Enzyme-mediated optical resolution of 2-methyl-3,4-pentadien-1-ol, a chiral building block possessing terminal allenyl group

Synlett

Volumn 1997, Issue 11, 1997, Pages 1297-1299

  Konegawa, Tadayoshi ^a   Ohtsuka, Yoshikazu ^a   Ikeda, Hajime ^a   Sugai, Takeshi ^a   Ohta, Hiromichi ^a  

^a KEIO UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0013549779     PISSN: 09365214     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-1997-1034     Document Type: Article

References (71)

1. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
2. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
3. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
4. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
5. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
6. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
7. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
8. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
9. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
10. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
11. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
12. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
13. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
14. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
15. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
16. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
17. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
18. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
19. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
20. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
21. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
22. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
23. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
24. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
25. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
26. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
27. Henrick, C. A.; Willy, W. E.; McKean, D. R.; Baggiolini, E.; Siddal, J. B. J. Org. Chem. 1975, 40, 8-14. Tsuboi, S.; Masuda, T.; Makino, H.; Takeda, A. Tetrahedron Lett. 1982, 23, 209-212. Tsuboi, S.; Masuda, T.; Takeda, A. J. Org. Chem. 1982, 47, 4478-4482. Mori, K.; Maemoto, S. Liebigs Ann. Chem. 1987, 1987, 863-869. Friesen, R. W.; Giroux, A. Tetrahedron Lett. 1993, 34, 1867-1870. Lautens, M.; Delanghe, P. H. M. J. Am. Chem. Soc. 1994, 116, 8526-8535. Shibata, T.; Koga, Y.; Narasaka, K. Bull. Chem. Soc. Jpn. 1995, 68, 911-919. Yamaguchi, M.; Kido, Y.; Omata, K.; Hirama, M. Synlett 1995, 1181-1182. Lautens, M.; Ren, Y. J. Org. Chem. 1995, 61, 2210-2214. Kobayashi, S.; Nishio, K. J. Am. Chem. Soc. 1995, 117, 6392-6393. Friesen, R. W.; Bayly, C. I.; Fogg, J. A. J. Org. Chem. 1995, 61, 448-451. Shiratani, T.; Kimura, K.; Yoshihara, K.; Hatakeyama, S.; Irie, H.; Miyashita, M. Chem. Commun. 1996, 21-22. Laux, M.; Krause, N.; Koop, U. Synlett 1996, 87-88. Chino, M.; Liang, G. H.; Matsumoto. T.; Suzuki, K. Chem. Lett. 1996, 221-222. Okamoto, S.; Kasatkin, A.; Zubaidha, P. K.; Sato, F. J. Am. Chem. Soc. 1996, 118, 2208-2216. David, K.; Areinte, C.; Greiner, A.; Goré, J.; Cazes, B. Tetrahedron Lett. 1996, 37, 3335-3338. Myers, A. G.; Zheng, B. J. Am. Chem. Soc. 1996, 118, 4492-4493. Araki, S.; Usui, H.; Kato, M.; Butsugan, Y. J. Am. Chem. Soc. 1996, 118, 4699-4700. Grissom, J. W.; Gunawardena, G. U.; Klingberg, D.; Huang, D. Tetrahedron 1996, 52, 6453-6518. Okuro, K.; Alper, H. J. Org. Chem. 1997, 62, 1566-1567. Shepard, M. S.; Carreira, E. M. J. Am. Chem. Soc. 1997, 119, 2597-2605. Yamanoi, S.; Imai, T.; Matsumoto, T.; Suzuki, K. Tetrahedron Lett. 1997, 38, 3031-3034. Jin, J.; Weinreb, S. M. J. Am. Chem. Soc. 1997, 119, 5773-5784. See also reviews: Chan, T. H.; Ong, B. S. Tetrahedron 1980, 36, 2269. Pasto, D. J. Tetrahedron 1984, 40, 2805. Tsuboi, S. Yukigosei Kagaku Kyokaishi (J. Synth. Org. Chem. Soc., Jpn.) 1988, 46, 909-920. Fredrick, M. A.; Hulce, M. Tetrahedron 1997, 53, 10197-10227.
28. Suzuki, K.; Imai, T.; Yamanoi, S.; Chino, M.; Matsumoto, T.; Angew. Chem., Int. Ed. Engl., 1997, in press. For a general information of metalocene-mediated stereoselective synthesis, see also a review: Suzuki, K. Pure Appl. Chem. 1994, 66, 1557-1564.
29. Suzuki, K.; Imai, T.; Yamanoi, S.; Chino, M.; Matsumoto, T.; Angew. Chem., Int. Ed. Engl., 1997, in press. For a general information of metalocene-mediated stereoselective synthesis, see also a review: Suzuki, K. Pure Appl. Chem. 1994, 66, 1557-1564.
30. -1.
31. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
32. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
33. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
34. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.;
35. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
36. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
37. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
38. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
39. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
40. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
41. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
42. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
43. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
44. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
45. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
46. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
47. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
48. Lipase-catalyzed resolution of chiral primary alcohols: Terao, Y.; Murata, M.; Achiwa, K.; Nishio, T.; Akamatsu, M.; Kamimura, M. Tetrahedron Lett. 1988, 29, 5173-5176. Wang, Y.-F.; Wong, C.-H. J. Org. Chem. 1988, 53, 3127-3129. Bianchi, D.; Cesti, P. J. Org. Chem. 1990, 55, 5657-5659. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. J. Org. Chem. 1990, 55, 6214-6216. Ferraboschi, P.; Grisenti, P.; Santaniello, E. Synlett 1990, 545-546. Dealinck, D. L.; Margolin, A. L. Tetrahedron Lett. 1990, 31, 3093-3096. Chen, C.-S.; Liu, Y.-C. J. Org. Chem. 1991, 56, 1966-1968. Matsumoto, T.; Takeda, Y.; Terao, H.; Takahashi, T.; Wada, M. Chem. Pharm. Bull. 1993, 41, 1459-1461. Akita, H.; Umezawa, I.; Nozawa, M.; Nagumo, S. Tetrahedron: Asymmetry 1993, 3, 757-760. Bianchi, D.; Battistel, E.; Bosetti, A.; Cesti, P.; Fekéte, Z. Tetrahedron: Asymmetry 1993, 3, 777-782. Matsumoto, T.; Takeda, Y.; Iwata, E.; Sakamoto, M.; Ishida, T. Chem. Pharm. Bull. 1994, 42, 1191-1197. Akita, H.; Nozawa, M.; Nagumo, S. Chem. Pharm. Bull. 1994, 42, 1208-1212. Ferraboschi, P.; Grisenti, P.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1994, 5, 691-698. Nordin, O.; Hedenström, E.; Högberg, H.-E. Tetrahedron: Asymmetry 1994, 5, 785-788. Sih, C. J.; Gu, R. L. Tetrahedron: Asymmetry 1995, 6, 357-360. Ferraboschi, P.; Casati, S.; Manzocchi, A.; Santaniello, E. Tetrahedron: Asymmetry 1995, 6, 1521-1524. Akita, H.; Chen, C. Y.; Uchida, K. Tetrahedron: Asymmetry 1995, 6, 2131-2134. Gais, H.-J.; von der Weiden, I. Tetrahedron: Asymmetry 1996, 7, 1253-1256.
49. Enzyme-mediated discrimination of enantiomers caused by axial chirality of allene has been attempted. Rambeck, R.; Simon, H. Angew. Chem., Int. Ed. Engl. 1974, 13, 609. Bertrand, M.; Ferre, E.; Gil, G.; Le Petit, J.; Devoze, L. Tetrahedron Lett. 1980, 21, 1711-1714. Ferre, E.; Gil, G.; Bertrand, M.; Le Petit, J. Appl. Microbiol. Biotechnol. 1985, 21, 258-266. Ramaswamy, S.; Hui, R. A. H. F.; Jones, J. B. J. Chem. Soc., Chem. Commun. 1986, 1545-1546. Gil, G.; Ferre, E.; Meon, A.; Le Petit, J.; Triantaphylides Tetrahedron Lett. 1987, 28, 1647-1648. Beard, T.; Cohen, M. A.; Parratt, J. S.; Turner, N. J.; Crosby, J.; Moilliet, J. Tetrahedron: Asymmetry 1993, 4, 1085-1104.
50. Enzyme-mediated discrimination of enantiomers caused by axial chirality of allene has been attempted. Rambeck, R.; Simon, H. Angew. Chem., Int. Ed. Engl. 1974, 13, 609. Bertrand, M.; Ferre, E.; Gil, G.; Le Petit, J.; Devoze, L. Tetrahedron Lett. 1980, 21, 1711-1714. Ferre, E.; Gil, G.; Bertrand, M.; Le Petit, J. Appl. Microbiol. Biotechnol. 1985, 21, 258-266. Ramaswamy, S.; Hui, R. A. H. F.; Jones, J. B. J. Chem. Soc., Chem. Commun. 1986, 1545-1546. Gil, G.; Ferre, E.; Meon, A.; Le Petit, J.; Triantaphylides Tetrahedron Lett. 1987, 28, 1647-1648. Beard, T.; Cohen, M. A.; Parratt, J. S.; Turner, N. J.; Crosby, J.; Moilliet, J. Tetrahedron: Asymmetry 1993, 4, 1085-1104.
51. Enzyme-mediated discrimination of enantiomers caused by axial chirality of allene has been attempted. Rambeck, R.; Simon, H. Angew. Chem., Int. Ed. Engl. 1974, 13, 609. Bertrand, M.; Ferre, E.; Gil, G.; Le Petit, J.; Devoze, L. Tetrahedron Lett. 1980, 21, 1711-1714. Ferre, E.; Gil, G.; Bertrand, M.; Le Petit, J. Appl. Microbiol. Biotechnol. 1985, 21, 258-266. Ramaswamy, S.; Hui, R. A. H. F.; Jones, J. B. J. Chem. Soc., Chem. Commun. 1986, 1545-1546. Gil, G.; Ferre, E.; Meon, A.; Le Petit, J.; Triantaphylides Tetrahedron Lett. 1987, 28, 1647-1648. Beard, T.; Cohen, M. A.; Parratt, J. S.; Turner, N. J.; Crosby, J.; Moilliet, J. Tetrahedron: Asymmetry 1993, 4, 1085-1104.
52. Enzyme-mediated discrimination of enantiomers caused by axial chirality of allene has been attempted. Rambeck, R.; Simon, H. Angew. Chem., Int. Ed. Engl. 1974, 13, 609. Bertrand, M.; Ferre, E.; Gil, G.; Le Petit, J.; Devoze, L. Tetrahedron Lett. 1980, 21, 1711-1714. Ferre, E.; Gil, G.; Bertrand, M.; Le Petit, J. Appl. Microbiol. Biotechnol. 1985, 21, 258-266. Ramaswamy, S.; Hui, R. A. H. F.; Jones, J. B. J. Chem. Soc., Chem. Commun. 1986, 1545-1546. Gil, G.; Ferre, E.; Meon, A.; Le Petit, J.; Triantaphylides Tetrahedron Lett. 1987, 28, 1647-1648. Beard, T.; Cohen, M. A.; Parratt, J. S.; Turner, N. J.; Crosby, J.; Moilliet, J. Tetrahedron: Asymmetry 1993, 4, 1085-1104.
53. Enzyme-mediated discrimination of enantiomers caused by axial chirality of allene has been attempted. Rambeck, R.; Simon, H. Angew. Chem., Int. Ed. Engl. 1974, 13, 609. Bertrand, M.; Ferre, E.; Gil, G.; Le Petit, J.; Devoze, L. Tetrahedron Lett. 1980, 21, 1711-1714. Ferre, E.; Gil, G.; Bertrand, M.; Le Petit, J. Appl. Microbiol. Biotechnol. 1985, 21, 258-266. Ramaswamy, S.; Hui, R. A. H. F.; Jones, J. B. J. Chem. Soc., Chem. Commun. 1986, 1545-1546. Gil, G.; Ferre, E.; Meon, A.; Le Petit, J.; Triantaphylides Tetrahedron Lett. 1987, 28, 1647-1648. Beard, T.; Cohen, M. A.; Parratt, J. S.; Turner, N. J.; Crosby, J.; Moilliet, J. Tetrahedron: Asymmetry 1993, 4, 1085-1104.
54. Enzyme-mediated discrimination of enantiomers caused by axial chirality of allene has been attempted. Rambeck, R.; Simon, H. Angew. Chem., Int. Ed. Engl. 1974, 13, 609. Bertrand, M.; Ferre, E.; Gil, G.; Le Petit, J.; Devoze, L. Tetrahedron Lett. 1980, 21, 1711-1714. Ferre, E.; Gil, G.; Bertrand, M.; Le Petit, J. Appl. Microbiol. Biotechnol. 1985, 21, 258-266. Ramaswamy, S.; Hui, R. A. H. F.; Jones, J. B. J. Chem. Soc., Chem. Commun. 1986, 1545-1546. Gil, G.; Ferre, E.; Meon, A.; Le Petit, J.; Triantaphylides Tetrahedron Lett. 1987, 28, 1647-1648. Beard, T.; Cohen, M. A.; Parratt, J. S.; Turner, N. J.; Crosby, J.; Moilliet, J. Tetrahedron: Asymmetry 1993, 4, 1085-1104.
55. R (min): 1.94 (1b), 3.63 (1c). A conventional workup and chromatography afforded the hydrolyzed product 1b and the recovery of the starting material 1c.
56. Chen, C.-S.; Fujimoto, Y.; Girdaukas, G.; Sih, C. J. J. Am. Chem. Soc. 1982, 104, 7294-7299.
57. Indlekofer, M.; Reuss, M.; Barth, S.; Effenberger, F. Biocatalysis 1993, 7, 249-266. Barth, S.; Effenberger, F. Tetrahedron: Asymmetry 1993, 4, 823-834. Majeric, M.; Sunjic, V. Tetrahedron: Asymmetry 1996, 7, 815-824. For the enantioselectivity-structure relationship, see also Weissfloch, A. N. E.; Kazlauskas, R. J. J. Org. Chem. 1995, 60, 6959-6969.
58. Indlekofer, M.; Reuss, M.; Barth, S.; Effenberger, F. Biocatalysis 1993, 7, 249-266. Barth, S.; Effenberger, F. Tetrahedron: Asymmetry 1993, 4, 823-834. Majeric, M.; Sunjic, V. Tetrahedron: Asymmetry 1996, 7, 815-824. For the enantioselectivity-structure relationship, see also Weissfloch, A. N. E.; Kazlauskas, R. J. J. Org. Chem. 1995, 60, 6959-6969.
59. Indlekofer, M.; Reuss, M.; Barth, S.; Effenberger, F. Biocatalysis 1993, 7, 249-266. Barth, S.; Effenberger, F. Tetrahedron: Asymmetry 1993, 4, 823-834. Majeric, M.; Sunjic, V. Tetrahedron: Asymmetry 1996, 7, 815-824. For the enantioselectivity-structure relationship, see also Weissfloch, A. N. E.; Kazlauskas, R. J. J. Org. Chem. 1995, 60, 6959-6969.
60. Indlekofer, M.; Reuss, M.; Barth, S.; Effenberger, F. Biocatalysis 1993, 7, 249-266. Barth, S.; Effenberger, F. Tetrahedron: Asymmetry 1993, 4, 823-834. Majeric, M.; Sunjic, V. Tetrahedron: Asymmetry 1996, 7, 815-824. For the enantioselectivity-structure relationship, see also Weissfloch, A. N. E.; Kazlauskas, R. J. J. Org. Chem. 1995, 60, 6959-6969.
61. Ohtsuka, Y.; Katoh, O.; Sugai, T.; Ohta, H. Bull. Chem. Soc., Jpn. 1997, 70, 483-491.
62. For the effect of solvent and temperature, Sakai, T.; Kawabata, I.; Kishimoto, T.; Ema, T.; Utaka, M. J. Org. Chem. 1997, 62, 4906-4907. A review: Chen, C.-S.; Sih, C. J. Angew. Chem. Int. Ed. Engl. 1989, 28, 695-707. Kvittingen, L. Tetrahedron 1994, 50, 8253-8274.
63. For the effect of solvent and temperature, Sakai, T.; Kawabata, I.; Kishimoto, T.; Ema, T.; Utaka, M. J. Org. Chem. 1997, 62, 4906-4907. A review: Chen, C.-S.; Sih, C. J. Angew. Chem. Int. Ed. Engl. 1989, 28, 695-707. Kvittingen, L. Tetrahedron 1994, 50, 8253-8274.
64. For the effect of solvent and temperature, Sakai, T.; Kawabata, I.; Kishimoto, T.; Ema, T.; Utaka, M. J. Org. Chem. 1997, 62, 4906-4907. A review: Chen, C.-S.; Sih, C. J. Angew. Chem. Int. Ed. Engl. 1989, 28, 695-707. Kvittingen, L. Tetrahedron 1994, 50, 8253-8274.
65. Takagi, Y.; Teramoto, J.; Kihara, H.; Itoh, T.; Tsukube, H. Tetrahedron Lett. 1996, 37, 4991-4992.
66. Ema, T.; Maeno, S.; Takaya, Y.; Sakai, T.; Utaka, M. Tetrahedron: Asymmetry 1996, 7, 625-628.
67. 3); 95.9% e.e.
68. 6: C, 53.42; H, 4.14; N, 9.58. Found: C, 53.41; H, 4.17; N, 9.43. which was hydrolyzed to give 1b and further converted to 1a. It was confirmed to be enantiomerically pure within the experimental error of the GLC analysis.
69. Cradall, J. K.; Tindell, G. L. J. Chem. Soc., Chem. Commun. 1970, 1411-1412. Dauben, W. G.; Shapiro, G. J. Org. Chem. 1984, 49, 4252-4258.
70. Cradall, J. K.; Tindell, G. L. J. Chem. Soc., Chem. Commun. 1970, 1411-1412. Dauben, W. G.; Shapiro, G. J. Org. Chem. 1984, 49, 4252-4258.
71. Yamanoi, S.; Matsumoto, T.; Suzuki, K., personal communication. They prepared (R)-1a from commercially available methyl (S)-3-hydroxy-2-methylpropionate.