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Volumn 579, Issue 1-2, 1999, Pages 18-23

A methylene bridged dialuminium compound as a chelating Lewis acid - Complexation of azide and acetate anions by R2Al-CH2-AlR2 [R = CH(SiMe3)2]

Author keywords

Aluminium; Chelates; Lewis acids

Indexed keywords


EID: 0002956662     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(98)01150-4     Document Type: Article
Times cited : (68)

References (64)
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    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
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    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
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    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
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    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
    • (1997) J. Organomet. Chem. , vol.539 , pp. 187
    • Kaul, F.A.R.1    Tschinkl, M.2    Gabbai, F.P.3
  • 11
    • 0000173891 scopus 로고
    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
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    • Khan, M.A.1    Peppe, C.2    Tuck, D.G.3
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    • 0002001369 scopus 로고    scopus 로고
    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
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    • Gabbai, F.P.1    Schier, A.2    Riede, J.3
  • 13
    • 0001685792 scopus 로고    scopus 로고
    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
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    • Gabbai, F.P.1    Schier, A.2    Riede, J.3    Schichl, D.4
  • 14
    • 0000452878 scopus 로고    scopus 로고
    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
    • (1997) Organometallics , vol.16 , pp. 4759
    • Tschinkl, M.1    Schier, A.2    Riede, J.3    Schmidt, E.4    Gabbai, F.P.5
  • 15
    • 0001149019 scopus 로고    scopus 로고
    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
    • (1997) Inorg. Chem. , vol.36 , pp. 5694
    • Gabbai, F.P.1    Schier, A.2    Riede, J.3    Sladek, A.4    Görlitzer, H.W.5
  • 16
    • 0000661734 scopus 로고    scopus 로고
    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
    • (1997) Inorg. Chem. , vol.36 , pp. 5706
    • Tschinkl, M.1    Schier, A.2    Riede, J.3    Gabbai, F.P.4
  • 17
    • 0000315026 scopus 로고    scopus 로고
    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
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    • Saied, O.1    Simard, M.2    Wuest, J.D.3
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    • Some examples for chelating Lewis acids, more derivatives are cited in the following references: (a) M.R. Ort, E.H. Mottus, J. Organomet. Chem. 50 (1973) 47. (b) H. Martin, H. Bretinger, Z. Naturforsch. B: Chem. Sci. 46 (1991) 615. (c) W. Uhl, M. Layh, J. Organomet. Chem. 415 (1991) 181. (d) F.A.R. Kaul, M. Tschinkl, F.P. Gabbai, ibid. 539 (1997) 187. (e) M.A. Khan, C. Peppe, D.G. Tuck, Organometallics 5 (1986) 525. (f) F.P. Gabbai, A. Schier, J. Riede, Chem. Commun. (1996) 1121. (g) F.P. Gabbai, A. Schier, J. Riede, D. Schichl, Organometallics 15 (1996) 4119. (h) M. Tschinkl, A. Schier, J. Riede, E. Schmidt, F.P. Gabbai, ibid. 16 (1997) 4759. (i) F.P. Gabbai, A. Schier, J. Riede, A. Sladek, H.W. Görlitzer, Inorg. Chem. 36 (1997) 5694. (j) M. Tschinkl, A. Schier, J. Riede, F.P. Gabbai, ibid. 36 (1997) 5706. (k) O. Saied, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1128. (l) E.C. Ashby, R.S. Smith, J. Organomet. Chem. 225 (1982) 71. A dialuminium compound has been used in catalytic processes: (m) T. Ooi, M. Takahashi, K. Maruoka, J. Am. Chem. Soc. 118 (1996) 11307. (n) T. Ooi, E. Tayama, T. Takahashi, K. Maruoka, Tetrahedron Lett. 38 (1997) 7403. (o) T. Ooi, T. Miura, K. Maruoka, Angew. Chem. 110 (1998) 2524; Angew. Chem. Int. Ed. Engl. 37 (1998) 2347.
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    • The crystallographic data of 7 and 8 (excluding structure factors) were deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-104482 (7) and -104483 (8). Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, GB-Cambridge CB2 IEZ, UK (fax: +44-(1223) 336-033; e-mail: deposit@chemcrys.cam.ac.uk)
    • The crystallographic data of 7 and 8 (excluding structure factors) were deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-104482 (7) and -104483 (8). Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, GB-Cambridge CB2 IEZ, UK (fax: +44-(1223) 336-033; e-mail: deposit@chemcrys.cam.ac.uk).


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