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Care was taken in order to compensate for the solution resistance. However, a contribution from residual uncompensated resistance cannot be totally ruled out.
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The electrochemical techniques usually used for these kinetics studies are powerful tools but they suffer from difficulties when the electrode surface is modified during the oxidation process as in our case (irreversible wave). Laser flash photolysis and pulse radiolysis are additional independent methods that allow study of the production of radicals and determination of rate constants of their ensuing reactions.
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The detection concerning the material itself (that means the oligothiophenes constituting the polymeric backbone) failed. It may be caused by its lack of solubility, leading to its precipitation in the matrix. On the other hand, some experiments have shown that there is a good affinity between HPβCD and DMF: for instance, solubilization of a BT-βCD complex in DMF leads to its dethreading. As a result, DMF could extract the HPβCD molecules from the material and these latter could be readily detected through MALDI-MS.
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