Synthesis and Structural Characterization of the Solvent-Free Potassium Derivative of a Terphenyl-Substituted Primary Phosphane: [(2,6-Dimesitylphenyl)P(H)K]4

Inorganic Chemistry

Volumn 37, Issue 25, 1998, Pages 6541-6543

  Rabe, Gerd W ^a   Kheradmandan, Sohrab ^a   Yap, Glenn P A ^b  

^a TECHNICAL UNIVERSITY OF MUNICH   (Germany)

^b UNIVERSITY OF OTTAWA   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0001566219     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic980585m     Document Type: Article

References (65)

1. (a) Bartlett, R. A.; Olmstead, M. M.; Power, P. P.; Sigel, G. A. Inorg. Chem. 1987, 26, 1941.
2. (b) Bartlett, R. A.; Olmstead, M. M.; Power, P. P. Inorg. Chem. 1986, 25, 1243.
3. (c) Hope, H.; Olmstead, M. M.; Power, P. P.; Xu, X. J. Am. Chem. Soc. 1984, 106, 819.
4. (d) Bartlett, R. A.; Dias, H. V. R.; Hope, H.; Murray, B. D.; Olmstead, M. M.; Power, P. P. J. Am. Chem. Soc. 1986, 108, 6921.
5. (e) Hitchcock, P. B.; Lappert, M. F.; Power, P. P.; Smith, S. J. J. Chem. Soc., Chem. Commun. 1984, 1669.
6. (f) Hey-Hawkins, E.; Sattler, E. J. Chem. Soc., Chem. Commun. 1992, 775.
7. (g) Rabe, G. W.; Schier, A.; Riede, J. Acta Crystallogr. 1996, A52, 1350.
8. (h) Kurz, S.; Hey-Hawkins, E. Organometallics 1992, 11, 2729.
9. (i) Niediek, K.; Neumüller, B. Z. Anorg. Allg. Chem. 1993, 619, 885.
10. (j) Hey, E.; Hitchcock, P. B.; Lappert, M. F.; Rai, A. K. J. Organomet. Chem. 1987, 325, 1.
11. (k) Driess, M.; Huttner, G.; Knopf, N.; Pritzkow, H.; Zsolnai, L. Angew. Chem., Int. Ed. Engl. 1995, 34, 316.
12. (l) Driess, M.; Rell, S.; Pritzkow, H.; Janoschek, R. J. Chem. Soc., Chem. Commun. 1996, 305.
13. (m) Driess, M.; Pritzkow, H.; Martin, S.; Rell, S.; Fenske, D.; Baum, G. Angew. Chem., Int. Ed. Engl. 1996, 35, 986.
14. (n) Jones, R. A.; Stuart, A. L.; Wright, T. C. J. Am. Chem. Soc. 1983, 105, 7459.
15. (o) Hey-Hawkins, E.; Kurz, S. Phosphorus, Sulfur Silicon 1994, 90, 281.
16. (p) Hey, E.; Weller, F. J. Chem. Soc., Chem. Commun. 1988, 782.
17. (q) Becker, G.; Eschbach, B.; Käshammer, D.; Mundt, O. Z. Anorg. Allg. Chem. 1994, 620, 29.
18. (r) Becker, G.; Eschbach, B.; Mundt, O.; Seidler, N. Z. Anorg. Allg. Chem. 1994, 620, 1381.
19. (s) Pauer, F.; Power, P. P. In Lithium Chemistry: A Theoretical and Experimental Overview; Sapse, A.-M., Schleyer, P. v. R., Eds.; Wiley: New York, 1994; Chapter 9, p 361 and references therein.
20. (a) Rabe, G. W.; Kheradmandan, S.; Heise, H.; Liable-Sands, L. M.; Guzei, I. A.; Rheingold, A. L. Main Group Chem. 1998, 2, 221.
21. (b) Aspinall, H. C.; Tillotson, M. R. Inorg. Chem. 1996, 35, 5.
22. (c) Koutsantonis, G. A.; Andrews, P. C.; Raston, C. L. J. Chem. Soc., Chem. Commun. 1995, 47.
23. (d) Andrianarison, M.; Stalke, D.; Klingebiel, U. Chem. Ber. 1990, 123, 71.
24. (e) Frenzel, C.; Jörchel, P.; Hey-Hawkins, E. J. Chem. Soc., Chem. Commun. 1998, 1363.
25. (f) Driess, M.; Pritzkow, H.; Skipinski, M.; Winkler, U. Organometallics 1997, 16, 5108.
26. (g) Englich, U.; Hassler, K.; Ruhlandt-Senge, K.; Uhlig, F. Inorg. Chem. 1998, 37, 3532.
27. (h) Paul, F.; Carmichael, D.; Ricard, L.; Mathey, F. Angew. Chem., Int. Ed. Engl. 1996, 35, 1125.
28. (i) Gosink, H.-J.; Nief, F.; Ricard, L.; Mathey, F. Inorg. Chem. 1995, 34, 1306.
29. (j) Fermin, M. C.; Ho, J.; Stephan, D. W. J. Am. Chem. Soc. 1994, 116, 6033.
30. (k) Fermin, M. C.; Ho, J.; Stephan, D. W. Organometallics 1995, 14, 4247.
31. Rabe, G. W.; Yap, G. P. A.; Rheingold, A. L. Inorg. Chem. 1997, 36, 1990.
32. Rabe, G. W.; Heise, H.; Yap, G. P. A.; Liable-Sands, L. M.; Guzei, I. A.; Rheingold, A. L. Inorg. Chem. 1998, 37, 4235.
33. (a) Cowley, A. H.; Norman, N. C.; Pakulski, M.; Backer, G.; Layh, M.; Kirchner, E.; Schmidt, M. Inorg. Synth. 1990, 27, 235.
34. (b) Yoshifuji, M.; Shima, I.; Inamoto, N.; Hirotsu, K.; Higuchi, T. J. Am. Chem. Soc. 1981, 103, 4587.
35. (a) Du, F. C.; Hart, H.; Ng, K. D. J. Org. Chem. 1986, 51, 3162.
36. (b) Ruhlandt-Senge, K.; Ellison, J. E.; Wehmschulte, R. J.; Pauer, F.; Power, P. P. J. Am. Chem. Soc. 1993, 115, 11353.
37. (c) Saednya, A.; Hart, H. Synthesis 1996, 1455.
38. (a) Rabe, G. W.; Kheradmandan, S.; Liable-Sands, L. M.; Guzei, I. A.; Rheingold, A. L. Angew. Chem., Int. Ed. Engl. 1998, 37, 1404.
39. (b) Smith, J. D. Angew. Chem., Int. Ed. Engl. 1998, 37, 2071.
40. Urnezius, E.; Protasiewicz, J. D. Main Group Chem. 1996, 1, 369.
41. -3. All software and sources of scattering factors are contained in the SHELXTL (5.03) program library (G. Sheldrick, Siemens XRD, Madison, WI).
42. (a) Hitchcock, P. B.; Lappert, M. F.; Lawless, G. A.; Royo, B. J. Chem. Soc., Chem. Commun. 1993, 554.
43. (b) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Smith, J. D. Angew. Chem., Int. Ed. Engl. 1995, 34, 2679.
44. (c) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Smith, J. D. Angew. Chem., Int. Ed. Engl. 1995, 34, 687.
45. (d) Eaborn, C.; Hitchcock, P. B.; Izod, K.; Jaggar, A. J.; Smith, J. D. Organometallics 1994, 13, 753.
46. (e) Schaverien, C. J.; van Mechelen, J. B. Organometallics 1991, 10, 1704.
47. (f) Hoffmann, D.; Bauer, W.; Schleyer, P. v. R.; Pieper, U.; Stalke, D. Organometallics 1993, 12, 1193.
48. (g) McGeary, M. J.; Cayton, R. H.; Folting, K.; Huffman, J. C.; Caulton, K. G. Polyhedron 1992, 11, 1369.
49. (h) Fuentes, G. R.; Coan, P. S.; Streib, W. E.; Caulton, K. G. Polyhedron 1991, 10, 2371.
50. (i) Clark, D. L.; Hollis, R. V.; Scott, B. L.; Watkin, J. G. Inorg. Chem. 1996, 35, 667.
51. (j) Steiner, A.; Stalke, D. Inorg. Chem. 1993, 32, 1977.
52. (k) Neumüller, B.; Gahlmann, F. Chem. Ber. 1993, 126, 1579.
53. (1) Klinkhammer, K. W.; Schwarz, W. Z. Anorg. Allg. Chem. 1993, 619, 1777.
54. (m) Niemeyer, M.; Power, P. P. Inorg. Chem. 1996, 35, 7264.
55. (n) Klinkhammer, K. W. Chem. - Eur. J. 1997, 3, 1418.
56. (o) Bock, H.; Hauch, T.; Näther, C. Organometallics 1996, 15, 1527.
57. (p) Gregory, K.; Bremer, M.; Schleyer, P. v. R.; Klusener, P. A. A.; Brandsma, L. Angew. Chem., Int. Ed. Engl. 1989, 28, 1224.
58. (q) Smith, J. D. Adv. Organomet. Chem. 1999, 43, 267.
59. von Schnering, H. G.; Hönle, W. Z. Anorg. Allg. Chem. 1979, 456, 194.
60. Mulvey, R. E. Chem. Soc. Rev. 1991, 20, 167 and references therein.
61. Gregory, K.; Schleyer, P. v. R.; Snaith, R. Adv. Inorg. Chem. 1991, 37, 47 and references therein.
62. Kennedy, A. R.; Mulvey, R. E.; Robertson, A. J. Chem. Soc., Chem. Commun. 1998, 89.
63. Barnett, N. D. R.; Clegg, W.; Horsburgh, L.; Lindsay, D. M.; Liu, Q.-Y.; Mackenzie, F. M.; Mulvey, R. E.; Williard, P. G. J. Chem. Soc., Chem. Commun. 1996, 2321.
64. Kuhn, N.; Henkel, G.; Kreutzberg, J. Angew. Chem., Int. Ed. Engl. 1990, 29, 1143.
65. Kowach, G. R.; Warren, C. J.; Haushalter, R. C.; Disalvo, F. J. Inorg. Chem. 1998, 37, 156.