[R-PLi2(F-R)]2 [R = SiPri2(C6H2Pri 3-2,4,6)] the first structural characterization of a dilithium phosphandiide in the form of a fluorosilane complex

Chemical Communications

Volumn , Issue 3, 1996, Pages 305-306

  Driess, Matthias ^a   Rell, Stefan ^a   Pritzkow, Hans ^a   Janoschek, Rudolf ^b  

^a UNIVERSITY OF HEIDELBERG   (Germany)

^b UNIVERSITY OF GRAZ   (Austria)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0007438301     PISSN: 13597345     EISSN: None     Source Type: Journal    
DOI: 10.1039/CC9960000305     Document Type: Article

References (21)

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2. G. W. Parshall and R. V. Lindsey Jr., J. Am. Chem. Soc., 1959, 81, 6273; G. Fritz, H. Schäfer and W. Holderich. Z. Anorg. Allg. Chem., 1974, 407, 266; R. Appel and K. Geisler, J. Organomet. Chem., 1976, 112, 61; G. Becker, O. Mundt, M. Rössler and E. Schneider. Z. Anorg. Allg. Chem., 1978, 433, 42. G. Becker, B. Eschbach, D. Käshammer and O. Mundt. Z. Anorg. Allg. Chem., 1994, 620, 29 and references therein.
3. G. W. Parshall and R. V. Lindsey Jr., J. Am. Chem. Soc., 1959, 81, 6273; G. Fritz, H. Schäfer and W. Holderich. Z. Anorg. Allg. Chem., 1974, 407, 266; R. Appel and K. Geisler, J. Organomet. Chem., 1976, 112, 61; G. Becker, O. Mundt, M. Rössler and E. Schneider. Z. Anorg. Allg. Chem., 1978, 433, 42. G. Becker, B. Eschbach, D. Käshammer and O. Mundt. Z. Anorg. Allg. Chem., 1994, 620, 29 and references therein.
4. G. W. Parshall and R. V. Lindsey Jr., J. Am. Chem. Soc., 1959, 81, 6273; G. Fritz, H. Schäfer and W. Holderich. Z. Anorg. Allg. Chem., 1974, 407, 266; R. Appel and K. Geisler, J. Organomet. Chem., 1976, 112, 61; G. Becker, O. Mundt, M. Rössler and E. Schneider. Z. Anorg. Allg. Chem., 1978, 433, 42. G. Becker, B. Eschbach, D. Käshammer and O. Mundt. Z. Anorg. Allg. Chem., 1994, 620, 29 and references therein.
5. G. W. Parshall and R. V. Lindsey Jr., J. Am. Chem. Soc., 1959, 81, 6273; G. Fritz, H. Schäfer and W. Holderich. Z. Anorg. Allg. Chem., 1974, 407, 266; R. Appel and K. Geisler, J. Organomet. Chem., 1976, 112, 61; G. Becker, O. Mundt, M. Rössler and E. Schneider. Z. Anorg. Allg. Chem., 1978, 433, 42. G. Becker, B. Eschbach, D. Käshammer and O. Mundt. Z. Anorg. Allg. Chem., 1994, 620, 29 and references therein.
6. G. W. Parshall and R. V. Lindsey Jr., J. Am. Chem. Soc., 1959, 81, 6273; G. Fritz, H. Schäfer and W. Holderich. Z. Anorg. Allg. Chem., 1974, 407, 266; R. Appel and K. Geisler, J. Organomet. Chem., 1976, 112, 61; G. Becker, O. Mundt, M. Rössler and E. Schneider. Z. Anorg. Allg. Chem., 1978, 433, 42. G. Becker, B. Eschbach, D. Käshammer and O. Mundt. Z. Anorg. Allg. Chem., 1994, 620, 29 and references therein.
7. M. Driess, G. Huttner, N. Knopf, H. Pritzkow and L. Zsolnai. Angew. Chem., 1995, 107, 354; Angew. Chem., Int. Ed. Engl., 1995, 35, 316.
8. M. Driess, G. Huttner, N. Knopf, H. Pritzkow and L. Zsolnai. Angew. Chem., 1995, 107, 354; Angew. Chem., Int. Ed. Engl., 1995, 35, 316.
9. D. R. Armstrong, D. Barr, W. Clegg, S. R. Drake, R. J. Singer, R. Snaith, D. Stalke and D. S. Wright, Angew. Chem., 1991, 103, 1702; Angew. Chem., Int. Ed. Engl., 1991, 30, 1707.
10. D. R. Armstrong, D. Barr, W. Clegg, S. R. Drake, R. J. Singer, R. Snaith, D. Stalke and D. S. Wright, Angew. Chem., 1991, 103, 1702; Angew. Chem., Int. Ed. Engl., 1991, 30, 1707.
11. M. J. Frisch, G. W. Trucks, M. Head-Gordon, P. M. W. Gill, M. W. Wong, J. B. Foresman, B. G. Johnson, H. B. Schlegel, M. A. Robb, E. S. Replogle, R. Gomperts, J. L. Andres, K. Raghavachari, J. S. Binkley, C. Gonzales, R. L. Martin, D. J. Fox, D. J. Defrees, J. Baker, J. J. P. Stewart and J. A. Pople, Gaussian 92, Revision C.4. Gaussian, Inc., Pittsburgh, PA, 1992.
12. E. D. Glendening, A. E. Reed, J. E. Carpenter and F. Weinhold, NBO Version 3.1, University of Wisconsin, Madison, 1990.
13. Other compounds with relatively short Li-F distances: D. Stalke and K. H. Whitmire, J. Chem. Soc. Chem. Commun., 1990, 833; D. Stalke, N. Keweloh, U. Klingebiel, M. Noltemeyer and G. M. Sheldrick, Z. Naturforsch., Teil B, 1987, 42, 1237; D. Stalke, U. Klingebiel and G. M. Sheldrick. J. Organomet. Chem., 1988, 344, 37; Lithium (fluorosilyl)phosphanides: R. Boese, D. Blaser, M. Andrianarison and U. Klingebiel. Z. Naturforsch., Teil B, 1989, 44, 265; M. Andrianarison, U. Klingebiel, D. Stalke and G. M. Sheldrick, Phosphorus, Sulfur, Silicon Relat. Elem., 1989, 46, 183; U. Klingebiel, M. Meyer, U. Pieper and D. Stalke. J. Organomet. Chem., 1991, 408, 19; M. Driess, U. Winkler, W. Imhof, L. Zsolnai and G. Huttner. Chem. Ber., 1994, 127, 1031 and references therein.
14. Other compounds with relatively short Li-F distances: D. Stalke and K. H. Whitmire, J. Chem. Soc. Chem. Commun., 1990, 833; D. Stalke, N. Keweloh, U. Klingebiel, M. Noltemeyer and G. M. Sheldrick, Z. Naturforsch., Teil B, 1987, 42, 1237; D. Stalke, U. Klingebiel and G. M. Sheldrick. J. Organomet. Chem., 1988, 344, 37; Lithium (fluorosilyl)phosphanides: R. Boese, D. Blaser, M. Andrianarison and U. Klingebiel. Z. Naturforsch., Teil B, 1989, 44, 265; M. Andrianarison, U. Klingebiel, D. Stalke and G. M. Sheldrick, Phosphorus, Sulfur, Silicon Relat. Elem., 1989, 46, 183; U. Klingebiel, M. Meyer, U. Pieper and D. Stalke. J. Organomet. Chem., 1991, 408, 19; M. Driess, U. Winkler, W. Imhof, L. Zsolnai and G. Huttner. Chem. Ber., 1994, 127, 1031 and references therein.
15. Other compounds with relatively short Li-F distances: D. Stalke and K. H. Whitmire, J. Chem. Soc. Chem. Commun., 1990, 833; D. Stalke, N. Keweloh, U. Klingebiel, M. Noltemeyer and G. M. Sheldrick, Z. Naturforsch., Teil B, 1987, 42, 1237; D. Stalke, U. Klingebiel and G. M. Sheldrick. J. Organomet. Chem., 1988, 344, 37; Lithium (fluorosilyl)phosphanides: R. Boese, D. Blaser, M. Andrianarison and U. Klingebiel. Z. Naturforsch., Teil B, 1989, 44, 265; M. Andrianarison, U. Klingebiel, D. Stalke and G. M. Sheldrick, Phosphorus, Sulfur, Silicon Relat. Elem., 1989, 46, 183; U. Klingebiel, M. Meyer, U. Pieper and D. Stalke. J. Organomet. Chem., 1991, 408, 19; M. Driess, U. Winkler, W. Imhof, L. Zsolnai and G. Huttner. Chem. Ber., 1994, 127, 1031 and references therein.
16. Other compounds with relatively short Li-F distances: D. Stalke and K. H. Whitmire, J. Chem. Soc. Chem. Commun., 1990, 833; D. Stalke, N. Keweloh, U. Klingebiel, M. Noltemeyer and G. M. Sheldrick, Z. Naturforsch., Teil B, 1987, 42, 1237; D. Stalke, U. Klingebiel and G. M. Sheldrick. J. Organomet. Chem., 1988, 344, 37; Lithium (fluorosilyl)phosphanides: R. Boese, D. Blaser, M. Andrianarison and U. Klingebiel. Z. Naturforsch., Teil B, 1989, 44, 265; M. Andrianarison, U. Klingebiel, D. Stalke and G. M. Sheldrick, Phosphorus, Sulfur, Silicon Relat. Elem., 1989, 46, 183; U. Klingebiel, M. Meyer, U. Pieper and D. Stalke. J. Organomet. Chem., 1991, 408, 19; M. Driess, U. Winkler, W. Imhof, L. Zsolnai and G. Huttner. Chem. Ber., 1994, 127, 1031 and references therein.
17. Other compounds with relatively short Li-F distances: D. Stalke and K. H. Whitmire, J. Chem. Soc. Chem. Commun., 1990, 833; D. Stalke, N. Keweloh, U. Klingebiel, M. Noltemeyer and G. M. Sheldrick, Z. Naturforsch., Teil B, 1987, 42, 1237; D. Stalke, U. Klingebiel and G. M. Sheldrick. J. Organomet. Chem., 1988, 344, 37; Lithium (fluorosilyl)phosphanides: R. Boese, D. Blaser, M. Andrianarison and U. Klingebiel. Z. Naturforsch., Teil B, 1989, 44, 265; M. Andrianarison, U. Klingebiel, D. Stalke and G. M. Sheldrick, Phosphorus, Sulfur, Silicon Relat. Elem., 1989, 46, 183; U. Klingebiel, M. Meyer, U. Pieper and D. Stalke. J. Organomet. Chem., 1991, 408, 19; M. Driess, U. Winkler, W. Imhof, L. Zsolnai and G. Huttner. Chem. Ber., 1994, 127, 1031 and references therein.
18. Other compounds with relatively short Li-F distances: D. Stalke and K. H. Whitmire, J. Chem. Soc. Chem. Commun., 1990, 833; D. Stalke, N. Keweloh, U. Klingebiel, M. Noltemeyer and G. M. Sheldrick, Z. Naturforsch., Teil B, 1987, 42, 1237; D. Stalke, U. Klingebiel and G. M. Sheldrick. J. Organomet. Chem., 1988, 344, 37; Lithium (fluorosilyl)phosphanides: R. Boese, D. Blaser, M. Andrianarison and U. Klingebiel. Z. Naturforsch., Teil B, 1989, 44, 265; M. Andrianarison, U. Klingebiel, D. Stalke and G. M. Sheldrick, Phosphorus, Sulfur, Silicon Relat. Elem., 1989, 46, 183; U. Klingebiel, M. Meyer, U. Pieper and D. Stalke. J. Organomet. Chem., 1991, 408, 19; M. Driess, U. Winkler, W. Imhof, L. Zsolnai and G. Huttner. Chem. Ber., 1994, 127, 1031 and references therein.
19. Other compounds with relatively short Li-F distances: D. Stalke and K. H. Whitmire, J. Chem. Soc. Chem. Commun., 1990, 833; D. Stalke, N. Keweloh, U. Klingebiel, M. Noltemeyer and G. M. Sheldrick, Z. Naturforsch., Teil B, 1987, 42, 1237; D. Stalke, U. Klingebiel and G. M. Sheldrick. J. Organomet. Chem., 1988, 344, 37; Lithium (fluorosilyl)phosphanides: R. Boese, D. Blaser, M. Andrianarison and U. Klingebiel. Z. Naturforsch., Teil B, 1989, 44, 265; M. Andrianarison, U. Klingebiel, D. Stalke and G. M. Sheldrick, Phosphorus, Sulfur, Silicon Relat. Elem., 1989, 46, 183; U. Klingebiel, M. Meyer, U. Pieper and D. Stalke. J. Organomet. Chem., 1991, 408, 19; M. Driess, U. Winkler, W. Imhof, L. Zsolnai and G. Huttner. Chem. Ber., 1994, 127, 1031 and references therein.
20. (a) G. M. Sheldrick, SHELXL86, Göttingen, 1986;
21. (b) G. M. Sheldrick, SHELXL93, Göttingen, 1993.