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2 systems (M = Pd, Pt), where R is an alkyl group: (a) DiCosimo, R.; Whitesides, G. M. J. Am. Chem. Soc. 1982, 104, 3601-3607. (b) Ozawa, F.; Ito, T.; Nakamura, Y.; Yamamoto, A. Bull. Chem. Soc. Jpn. 1981, 54, 1868-1880. (c) Gille, A.; Stille, J. K. J. Am. Chem. Soc. 1980, 102, 4933-4941. (d) Moravskiy, A.; Stille, J. K. J. Am. Chem. Soc. 1981, 103, 4182-4186. (e) Foley, P.; DiCosimo, R.; Whitesides, G. M. J. Am. Chem. Soc. 1980, 102, 6713-6725. (f) McCarthy, T. J.; Nuzzo, R. G. Whitesides, G. M. J. Am. Chem. Soc. 1981, 103, 3396-3403. (g) Tatsumi, K.; Hoffmann, R.; Yamamoto, A.; Stille, J. K. Bull. Chem. Soc. Jpn. 1981, 54, 1857-1867. However, when at least one organic group is unsaturated, reductive elimination often occurs directly from the four-coordinate species: (h) Loar, M. K.; Stille, J. K. J. Am. Chem. Soc. 1981, 103, 4174-4181. (i) Brown, J. M.; Cooley, N. A. Chem. Rev. 1988, 88, 1031-1046, and references therein, (j) Ozawa, F.; Kurihara, K.; Fujimori, M.; Hidaka, T.; Toyoshima, T.; Yamamoto, A. Organometallics 1989, 8, 180-188. (k) Calhorda, M. J.; Brown, J. M.; Cooley, N. A. Organometallics 1991, 10, 1431-1438. (l) Kohara, T.; Yamamoto, T.; Yamamoto, A. J. Organomet. Chem. 1980, 192, 265-274. (m) Abis, L.; Sen, A.; Halpern, J. J. Am. Chem. Soc. 1978, 100, 2915-2916.
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85034301028
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note
-
It has been noted that the integration program SAINT produces cell constant errors that are unreasonably small, since systematic error is not included. More reasonable errors might be estimated at 10× the listed value.
-
-
-
-
75
-
-
84977289324
-
-
The SADABS program is based on the method of Blessing; see: Blessing, R. H. Acta Crystallogr., Sect A 1995, 51, 33-38.
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Blessing, R.H.1
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