Recent advances in microwave-assisted organic syntheses

Current Opinion in Drug Discovery and Development

Volumn 3, Issue 4, 2000, Pages 454-461

  Krstenansky, John L ^a   Cotterill, Lan ^a  

^a EnzyMed Division   (United States)

Author keywords

Microwave heating; Microwave assisted organic synthesis; Non thermal effects; Solvent free reactions; Supported reagents

Indexed keywords

ARTICLE; CHEMICAL REACTION; MICROWAVE RADIATION; SYNTHESIS;

EID: 0033940859     PISSN: 13676733     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (19)

1. Fini A, Breccia A: Chemistry by microwaves. Pure Appl Chem (1999) 71(4):573-579. Good concise review of microwave theory and application to chemistry.
2. Gedye RN, Wei JB: Rate enhancement of organic reactions by microwaves at atmospheric pressure. Can J Chem (1998)76:525-532.
3. Loupy A, Petit A, Hamelin J, Texier-Boullet F, Jacquault P, Mathe D: New solvent-free organic synthesis using focused microwaves. Synthesis (1998):1213-1234. Excellent comprehensive review of solvent-free microwave chemistry until 1998.
4. Deshayes S, Liagre M, Loupy A, Luche J-L, Petit A: Microwave activation in phase transfer catalysis. Tetrahedron (1999) 55:10851-10870.
5. Bose DS, Jayalakshmi B: Reagents for organic synthesis: Use of organostannyl oxides as catalytic neutral agents in the preparation of nitriles from primary amides under microwave irradiation. J Org Chem (1999) 64:1713-1714.
6. Bremberg U, Larhed M, Moberg C, Hallberg A: Rapid microwave-induced palladium-catalyzed asymmetric allylic alkylation. J Org Chem (1999) 64:1082-1083.
7. Blettner CG, König WA, Stenzel W, Schotten T: Microwaveassisted aqueous Suzuki cross-coupling reactions. J Org Chem (1999) 64:3885-3890.
8. Kad GL, Kaur KP, Singh V, Singh J: Microwave induced rate enhancement in aldol condensation. Synth Commun (1999) 29:2583-2586.
9. Brain CT, Paul JM, Loong Y, Oakley PJ: Novel procedure for the synthesis of 1,3,4-oxadiazoles from 1,2diacylhydrazines using polymer-supported Burgess reagent under microwave conditions. Tetrahedron Lett (1999)40:3275-3278.
10. Hu Y, Yu J, Yang S, Wang J-X, Yin Y: Substitution reaction of nitro group on a-nitrostyrene by organozinc halides under microwave irradiation. Synth Commun (1999) 29:1157-1164.
11. Beeson T, Guillard J, Rees CW: Multistep synthesis of thiazoloquinazolines under microwave irradiation in solution. Tetrahedron Lett (2000) 41:1027-1030.
12. Chakraborty V, Bordoloi M: Microwave-assisted oxidation of alcohols by pyridinium chlorochromate. J Chem Res (1999):118-119.
13. Diaz-Ortiz A, Carrillo JR, Gomez-Escalonilla MJ, de la Hoz A, Moreno A, Prieto P: First Diels-Alder reaction of pyrazolyl imines under microwave irradiation. Synlett (1998):1069-1070.
14. de la Hoz A, Moreno A, Vazquez E: Use of microwave irradiation and solid acid catalysis in an enhanced and environmentally friendly synthesis of coumarin derivatives. Synlett (1999):608-610.
15. Marquez H, Pérez ER, Pluti'n AM, Morales M, Loupy A: Synthesis of 1-benzoyl-3-alkylthioureas by transamidation under microwave in dry media. Tetrahedron Lett (2000) 41:1753-1756.
16. Herr RJ, Meckler H, Scuderi F Jr: Observed acidities of charcoals, clays and common laboratory purification reagents in aqueous and organic solutions. Org Process ResDev (2000) 4:43-45.
17. R as novel heterogeneous catalysts for rapid synthesis of nitriles from aldoximes in absence of solvent. Synth Commun (1999) 29(19):3409-3413.
18. Ranu BC, Hajra A, Jana U: Microwave-assisted simple synthesis of quinolines from anilines and a Iky I vinyl ketones on the surface of silica gel in the presence of indium(lll) chloride. Tetrahedron Lett (2000) 41:531-533.
19. Williams L: Thin layer chromatography as a tool for reaction optimization in microwave assisted synthesis. Chem Commun (2000):435-436.