Porphyrin supermolecules: Synthesis and self-assembly features of zinc-5-(3′-pyridyl)-10,15,20-tris(4′-hydroxyphenyl)porphyrin

Inorganic Chemistry

Volumn 43, Issue 24, 2004, Pages 7582-7584

  Vinodu, Mikki ^a   Stein, Zafra ^a   Goldberg, Israel ^a  

^a TEL AVIV UNIVERSITY   (Israel)

Author keywords

[No Author keywords available]

Indexed keywords

PORPHYRIN DERIVATIVE; UNCLASSIFIED DRUG; ZINC 5 (3' PYRIDYL) 10,15,20 TRIS(4' HYDROXYPHENYL)PORPHYRIN;

ARTICLE; CHEMICAL BOND; CHEMICAL MODIFICATION; CHEMICAL REACTION KINETICS; CHEMICAL STRUCTURE; SUPRAMOLECULAR CHEMISTRY; X RAY DIFFRACTION;

CRYSTALLOGRAPHY, X-RAY; METALLOPORPHYRINS; MODELS, MOLECULAR; MOLECULAR CONFORMATION; MOLECULAR STRUCTURE; SPECTROMETRY, MASS, MATRIX-ASSISTED LASER DESORPTION-IONIZATION; ZINC;

EID: 9444254072     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic049374+     Document Type: Article

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16. While this work was in progress, similarly structured porphyrin tetramers were reported: (a) Balaban, T. S.; Goddard, R.; Linke-Schaetzel, M.; Lehn, J.-M. J. Am. Chem. Soc. 2003, 125, 4233-4239. (b) Tsuda, A.; Sakamoto, S.; Yamaguchi, K.; Aida, T. J. Am. Chem. Soc. 2003, 125, 15722-15723.
17. While this work was in progress, similarly structured porphyrin tetramers were reported: (a) Balaban, T. S.; Goddard, R.; Linke-Schaetzel, M.; Lehn, J.-M. J. Am. Chem. Soc. 2003, 125, 4233-4239. (b) Tsuda, A.; Sakamoto, S.; Yamaguchi, K.; Aida, T. J. Am. Chem. Soc. 2003, 125, 15722-15723.
18. 3Zn). MS(MALDI): 727.1, 1453.2, 2176.3, and 2909.2, peaks that correspond to mono-, di-, tri-, and tetrameric porphyrin clusters, respectively.
19. The low yields of the free-base porphyrin and 2 did not afford enough material for a reliable elemental analysis. A powder diffraction pattern from a bulk sample of 2 compared reasonably well with that calculated from the single-crystal structure, but its complexity (due to the very large unit cell) prevented an accurate analysis.
20. 3, Z = 4].
21. 3, Z = 4].
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