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33747572789
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note
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3, Z = 2. At convergence, wR2 = 0.1261 and GOF= 1.371 for 182 variables refined against all 4559 unique data (as a comparison for refinement on F, R1 = 0.0505 for those 4068 data with (F>4σ(F)).
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33
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33747557921
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note
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3, Z = 2. At convergence, wR2 = 0.1530 and GOF = 1.324 for 181 variables refined against all 4778 unique data (as a comparison for refinement on F, R1 = 0.0510 for those 4574 data with (F>4σ(F)).
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34
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33747544665
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note
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b) Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Center as supplementary publication no. CCDC-112873 and CCDC-112874. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: (+44)1223-336-033; e-mail: deposit@ccdc.cam. ac.uk).
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