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7
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0001758253
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15
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0347716924
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Aryldiazoacetates and vinyldiazoacetates have been used as carbenoid precursors in asymmetric intermolecular C-H insertions. Other diazo compounds that generate chemoselective donor/acceptor substituted carbenoids are alkynyldiazoacetates and heteroaryldiazoacetates. For a general review, see: Davies, H. M. L.: Antoulinakis, E. G. J. Organomet. Chem. 2001, 617-618, 47
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(a) Davies, H. M. L.; Antoulinakis, E. G.; Hansen, T. Org. Lett. 1999, 1, 383.
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(a) Davies, H. M. L.; Hansen, T.; Hopper, D.; Panaro, S. A. J. Am. Chem. Soc. 1999, 121, 6509.
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21
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0000217402
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Trost, B. M., Ed.; Pergamon Press: Oxford
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For a review, see: (a) Wipf, P. In Comprehensive Organic Synthesis; Trost, B. M., Ed.; Pergamon Press: Oxford, 1991; Vol. 5, pp 827-874.
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Wipf, P.1
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0033553990
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(b) Axten, J. M.; Ivy; R.; Krim, L.; Winkler, J. D. J. Am. Chem. Soc. 1999, 121, 6511.
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(b) Davies, H. M. L.; Hansen, T.; Churchill, M. R. J. Am. Chem. Soc. 2000, 122, 3063.
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(a) Davies, H. M. L.; Stafford, D. G.; Hansen, T. Org. Lett. 1999, 1, 233.
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(b) Davies, H. M. L.; Stafford, D. G.; Hansen, T.; Churchill, M. R.; Keil, K. M. Tetrahedron Lett. 2000, 41, 2035.
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Davies, H. M. L.; Bruzinski, P. R.; Lake, D. H.; Kong, N.; Fall, M. J. J. Am. Chem. Soc. 1996, 118, 6897.
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Fall, M.J.5
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31
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0042728146
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The absolute configuration of 4 was determined to be (R) by comparison to a known sample (see ref 12b). The absolute configuration of the other C-H insertion products is assigned by analogy.
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The absolute configuration of 4 was determined to be (R) by comparison to a known sample (see ref 12b). The absolute configuration of the other C-H insertion products is assigned by analogy.
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32
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0035971991
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Relative stereochemistry is readily achived on the basis of distinctive chemical shifts in the proton NMR. For details, see: Davies, H. M. L.; Ren, P. Tetrahedron Lett. 2001, 42, 3149.
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Davies, H.M.L.1
Ren, P.2
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33
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0042227251
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note
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The determination of the relative and absolute stereochemistry for 16 and 17 is described in detail in Supporting Information.
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