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Volumn 121, Issue 16, 1999, Pages 4070-4071

Evidence for the existence of a late-metal terminal sulfido complex

Author keywords

[No Author keywords available]

Indexed keywords

NICKEL COMPLEX; NICKEL SUBSULFIDE; ORGANOSULFUR DERIVATIVE; SULFIDE;

EID: 0033612017     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja984136x     Document Type: Article
Times cited : (54)

References (48)
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    • See, for example: (a) Sánchez, G.; Momblona, F.; Sánchez, M.; Pérez, J.; López, G.; Casabó, J.; Molins, E.; Miravitlles, C. Eur. J. Inorg. Chem. 1998, 1199. (b) Sánchez, G.; Momblona, F.; Garcia, G.; López, G.; Pinilla, E.; Monge, A. J. Chem. Soc., Dalton Trans. 1994, 2271. Wei, C. H.; Dahl, L. F. Inorg. Chem. 1970, 9, 1878. Gibson, D.; Lippard, S. J. Inorg. Chem. 1986, 25, 219. (e) Henkel, G.; Kriege, M.; Matsumoto, K. J. Chem. Soc., Dalton Trans. 1988, 657. See, for example: (a) Song, L.-C.; Dong, Y.-B.; Hu, Q.-M.; Li, Y.-K.; Sun, J. Polyhedron 1998, 17, 1579. (b) Teo, B. K.; Bakirtzis, V.; Snyder-Robinson, P. A. J. Am. Chem. Soc. 1983, 105, 6330. North, T. E.; Thoden, J. B.; Spencer, B.; Dahl, L. F. Organometallics 1993, 12, 1299. Braunstein, P.; Sappa, E.; Tiripicchio, A.; Tiripicchio Camellini, M. Inorg. Chim. Acta 1980,45, L191. (e) Cecconi, F.; Ghilardi, C. A.; Midollini, S.; Orlandini, A.; Vacca, A.; Ramirez, J. A. J. Chem. Soc., Dalton Trans. 1990, 773.
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    • See, for example: (a) Sánchez, G.; Momblona, F.; Sánchez, M.; Pérez, J.; López, G.; Casabó, J.; Molins, E.; Miravitlles, C. Eur. J. Inorg. Chem. 1998, 1199. (b) Sánchez, G.; Momblona, F.; Garcia, G.; López, G.; Pinilla, E.; Monge, A. J. Chem. Soc., Dalton Trans. 1994, 2271. Wei, C. H.; Dahl, L. F. Inorg. Chem. 1970, 9, 1878. Gibson, D.; Lippard, S. J. Inorg. Chem. 1986, 25, 219. (e) Henkel, G.; Kriege, M.; Matsumoto, K. J. Chem. Soc., Dalton Trans. 1988, 657. See, for example: (a) Song, L.-C.; Dong, Y.-B.; Hu, Q.-M.; Li, Y.-K.; Sun, J. Polyhedron 1998, 17, 1579. (b) Teo, B. K.; Bakirtzis, V.; Snyder-Robinson, P. A. J. Am. Chem. Soc. 1983, 105, 6330. (c) North, T. E.; Thoden, J. B.; Spencer, B.; Dahl, L. F. Organometallics 1993, 12, 1299. Braunstein, P.; Sappa, E.; Tiripicchio, A.; Tiripicchio Camellini, M. Inorg. Chim. Acta 1980,45, L191. (e) Cecconi, F.; Ghilardi, C. A.; Midollini, S.; Orlandini, A.; Vacca, A.; Ramirez, J. A. J. Chem. Soc., Dalton Trans. 1990, 773.
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    • See, for example: (a) Sánchez, G.; Momblona, F.; Sánchez, M.; Pérez, J.; López, G.; Casabó, J.; Molins, E.; Miravitlles, C. Eur. J. Inorg. Chem. 1998, 1199. (b) Sánchez, G.; Momblona, F.; Garcia, G.; López, G.; Pinilla, E.; Monge, A. J. Chem. Soc., Dalton Trans. 1994, 2271. Wei, C. H.; Dahl, L. F. Inorg. Chem. 1970, 9, 1878. Gibson, D.; Lippard, S. J. Inorg. Chem. 1986, 25, 219. (e) Henkel, G.; Kriege, M.; Matsumoto, K. J. Chem. Soc., Dalton Trans. 1988, 657. See, for example: (a) Song, L.-C.; Dong, Y.-B.; Hu, Q.-M.; Li, Y.-K.; Sun, J. Polyhedron 1998, 17, 1579. (b) Teo, B. K.; Bakirtzis, V.; Snyder-Robinson, P. A. J. Am. Chem. Soc. 1983, 105, 6330. North, T. E.; Thoden, J. B.; Spencer, B.; Dahl, L. F. Organometallics 1993, 12, 1299. (d) Braunstein, P.; Sappa, E.; Tiripicchio, A.; Tiripicchio Camellini, M. Inorg. Chim. Acta 1980,45, L191. (e) Cecconi, F.; Ghilardi, C. A.; Midollini, S.; Orlandini, A.; Vacca, A.; Ramirez, J. A. J. Chem. Soc., Dalton Trans. 1990, 773.
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    • See, for example: (a) Sánchez, G.; Momblona, F.; Sánchez, M.; Pérez, J.; López, G.; Casabó, J.; Molins, E.; Miravitlles, C. Eur. J. Inorg. Chem. 1998, 1199. (b) Sánchez, G.; Momblona, F.; Garcia, G.; López, G.; Pinilla, E.; Monge, A. J. Chem. Soc., Dalton Trans. 1994, 2271. Wei, C. H.; Dahl, L. F. Inorg. Chem. 1970, 9, 1878. Gibson, D.; Lippard, S. J. Inorg. Chem. 1986, 25, 219. (e) Henkel, G.; Kriege, M.; Matsumoto, K. J. Chem. Soc., Dalton Trans. 1988, 657. See, for example: (a) Song, L.-C.; Dong, Y.-B.; Hu, Q.-M.; Li, Y.-K.; Sun, J. Polyhedron 1998, 17, 1579. (b) Teo, B. K.; Bakirtzis, V.; Snyder-Robinson, P. A. J. Am. Chem. Soc. 1983, 105, 6330. North, T. E.; Thoden, J. B.; Spencer, B.; Dahl, L. F. Organometallics 1993, 12, 1299. Braunstein, P.; Sappa, E.; Tiripicchio, A.; Tiripicchio Camellini, M. Inorg. Chim. Acta 1980,45, L191. (e) Cecconi, F.; Ghilardi, C. A.; Midollini, S.; Orlandini, A.; Vacca, A.; Ramirez, J. A. J. Chem. Soc., Dalton Trans. 1990, 773.
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    • Evidence has been provided for the existence of a terminal sulfido complex of nickel in the gas phase. See: Gregor, I. K.; Gregor, R. C. Inorg. Chim. Acta 1992, 194, 37.
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    • For an in depth review see: Parkin, G. Prog. Inorg. Chem. 1998, 47, 1. For recent examples, see: (a) Sweeney, Z. K.; Polse, J. L.; Andersen, R. A.; Bergman, R. G. J. Am. Chem. Soc. 1998, 120, 7825. (b) Kuchta, M. C.; Parkin, G. J. Chem. Soc., Dalton Trans. 1998, 2279. Kuchta, M. C.; Hascall, T.; Parkin, G. Chem. Commun. 1998, 751. Hagadom, J. R.; Arnold, J. Organometallics 1998, 17, 1355. (e) Firth, A. V.; Witt, E.; Stephan, D. W. Organometallics 1998, 17, 3716. (f) Hagadorn, J. R.; Arnold, J. Inorg. Chem. 1997, 36, 2928.
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    • For an in depth review see: Parkin, G. Prog. Inorg. Chem. 1998, 47, 1. For recent examples, see: (a) Sweeney, Z. K.; Polse, J. L.; Andersen, R. A.; Bergman, R. G. J. Am. Chem. Soc. 1998, 120, 7825. (b) Kuchta, M. C.; Parkin, G. J. Chem. Soc., Dalton Trans. 1998, 2279. Kuchta, M. C.; Hascall, T.; Parkin, G. Chem. Commun. 1998, 751. Hagadom, J. R.; Arnold, J. Organometallics 1998, 17, 1355. (e) Firth, A. V.; Witt, E.; Stephan, D. W. Organometallics 1998, 17, 3716. (f) Hagadorn, J. R.; Arnold, J. Inorg. Chem. 1997, 36, 2928.
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    • For an in depth review see: Parkin, G. Prog. Inorg. Chem. 1998, 47, 1. For recent examples, see: (a) Sweeney, Z. K.; Polse, J. L.; Andersen, R. A.; Bergman, R. G. J. Am. Chem. Soc. 1998, 120, 7825. (b) Kuchta, M. C.; Parkin, G. J. Chem. Soc., Dalton Trans. 1998, 2279. Kuchta, M. C.; Hascall, T.; Parkin, G. Chem. Commun. 1998, 751. Hagadom, J. R.; Arnold, J. Organometallics 1998, 17, 1355. (e) Firth, A. V.; Witt, E.; Stephan, D. W. Organometallics 1998, 17, 3716. (f) Hagadorn, J. R.; Arnold, J. Inorg. Chem. 1997, 36, 2928.
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    • For an in depth review see: Parkin, G. Prog. Inorg. Chem. 1998, 47, 1. For recent examples, see: (a) Sweeney, Z. K.; Polse, J. L.; Andersen, R. A.; Bergman, R. G. J. Am. Chem. Soc. 1998, 120, 7825. (b) Kuchta, M. C.; Parkin, G. J. Chem. Soc., Dalton Trans. 1998, 2279. (c) Kuchta, M. C.; Hascall, T.; Parkin, G. Chem. Commun. 1998, 751. Hagadom, J. R.; Arnold, J. Organometallics 1998, 17, 1355. (e) Firth, A. V.; Witt, E.; Stephan, D. W. Organometallics 1998, 17, 3716. (f) Hagadorn, J. R.; Arnold, J. Inorg. Chem. 1997, 36, 2928.
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    • For an in depth review see: Parkin, G. Prog. Inorg. Chem. 1998, 47, 1. For recent examples, see: (a) Sweeney, Z. K.; Polse, J. L.; Andersen, R. A.; Bergman, R. G. J. Am. Chem. Soc. 1998, 120, 7825. (b) Kuchta, M. C.; Parkin, G. J. Chem. Soc., Dalton Trans. 1998, 2279. Kuchta, M. C.; Hascall, T.; Parkin, G. Chem. Commun. 1998, 751. (d) Hagadom, J. R.; Arnold, J. Organometallics 1998, 17, 1355. (e) Firth, A. V.; Witt, E.; Stephan, D. W. Organometallics 1998, 17, 3716. (f) Hagadorn, J. R.; Arnold, J. Inorg. Chem. 1997, 36, 2928.
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    • For an in depth review see: Parkin, G. Prog. Inorg. Chem. 1998, 47, 1. For recent examples, see: (a) Sweeney, Z. K.; Polse, J. L.; Andersen, R. A.; Bergman, R. G. J. Am. Chem. Soc. 1998, 120, 7825. (b) Kuchta, M. C.; Parkin, G. J. Chem. Soc., Dalton Trans. 1998, 2279. Kuchta, M. C.; Hascall, T.; Parkin, G. Chem. Commun. 1998, 751. Hagadom, J. R.; Arnold, J. Organometallics 1998, 17, 1355. (e) Firth, A. V.; Witt, E.; Stephan, D. W. Organometallics 1998, 17, 3716. (f) Hagadorn, J. R.; Arnold, J. Inorg. Chem. 1997, 36, 2928.
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    • For an in depth review see: Parkin, G. Prog. Inorg. Chem. 1998, 47, 1. For recent examples, see: (a) Sweeney, Z. K.; Polse, J. L.; Andersen, R. A.; Bergman, R. G. J. Am. Chem. Soc. 1998, 120, 7825. (b) Kuchta, M. C.; Parkin, G. J. Chem. Soc., Dalton Trans. 1998, 2279. Kuchta, M. C.; Hascall, T.; Parkin, G. Chem. Commun. 1998, 751. Hagadom, J. R.; Arnold, J. Organometallics 1998, 17, 1355. (e) Firth, A. V.; Witt, E.; Stephan, D. W. Organometallics 1998, 17, 3716. (f) Hagadorn, J. R.; Arnold, J. Inorg. Chem. 1997, 36, 2928.
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    • note
    • 8): δ 80.37 (d, J = 30.5 Hz), 70.61 (d, J = 30.5 Hz).
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    • Alternatively, A could react with 1b to generate 2b, although this pathway is more complicated than a simple dimerization of transient A as loss of a second molecule of benzene by a different mechanism must be involved
    • Alternatively, A could react with 1b to generate 2b, although this pathway is more complicated than a simple dimerization of transient A as loss of a second molecule of benzene by a different mechanism must be involved.
  • 48
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    • In control experiments, the sulfido dimers 2 do not react with 4 or 6 at room temperature to yield any observable products by NMR spectroscopy
    • In control experiments, the sulfido dimers 2 do not react with 4 or 6 at room temperature to yield any observable products by NMR spectroscopy.


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