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0001169001
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4 (Ashton, P. R.; Shibata, K.; Shipway, A. N.; Stoddart, J.F. Angew. Chem. Int. Ed. Engl. 1997, 36, 2781) have also been reported to proceed in good yields. 1,3,5-tris(hydroxymethylbenzene) was prepared by reduction with lithium aluminium hydride in refluxing THF of the commercially available 1,3,5-trimethyl benzenetricarboxylate according to a modification of the procedure reported by Cochrane, W P.; Pauson, P. L., Stevens, T. S. J. Chem. Soc. (C) 1968, 630.
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Boekelheide, V.1
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0032491868
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have also been reported to proceed in good yields
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4 (Ashton, P. R.; Shibata, K.; Shipway, A. N.; Stoddart, J.F. Angew. Chem. Int. Ed. Engl. 1997, 36, 2781) have also been reported to proceed in good yields. 1,3,5-tris(hydroxymethylbenzene) was prepared by reduction with lithium aluminium hydride in refluxing THF of the commercially available 1,3,5-trimethyl benzenetricarboxylate according to a modification of the procedure reported by Cochrane, W P.; Pauson, P. L., Stevens, T. S. J. Chem. Soc. (C) 1968, 630.
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Ashton, P.R.1
Shibata, K.2
Shipway, A.N.3
Stoddart, J.F.4
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26
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37049129544
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4 (Ashton, P. R.; Shibata, K.; Shipway, A. N.; Stoddart, J.F. Angew. Chem. Int. Ed. Engl. 1997, 36, 2781) have also been reported to proceed in good yields. 1,3,5-tris(hydroxymethylbenzene) was prepared by reduction with lithium aluminium hydride in refluxing THF of the commercially available 1,3,5-trimethyl benzenetricarboxylate according to a modification of the procedure reported by Cochrane, W P.; Pauson, P. L., Stevens, T. S. J. Chem. Soc. (C) 1968, 630.
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J. Chem. Soc. (C)
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Cochrane, W.P.1
Pauson, P.L.2
Stevens, T.S.3
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Although the presence of starting material 1 as well as the corresponding triacetate was also observed in the crude mixture, all the products were easily separated by column chromatography
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Although the presence of starting material 1 as well as the corresponding triacetate was also observed in the crude mixture, all the products were easily separated by column chromatography.
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