Template Synthesis of One-Dimensional Au, Au-Poly(pyrrole), and Poly(pyrrole) Nanoparticle Arrays

Chemistry of Materials

Volumn 10, Issue 5, 1998, Pages 1214-1219

  Marinakos, Stella M ^a   Brousseau III, Louis C ^a   Jones, Angela ^a   Feldheim, Daniel L ^a  

^a NORTH CAROLINA STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000726187     PISSN: 08974756     EISSN: None     Source Type: Journal    
DOI: 10.1021/cm980059t     Document Type: Article

References (39)

1. (a) Murray, C. B.; Kagan, C. R.; Bawendi, M. G. Science 1995, 270, 1335.
2. (b) Kagan, C. R.; Murray, C. B.; Nirmal, M.; Bawendi, M. G. Phys. Rev. Lett. 1996, 76, 1517.
3. (a) Mirkin, C. A.; Letsinger, R. L.; Mucic, R. C.; Storhoff, J. J. Nature 1996, 382, 607.
4. (b) Emory, S. R.; Nie, S. Science 1997, 275, 1102.
5. (a) Freeman, R. G.; Grabar, K. C.; Allison, K. J.; Bright, R. M.; Davis, J. A.; Guthrie, A. P.; Hommer, M. B.; Jackson, M. A.; Smith, P. C.; Walter, D. G.; Natan, M. J. Science 1995, 267, 1629.
6. (b) Grabar, K. C.; Smith, P. C.; Musick, M. D.; Davis, J. A.; Walter, D. G.; Jackson, M. A.; Guthrie, A. P.; Natan, M. J. J. Am. Chem. Soc. 1996, 118, 1148.
7. Hostetler, M. J.; Green, S. J.; Stokes, J. J.; Murray, R. W. J. Am. Chem. Soc. 1996, 118, 4212.
8. (a) Chumanov, G.; Sokolov, K.; Gregory, B.; Cotton, T. M. J. Phys. Chem. 1995, 99, 9466.
9. (b) Feilchenfeld, H.; Chumanov, G.; Cotton, T. M. J. Phys. Chem. 1996, 100, 4937.
10. Andres, R. P.; Bein, T.; Dorogi, M.; Feng, S.; Henderson, J. I.; Kubiak, C. P.; Mahoney, W.; Osifchin, R. G.; Reifenberger, R. Science 1996, 272, 1323.
11. Alvarez, M. M.; Khoury, J. T.; Schaaff, T. G.; Shafigullin, M. N.; Vezmar, I.; Whetten, R. L. J. Phys. Chem. B 1997, 101, 3706.
12. (a) Feldheim, D. L.; Keating, C. D. Chem. Soc. Rev. 1998, 27, 1.
13. (b) Doron, A.; Katz, E.; Willner, I. Langmuir 1995, 11, 1313.
14. Tian, Y.; Fendler, J. H. Chem. Mater. 1996, 8, 969.
15. Peschel, S.; Schmid, G. Angew. Chem., Int. Ed. Engl. 1995, 34, 1442.
16. (e) Colvin, V. L.; Goldstein, A. N.; Alivisatos, A. P. J. Am. Chem. Soc. 1992, 114, 5221.
17. (f) Hostetler, M. J.; Wingate, J. E.; Zhong, C.-J.; Harris, J. E.; Vachet, R. W.; Clark, M. R.; Londono, J. D.; Green, S. J.; Stokes, J. J.; Wignall, G. D.; Glish, G. L.; Porter, M. D.; Evans, N. D.; Murray, R. W. Langmuir 1998, 14, 17.
18. (g) Collier, C. D.; Saykally, R. J.; Shiang, J. J.; Henrichs, S. E.; Heath, J. R. Science 1997, 277, 1978.
19. (h) Chemseddine, A.; Jungblut, H.; Boulmaaz, S. J. Phys. Chem. 1996, 100, 12546.
20. Brust, M.; Walker, M.; Bethell, D.; Schiffrin, D. J.; Whyman, R. J. Chem. Soc., Chem. Commun. 1994, 801.
21. (a) Averin, D. V.; Likharev, K. K. Single Electronics: A Correlated Transfer of Single Electrons and Cooper Pairs in Systems of Small Tunnel Junctions In Mesoscopic Phenomena in Solids; Altshuler, B. L., Lee, P. A., Webb, R. A., Eds.; Elsevier Science Publishers: New York, 1991, Vol. 30. p 173.
22. (b) Mullen, K., Ben-Jacob, E., Jaklevic, R. C., Schuss, Z. Phys. Rev. B 1988, 37 (1), 98.
23. Single Charge Tunneling; Grabert, H., Devoret, M. H., Eds.; Plenum Press: New York, 1992.
24. Mann, S. J. Chem. Soc., Dalton Trans. 1993, 1.
25. (a) Alivisatos, A. P.; Johnsson, K. P.; Peng, X.; Wilson, T. E.; Loweth, C. J.; Bruchez, M. P.; Jr.; Schultz, P. G. Nature 1996, 382, 609.
26. (b) Peng, X.; Wilson, T. E.; Alivisatos, A. P.; Schultz, P. G. Angew. Chem., Int. Ed. Engl. 1997, 36 (1/2), 145.
27. Hornyak, G. L.; Kroll, M.; Pugin, R.; Sawitowski, T.; Schmid, G.; Bovin, J.-O.; Karsson, G.; Hofmeister, H.; Hopfe, S. Chem. Eur. J. 1997, 3, 1951.
28. Diaz, A. F.; Bargon, J. Handbook of Conducting Polymers; Marcel Dekker: New York, 1986; Vol. 1.
29. (a) Liang, W.; Martin, C. R. Chem. Mater. 1991, 3, 390.
30. (b) Brumlik, C. J.; Menon, V. P.; Martin, C. R. J. Mater. Res. 1994, 9 (5), 1174.
31. 3 channels is currently not clear. Possibilities include chemical interactions between Au and the membrane, physical entrapment in the tortuous channel system which exists on the barrier side of the membrane (the 20 nm diameter side), or simply that the solution containing particles remains in the pores after filtration due to capillary forces. TEM images show that a high density of particles were trapped in the large-diameter regions of the membrane, suggesting that the entire pore was filled with particles. This supports the latter mechanism.
32. 3 membrane for background subtraction.
33. Bohren, C. T.; Huffman, D. R. Absorption and Scattering of Light by Small Particles; Wiley: New York, 1983.
34. 2,3,12 This variation is likely a result of subtle differences in size and shape between colloids prepared in different laboratories and differing states of particle agglomeration. Colloidal Au particles synthesized in our laboratory absorb at 526 nm in aqueous solution. Thus we cannot discount the possibility that Au particle dimers and trimers are present in solution which are then oriented along the pore axis due to shear forces or interactions with pore walls during vacuum entrapment. However, TEM images of an aqueous solution of colloids showed mostly individual particles.
35. (b) Al-Rawashdeh, N. A. F.; Sandrock, M. L.; Seugling, C. J.; Foss, C. A., Jr. J. Phys. Chem. 1998, 102, 361.
36. Foss, C. A., Jr.; Hornyak, G. L.; Stockert, J. A.; Martin, C. R. J. Phys. Chem. 1994, 98, 1963.
37. Marinakos, S.; Brousseau, L. C., III; Novak, J. P.; Feldheim, D. L. (submitted for publication).
38. Polycarbonate membranes were treated with glacial acetic acid for 12 h prior to use to remove the polyvinylpyrolidone wetting agent.
39. Zeman, E. J.; Schatz, G. C. J. Phys. Chem. 1987, 91, 634.