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Details on crystallographic and structural parameters are reported in the Supporting Information
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Details on crystallographic and structural parameters are reported in the Supporting Information.
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2, conditioned as a 70 wt % solution in toluene
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2, conditioned as a 70 wt % solution in toluene.
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47
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33847526863
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The metal alkoxides were generated in situ from the reaction of metal chlorides with potassium tert-pentylate in THF
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The metal alkoxides were generated in situ from the reaction of metal chlorides with potassium tert-pentylate in THF.
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Complex G has been characterized by X-ray crystal structure, and recently shown to reduce ketones. (see ref 27b)
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We thank a reviewer for this pertinent suggestion
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We thank a reviewer for this pertinent suggestion.
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NMR spectra are reported in the Supporting Information
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NMR spectra are reported in the Supporting Information.
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64
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84985265311
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This is a modified procedure from the original method using 1,2dichloroethane and α-phenylethylamine. Horner, L.; Dickerhof, K. Liebigs Ann. Chem. 1984, 1240.
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