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Volumn , Issue 6, 1998, Pages 471-472

Benzo[1,2:4,5]bis(1,1,2,2-tetraisopropyldisilacyclobutene)

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Indexed keywords


EID: 0032361280     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1998.471     Document Type: Article
Times cited : (28)

References (34)
  • 22
    • 0043210575 scopus 로고    scopus 로고
    • note
    • A solution of 3 (0.910 g, 1.35 mmol) in toluene (5 ml) was added to a mixture of sodium (0.220 g, 9.57 mmol) and toluene (30 ml) under reflux. The reaction mixture was refluxed for 33 h. Insoluble materials were filtered off, and the solvent was removed under reduced pressure. The residue was recrystallized from hexane to give 1 (0.607 g, 85%) as colorless crystals.
  • 23
    • 0041707873 scopus 로고    scopus 로고
    • note
    • 4: C, 67.84; H, 11.01%.
  • 24
    • 0043210574 scopus 로고    scopus 로고
    • note
    • We also synthesized benzo[1,2:4,5]bis(1,1,2.2-tetramethyldisilacyclobutene). However, this compound is quite easily oxidized in air.
  • 25
    • 0042208287 scopus 로고    scopus 로고
    • note
    • 0)) for 2.382 observed reflections.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.