKA PHARMACEUTICAL CO LTD   (Japan)

Author keywords

Benzazepine; Enantioselective; Kinetic resolution; Vasopressin

Indexed keywords

ALCOHOL; DIMETHYLAMINE; DRUG METABOLITE; MOZAVAPTAN; TRIACYLGLYCEROL LIPASE; VASOPRESSIN V2 RECEPTOR; VINYL ACETATE;

ARTICLE; ESTERIFICATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRIORITY JOURNAL; SYNTHESIS;

STAPHYLOCOCCUS PHAGE 3A;

EID: 0034733625     PISSN: 00404020     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4020(00)00388-4     Document Type: Article

References (11)

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4. (a) Matsubara, J.; Morita, S.; Yamashita, H.; Otsubo, K.; Kitano, K.; Ohtani, T.; Kawano, Y.; Bando, M.; Kido, M.; Uchida, M.; Tabusa, F. Heterocycles 2000, 54, in press.
5. (b) Kitano, K.; Matsubara, J.; Ohtani, T.; Otsubo, K.; Kawano, Y.; Morita, S.; Uchida, M. Tetrahedron Lett. 1999, 40, 5235.
6. (c) Morita, S.; Matsubara, J.; Otsubo, K.; Kitano, K.; Ohtani, T.; Kawano, Y.; Uchida, M. Tetrahedron: Asymmetry 1997, 8, 3707.
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10. TEXSAN, TEXRAY Structure Analysis Package; Molecular Structure Corporation (1995). Single Crystal Structure Analysis Software. Version 1.7. MSC, 3200A Research Forest Drive, The Woodlands, TX 77381, USA.
11. The author has deposited atomic coordinates for this structure with the Cambridge Crystallographic Data Center. The coordinates can be obtained on request from The Director, Cambridge Crystallographic Data Center, University Chemical Laboratory, Lensfield Road, Cambridge CB12 1EW, UK.