Preparation, properties and reactions of metal-containing heterocycles: Part C: Tetraazatetraphosphadimolybdacyclophanes: Synthesis, isolation, characterization, and X-ray crystal structures

Journal of Organometallic Chemistry

Volumn 595, Issue 2, 2000, Pages 166-177

  Lindner, Ekkehard ^a   Mohr, Markus ^a   Nachtigal, Christiane ^a   Fawzi, Riad ^a   Henkel, Gerald ^b  

^a UNIVERSITY OF TÜBINGEN   (Germany)

^b UNIVERSITY OF DUISBURG ESSEN   (Germany)

Author keywords

Aminophosphines; Dimolybdacyclophanes; High dilution; Macrocyclization; Molybdenum complexes

Indexed keywords

EID: 0001247922     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(99)00587-2     Document Type: Article

References (61)

1. E. Lindner, C. Hermann, G. Baum, D. Fenske, Eur. J. Inorg. Chem. (1999) 679.
2. (a) J.L. Atwood, J.E.D. Davies, D.D. MacNicol, F. Vögtle (Eds.), Comprehensive Supramolecular Chemistry, vol. 2, Pergamon, Oxford, 1996.
3. (b) J.-M. Lehn, Supramolecular Chemistry, VCH, Weinheim, 1995.
4. (c) F. Diederich, Cyclophanes, The Royal Society of Chemistry, Cambridge, 1991.
5. (d) F. Vögtle, Cyclophan-Chemie, Teubner, Stuttgart, 1990.
6. (e) M. Inouye, K. Fujimoto, M. Furusyo, H. Nakazumi, J. Am. Chem. Soc. 121 (1999) 1452.
7. (f) C. Allot, H. Adams, P.L. Bernad, Jr., C.A. Hunter, C. Rotger, J.A. Thomas, Chem. Commun. (Cambridge) (1998) 2449.
8. (g) S.M. Ngola, P.C. Kearney, S. Mecozzi, K. Russell, D.A. Dougherty, J. Am. Chem. Soc. 121 (1999) 1192.
9. (a) C.D. Gutsche, Calixarenes Revisited, The Royal Society of Chemistry, Cambridge, 1998.
10. (b) C.D. Gutsche, Calixarenes, The Royal Society of Chemistry, Cambridge, 1989.
11. (b) A. Ikeda, S. Shinkai, Chem. Rev. 97 (1997) 1713.
12. (a) A. Collet, J.-P. Dutasta, B. Lozach, J. Canceill in: M.J.S. Dewar, J.D. Dunitz, K. Hafner, S. Ito, J.-M. Lehn, K.N. Raymond, C.W. Rees, J. Thiem, F. Vögtle (Eds.), Cyclotriveratrylenes and Cryptophanes: Their Synthesis and Applications to Host-Guest Chemistry and to the Design of New Materials: Topics in Current Chemistry, vol. 165, Springer, Heidelberg, 1993.
13. (b) M. Luhmer, B.M. Goodson, Y.-Q. Song, D.L. Laws, L. Kaiser, M.C. Cyrier, A. Pines, J. Am. Chem. Soc. 121 (1999) 3502.
14. (a) D.J. Cram, J.M. Cram, Container Molecules and Their Guests, The Royal Society of Chemistry, Cambridge, 1994.
15. (b) A. Jasat, J.C. Sherman, Chem. Rev. 99 (1999) 931.
16. (a) B. Olenyuk, A. Fechtenkötter, P.J. Stang, J. Chem. Soc. Dalton Trans. (1998) 1707.
17. (b) M. Fujita, D. Oguro, M. Miyazawa, H. Oka, K. Yamaguchi, K. Ogura, Nature 378 (1995) 469.
18. (c) P.N.W. Baxter, J.-M. Lehn, G. Baum, D. Fenske, Chem. Eur. J. 5 (1999) 103.
19. (d) P.N.W. Baxter, J.-M. Lehn, B.O. Kneisel, G. Baum, D. Fenske, Chem. Eur. J. 5 (1999) 113.
20. (a) I.A. Bagatin, D. Matt, H. Thönnessen, P.G. Jones, Inorg. Chem. 38 (1999) 1585.
21. (b) P. Molenveld, J.F.J. Engbersen, H. Kooijman, A.L. Spek, D.N. Reinhoudt, J. Am. Chem. Soc. 120 (1998) 6726.
22. (c) H.K.A.C. Coolen, J.A.M. Meeuwis, P.W.N.M. van Leeuwen, R.J.M. Nolte, J. Am. Chem. Soc. 117 (1995) 11906.
23. (a) E. Lindner, I. Krebs, R. Fawzi, M. Steimann, Organometallics 18 (1999) 480.
24. (b) F.S. McQuillan, C.J. Jones, Polyhedron 15 (1996) 1533.
25. (a) J. Vaugeois, M. Simard, J.D. Wuest, Organometallics 17 (1998) 1215.
26. (b) M.T. Reetz, C.M. Niemeyer, M. Hermes, R. Goddard, Angew. Chem. 104 (1992) 1054; Angew. Chem. Int. Ed. Engl. 31 (1992) 1017.
27. (b) M.T. Reetz, C.M. Niemeyer, M. Hermes, R. Goddard, Angew. Chem. 104 (1992) 1054; Angew. Chem. Int. Ed. Engl. 31 (1992) 1017.
28. Slone R.V., Yoon D.I., Calhoun R.M., Hupp J.T. J. Am. Chem. Soc. 117:1995;11813.
29. Inoue M.B., Velazquez E.F., Medrano F., Ochoa K.L., Galvez J.C., Inoue M., Fernando Q. Inorg. Chem. 37:1998;4070.
30. Jones C.J. Chem. Soc. Rev. 27:1998;289.
31. (a) J.R. Farrell, C.A. Mirkin, I.A. Guzei, L.M. Liable-Sands, A.L. Rheingold, Angew. Chem. 110 (1998) 484; Angew. Chem. Int. Ed. Engl. 37 (1998) 465.
32. (a) J.R. Farrell, C.A. Mirkin, I.A. Guzei, L.M. Liable-Sands, A.L. Rheingold, Angew. Chem. 110 (1998) 484; Angew. Chem. Int. Ed. Engl. 37 (1998) 465.
33. (b) K. Fujimoto, S. Shinkai, Tetrahedron Lett. 35 (1994) 2915.
34. (a) E. Lindner, M.W. Pitsch, R. Fawzi, M. Steimann, Chem. Ber. 129 (1996) 639.
35. (b) E. Lindner, W. Wassing, R. Fawzi, M. Steimann, Angew. Chem. 106 (1994) 363; Angew. Chem. Int. Ed. Engl. 33 (1994) 321.
36. (b) E. Lindner, W. Wassing, R. Fawzi, M. Steimann, Angew. Chem. 106 (1994) 363; Angew. Chem. Int. Ed. Engl. 33 (1994) 321.
37. (c) E. Lindner, W. Wassing, M.W. Pitsch, R. Fawzi, M. Steimann, Inorg. Chim. Acta 220 (1994) 107.
38. Lindner E., Günther M.F., Mayer H.A., Fawzi R., Steimann M. Chem. Ber. Recueil. 130:1997;1815.
39. (a) H. Adams, F.J. Carver, C.A. Hunter, N.J. Osborne, Chem. Commun. (Cambridge) (1996) 2529.
40. (b) F.S. McQuillan, H. Chen, T.A. Hamor, C.J. Jones, H.A. Jones, R.P. Sidebotham, Inorg. Chem. 38 (1999) 1555.
41. (c) M. Fujita, S. Nagao, M. Iida, K. Ogata, K. Ogura, J. Am. Chem. Soc. 115 (1993) 1574.
42. T.Q. Ly, A.M.Z. Slawin, J.D. Woollins, J. Chem. Soc. Dalton Trans. (1997) 1611.
43. Tarassoli A., Haltiwanger R.C., Norman A.D. Inorg. Chem. 21:1982;2684.
44. (a) J. Barluenga, A.M. Bayón, P. Campos, G. Asensio, E. Gonzalez-Nuñez, Y. Molina, J. Chem. Soc. Perkin Trans. I (1988) 1631.
45. (b) J. Barluenga, P.J. Campos, G. Canal, G. Asensio, Synlett (1990) 261.
46. (a) L. Rossa, F. Vögtle in: F. Vögtle (Ed.), Synthesis of Medio- and Macrocyclic Compounds by High Dilution Principle Techniques: Topics in Current Chemistry, vol. 113, Cyclophanes I, Springer, Heidelberg, 1983.
47. (b) P. Knops, N. Sendhoff, H.-B. Mekelburger, F. Vögtle in: E. Weber, F. Vögtle (Eds.), High Dilution Reactions - New Synthetic Applications: Topics in Current Chemistry, vol. 161, Macrocycles, Springer, Heidelberg, 1992.
48. S. Karbach, W. Löhr, F. Vögtle, J. Chem. Res. (S) (1981) 314; J. Chem. Res. (M) (1981) 3579.
49. S. Karbach, W. Löhr, F. Vögtle, J. Chem. Res. (S) (1981) 314; J. Chem. Res. (M) (1981) 3579.
50. Kayran C., Kozanoglu F., Özkar S., Saldamli S., Tekkaya A., Kreiter C.G. Inorg. Chim. Acta. 284:1999;229.
51. Berger S., Braun S., Kalinowski H.-O. NMR-Spektroskopie von Nichtmetallen. 1993;Georg Thieme Verlag, Stuttgart.
52. Pohl D., Ellermann J., Knoch F.A., Moll M., Bauer W. J. Organomet. Chem. 481:1994;259.
53. Jackson S.A., Eisenstein O., Martin J.D., Albeniz A.C., Crabtree R.H. Organometallics. 10:1991;3062.
54. (a) D.J. David, Analyst 86 (1961) 730.
55. (b) T.V. Ramakrishna, P.W. West, J.W. Robinson, Anal. Chim. Acta 44 (1969) 437.
56. (c) G.D. Kirkbright, A.M. Smith, T.S. West, Analyst 91 (1966) 700.
57. Tekkaya A., Kayran C., Özkar S., Kreiter C.G. Inorg. Chem. 33:1994;2439.
58. A. Talamona, E. Stump, Präparative Mitteldruck-Flüssigchromatographie (MPLC); Teil 1: Die Adsorptions-Chromatographie, Büchi Laboratoriums-Technik GmbH, Göppingen, Germany.
59. Harris R.K. Can. J. Chem. 42:1964;2275.
60. Sheldrick G.M. Acta Crystallogr. Sect. A. 51:1995;33.
61. G.M. Sheldrick, SHELXTL V5.03, Program for Crystal Structure Refinement, University of Göttingen, Germany, 1997.