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27
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0342303456
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note
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3) of 4-6, 8-10, and 10Zn, see the Supporting Information.
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28
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0000312932
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E. Alessio, M. Macchi, S. L. Heath, L. G. Marzilli, Inorg. Chem. 1997, 36, 5614-5623.
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0342738578
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note
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3).
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30
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0342738579
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note
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1H} NMR spectrum.
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31
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0342738576
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note
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[14] Therefore this effect seems to be attributable to the dppp ligand rather than to the metal. Examination of the solid-state structure of 10 suggests that these protons might fall into the shielding cone of the phenyl rings of dppp, whose conformation is not frozen in solution.
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0042416021
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Nottingham, UK
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E. Iengo, E. Ciani, E. Zangrando, S. Geremia, E. Alessio, Abstr. Pap. 7th Int. Conf. "The Chemistry of the Platinum Groups Metals" (Nottingham, UK) 1999, p. 101.
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Abstr. Pap. 7th Int. Conf. "The Chemistry of the Platinum Groups Metals"
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Iengo, E.1
Ciani, E.2
Zangrando, E.3
Geremia, S.4
Alessio, E.5
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33
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0342303454
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note
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[10]
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34
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0342303455
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note
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3 molecules (occupancy factor 0.5 each) and a molecule of n-hexane were detected on the AF map. Final R1 - 0.1171, wR2 0.2847, S (GOF) 1.252 for 5149 observed reflections [I > 2σ(I)] and 764 parameters. Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-132681. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: ( -44)1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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36
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0001474836
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Note added in proof (February 2, 2000): During publication of this work a paper containing the X-ray structure of 11 appeared: M. Schmitz, S. Leininger, T. Fan, A. M. Arif, P. J. Stang, Organometallics 1999, 18, 4817-4824.
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(1999)
Organometallics
, vol.18
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Schmitz, M.1
Leininger, S.2
Fan, T.3
Arif, A.M.4
Stang, P.J.5
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