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The % ee of 3e was determined by reaction of the oxidized product and a chiral shift reagent tris(3-trifluoromethylhydroxymethylene-d-camphorate) europium. See: McCreary, M. D.; Lewis, D. W.; Wernick, D. L.; Whitesides, G. M. J. Am. Chem. Soc. 1974, 96, 1038-1054.
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23
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8844253177
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note
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(a) See Supporting Information,
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24
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8844253350
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note
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(b) Absolute configurations were determined by X-ray crystallographic analysis of adducts derived from 3 and an enantiopure Pd complex of known absolute configuration. Note that the sense of chiral induction is the same in both reactions, although the descriptor of the absolute configuration of the major enantiomers changes from R (hydroamination) to S (hydrophosphination) due to different priority sequences of the substituents at the respective stereogenic center.
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