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We have recently found that in the case of the resolution of 2-arylalkanoic acids b enantiopure amino alcohols, the efficiency of resolution was considerably improved by using a rigid resolving agent, see: ref. 7.
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0010857061
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note
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We selected these resolving agents because both their enantiopure forms are available.
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44
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note
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For an example of the application of the Schröder-van Laar equation to the diastereomeric mixtures, see: ref. 1.
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47
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0010778941
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note
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A table of N...O and O...O distances in the diastereomeric salts is deposited as supporting information (Table S1).
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48
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0001263021
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0010847014
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note
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A table of the angles and lengths between the stacking aromatic rings is deposited as supporting information (Table S2).
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51
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33947470124
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0010778779
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note
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-1): less-soluble (R)-2·(R)-3f (3290, 1610, 1230), more-soluble (R)-2·(S)-3F (3310, 1625, 1245); less-soluble (S)-2·(S)-3g (3270, 1610, 1225), more-soluble (S)-2·(R)-3g (3330, 1630, 1245); less-soluble (S)-2·(S)-3k (3250, 1575, 1380), more-soluble (S)-2·(S)-3k (3350, 1635, 1420). In all cases, the absorption bands of the more-soluble salts were shifted upward from those of the corresponding less-soluble salts.
-
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55
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0010917956
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note
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0010857062
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note
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CRYSTAN GM, a computer program for the solution and refinement of crystal structures for X-ray diffraction data (Mac Science Corporation).
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