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Although Suzuki and co-workers have quite recently reported that the copolymers of 9,10-bis(chloromethylpropylsilyl)anthracene and dichloromethylphenylsilane have strong emission properties, the structure and the emission properties of the monomer 9,10-bis-(chloromethylpropylsilyl)anthracene itself have not been described. See: Suzuki, H.; Satoh, S.; Kimata, Y.; Kuriyama, A. Chem. Lett. 1995, 451.
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20 However, we could obtain 1-4 with butyllithium in diethyl ether or tertbutyllithium in THF without using TMEDA.
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