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1H NMR resonances in the δ = 0-40 ppm region indicates that the nickel complexes 1-6 are paramagnetic in solution. For complexes 2 and 5 this is further supported by temperature-dependent magnetic susceptibility measurements. [45] We anticipate performing a more detailed study of the electronic structures of the other compounds by temperature-dependent susceptibility measurements.
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For a complete listing of these IR absorptions see: Exp. Sect., complex 2.
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