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Mansky, P.1
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B. Collin, D. Chatenay, G. Coulon, D. Ausserre, Y. Gallot, Macromolecules 25, 1621 (1992); L. H. Radzilowski, B. L. Carvahlo, E. L. Thomas, J. Polym. Sci. Part B Polym. Phys. 34, 3081 (1996); P. Mansky, Y. Liu, E. Huang, T. P. Russell, C. Hawker, Science 275, 1458 (1997); S. I. Stupp et al., ibid. 276, 384 (1997).
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Stupp, S.I.1
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45
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1842385637
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note
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The inclination θ of neighboring columns was measured as a function of z, the distance from the dislocation along the Burger's vector (that is, perpendicular to the central column), and λ was determined most accurately by fitting the equation θ = 1/4√π a/√λz
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46
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0003943162
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De Gennes, P.-G.1
Prost, J.2
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50
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1842359642
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note
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The [001] zone axis is typically perpendicular to the film surface, and the ED pattern shown in Fig. 5C [containing the (200) and (210) reflections] was obtained at normal beam incidence. In addition, the following low-angle reflections in the [001] zone were observed: (400), (320), (220) and (310), listed in order of decreasing intensity. At wide angles, a diffuse ring was observed centered at 4.6 Å, indicating that the structure at the atomic level is disordered. The (211) reflection, which is strong and of comparable intensity to the (200) and (210) reflections, can be observed as expected, if the specimen is tilted 27° or 45° about the [100] axis.
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51
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0023834299
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P. Pradere, J. F. Revol, L. Nguyen, R. S. Manley, Ultramicroscopy 25, 69 (1988).
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Pradere, P.1
Revol, J.F.2
Nguyen, L.3
Manley, R.S.4
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0017884417
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C. Tanford, Science 200, 1012 (1978).
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Tanford, C.1
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53
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1842304756
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note
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4 staining. Identical ED patterns are obtained from unstained samples. However, the material is sensitive to the electron beam, and the low-angle reflections disappear during irradiation, because the electron beam induces structural rearrangements which destroy the order. Stained samples are more resistant to the electron beam.
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1842277885
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Supported by NSF and the Engineering and Physical Science Research Council, UK
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Supported by NSF and the Engineering and Physical Science Research Council, UK.
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