Thermal analysis of soil minerals

Methods of Soil Analysis, Part 5: Mineralogical Methods

Volumn 5, Issue , 2015, Pages 117-160

  Karathanasis, A D ^a  

^a UNIVERSITY OF KENTUCKY   (United States)

Author keywords

Combined thermal analysis techniques; Differential scanning calorimetry; Differential thermal analysis; Qualitative interpretations; Quantitative interpretations; Soil mineral studies; Thermogravimetry

Indexed keywords

EID: 85102876461     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.2136/sssabookser5.5.c5     Document Type: Chapter

References (105)

1. Acemana, S., N. Lahav, and S. Yariv. 1999. A thermo-FTIR-spectroscopy analysis of Al-pillared smectites differing in source of charge, in KBr disks. Thermochim. Acta 340:349-366.
2. Anderson, H., W. Besch, and D. Haberland. 1977. Investigation about methods of quantitative evaluation of DTA curves. J. Therm. Anal. 12:59-68.
3. Arazi, S.C., and T.G. Krenkel. 1970. Dehydroxylation heat of alunite. Am. Mineral. 55:1329-1337.
4. Asomoza, P.M., M.L. Razo, T.L. Chaidez, and S.R. Cassillas. 1978. Quantitative evaluation of N2CO3 and NaCl content of the clays of the ex-lake of Texcoco (Valley of Mexico) by means of thermogravimetry. J. Therm. Anal. 13:327-339.
5. Barnhisel, R.I., and P.M. Bertsch. 1989. Chlorites and hydroxyinterlayered vermiculite and smectite. p. 729-788. In J.B. Dixon and S.B. Weed (ed.) Minerals in soil environments. 2nd ed. SSSA Book Ser. 1. SSSA, Madison, WI.
6. Barshad, I. 1952. Temperature and heat of reaction calibration of the DTA apparatus. Am. Mineral. 37:667-694.
7. Bartenfelder, D.C., and A.D. Karathanasis. 1989. A differential scanning calorimetry evaluation of quartz status in geogenic and pedogenic environments. Soil Sci. Soc. Am. J. 53:961-967.
8. Barwood, H.L., and B.F. Hajek. 1979. Differential thermal characteristics of soil and reference quartz. Soil Sci. Soc. Am. J. 43:626-627.
9. Beck, J. 2003. Qualitative and quantitative analysis of highly weathered clays. Ph.D. diss. Auburn University, AL.
10. Bish, D.L., and C.J. Duffy. 1990. Thermogravimetric analysis of minerals. p. 96-157. In J. W. Stucki et al. (ed.) Thermal analysis in clay science. Clay Minerals Society, Boulder, CO.
11. Boss, B.D. 1967. DTA of biotitic vermiculite to determine vermiculite content. Am. Mineral. 52:293298.
12. Bracewell, J.M., and G.W. Robertson. 1980. Pyrolysis-mass spectrometry studies of humification in a peat and a peaty podzol. J. Anal. Appl. Pyrolysis 2:53-62.
13. Brindley, G.W., and J. Lemaitre. 1987. Thermal, oxidation, and reduction reactions of clay minerals. p. 319-370. In A.C.D. Newman (ed.) Chemistry of clays and clay minerals. Monogr. 6. Mineralogical Society, London.
14. Brown, M.E. 1998. Handbook of thermal analysis and calorimetry. Vol. 1. Principles and practice. Elsevier, Amsterdam.
15. Brown, M.E. 2001. Introduction to thermal analysis. Kluwer Academic Publishers, Dordrecht, The Netherlands.
16. Carleer, R., G. Reggers, M. Ruysen, and J. Mullens. 1998. TG-MS analysis as a tool for the evaluation of clay mixtures. Thermochim. Acta 323:169-178.
17. Charsley, E.L., and S.B. Warrington (ed.) 1992. Thermal analysis: Techniques and applications. Royal Society of Chemistry, Cambridge, UK.
18. Churchman, G.J., J.S. Whitton, G.G.C. Claridge, and B.K.G. Theng. 1984. Intercalation method using formamide for differentiating halloysite from kaolinite. Clays Clay Miner. 32:241-248.
19. Davis, C.E., and D.A. Holdridge. 1969. Quantitative estimation of clay minerals by DTA. Clay Miner. 8:193-200.
20. Dixon, J.B. 1966. Quantitative analysis of kaolinite and gibbsite in soils by DTA and selective dissolution methods. Clays Clay Miner. 14:83-89.
21. Drits, V.A. 2003. Structural and chemical heterogeneity of layer silicates and clay minerals. Clay Miner. 38:403-432.
22. Dubrawski, J.V. 1987. The effect of particle size on the determination of quartz by DSC. Thermochim. Acta 120:257-260.
23. Dubrawski, J.V., and S.S.J. Warne. 1988. Differential scanning calorimetry of the dolomite-ankerite mineral series in variable atmospheres. Thermochim. Acta 135:225-230.
24. Dunn, J.G. 1997. The oxidation of sulfide minerals. Thermochim. Acta 300:127-139.
25. Dunn, J.G. 1998. Applications of thermal methods of analysis to raw and processed minerals. Thermochim. Acta 324:59-66.
26. Dunn, J.G., B.T. Sturman, and W. Van Bronswijk. 1980. The determination of gypsum and lime in small samples of set plaster by a DSC-computer method. Thermochim. Acta 37:337-341.
27. Dyer, A. 1981. 1981. Thermomechanical analysis of zeolites. Anal. Proc. (October):447-450.
28. Earnest, C.M. 1984. Thermal analysis of clays, minerals, and coals. Perkin-Elmer, Norwalk.
29. Earnest, C.M. (ed.) 1988. Compositional analysis by thermogravimetry. ASTM, Philadelphia, PA.
30. El-Akkad, T.M., N.S. Flex, N.M. Guindy, S.R. El-Massry, and S. Nashed. 1982. Thermal analyses of monoand divalent montmorillonite cationic derivatives. Thermochim. Acta 59:9-17.
31. El-Barawy, K.A., B.S. Girgis, and N.S. Felix. 1986. Thermal treatment of some pure smectites. Thermochim. Acta 98:181-189.
32. Ford, R.G., and P.M. Bertsch. 1999. Distinguishing between surface and bulk dehydration-dehydroxylation reactions in synthetic goethites by high-resolution thermogravimetric analysis. Clays Clay Miner. 47:329-337.
33. Frost, R.L., and Z. Ding. 2003. Controlled rate thermal analysis and differential scanning calorimetry of sepiolites and palygorskites. Thermochim. Acta 397:119-128.
34. Frost, R.L., D.L. Wain, R.A. Wills, A. Musemeci, and W. Martens. 2006. A thermogravimetric study of the alunites of sodium, potassium, and ammonium. Thermochim. Acta 443:56-61.
35. Frost, R.L., M.L. Weier, and W. Martens. 2005. Thermal decomposition of jarosites of potassium, sodium, and lead. J. Therm. Anal. Calorim. 82:115-118.
36. Gallagher, P.K., and D.W. Johnson. 1973. The effects of sample size and heating rate on the kinetics of the thermal decomposition of CaCO3. Thermochim. Acta 6:67-83.
37. Haines, P.J. 1995. Thermal methods of analysis: Principles, applications, and problems. Blackie Academic and Professional, London.
38. Haines, P.J., M. Reading, and F.W. Wilburn. 1998. Differential thermal analysis and differential thermal calorimetry. p. 279-361. In M.E. Brown (ed.) Handbook of thermal analysis and calorimetry. Elsevier, New York.
39. Hajek, B.F. 1979. COLE determination by thermomechanical analysis. Soil Sci. Soc. Am. J. 43:427-428.
40. Hatakeyama, T., and Z. Liu. 1998. Handbook of thermal analysis. John Wiley and Sons, New York.
41. Heidbrink, J.L., J. Li, W.P. Pan, J.L. Gooding, S. Aubuchon, J. Foreman, and C.J. Lundgren. 1996. Distinction of nontronite from palagonite by thermal analysis and evolved-gas analysis: Application to Mars surface exploration. Thermochim. Acta 284:241-251.
42. Jackson, M.L. 1975. Soil chemical analysis-advanced course. 2nd ed. M.L. Jackson, Madison, WI.
43. Jorgensen, S.S., A.C. Birnie, B.F.L. Smith, and B.D. Mitchell. 1970. Assessment of gibbsitic material in soil clays by DTA and alkali dissolution methods. J. Therm. Anal. 2:227-282.
44. Kaiserberger, E. (ed.) 1997. Coupling thermal analysis and gas analysis methods. Thermochim. Acta 295:1-186.
45. Karathanasis, A.D., F. Adams, and B.F. Hajek. 1983. Stability relationships in kaolinite, gibbsite, and Al-hydroxyinterlayered vermiculite soil systems. Soil Sci. Soc. Am. J. 47:1247-1251.
46. Karathanasis, A.D., and V. P Evangelou. 1986. Water sorption characteristics of Aland Ca-saturated clays. Soil Sci. Soc. Am. J. 50:1063-1068.
47. Karathanasis, A.D., and V.P. Evangelou. 1987. Low temperature dehydration kinetics of Aland Casaturated clays. Soil Sci. Soc. Am. J. 51:1072-1078.
48. Karathanasis, A.D., and B.F. Hajek. 1982a. Revised methods for rapid quantitative determination of minerals in soil clays. Soil Sci. Soc. Am. J. 46:419-425.
49. Karathanasis, A.D., and B.F. Hajek. 1982b. Quantitative evaluation of water adsorption of soil clays. Soil Sci. Soc. Am. J. 46:1321-1325.
50. Karathanasis, A.D., and B.F. Hajek. 1985. Shrink-swell potential of montmorillonitic soils in udic moisture regimes. Soil Sci. Soc. Am. J. 49:159-166.
51. Karathanasis, A.D., and W.G. Harris. 1994. Quantitative thermal analysis of soil materials. p. 360-411. In J.E. Amonette and L.W. Zelazny (ed.) Quantitative methods in soil mineralogy. SSSA, Madison, WI.
52. Karathanasis, A.D., G.W. Hurt, and B.F. Hajek. 1986. Properties and classification of montmorilloniterich Hapludults in the Alabama Coastal Plain. Soil Sci. 142:1247-1251.
53. Kerr, P.F., and J.L. Kulp. 1948. Multiple differential thermal analysis. Am. Mineral. 33:387-419.
54. Kettrup, A., G. Matuschek, H. Utschick, C. Namendirf, and G. Brauer. 1997. A macro STA-system for environmental samples. Thermochim. Acta 295:119-131.
55. Kloprogge, J.T., R.L. Frost, and L. Hickey. 2000. Infrared emission spectroscopic study of the dehydroxylation of some hectorites. Thermochim. Acta 345:145-156.
56. Koel, M., M. Kudrjasova, K. Tonsuaadu, M. Peld, and M. Veiderma. 1998. Evolved gas analysis of apatite materials using thermochromatography. Thermochim. Acta 322:25-32.
57. Lodding, W., and L. Hammell. 1960. Differential thermal analysis of hydroxides in reducing atmosphere. Anal. Chem. 32:657-662.
58. Mackenzie, R.C. 1970. Differential thermal analysis. Academic Press, London.
59. Mackenzie, R.C., and S. Calliere. 1975. The thermal characteristics of soil minerals and the use of these characteristics in the qualitative and quantitative determination of clay minerals in soils. p. 529-571. In J.E. Gieseking (ed.) Soil components. Vol. II. Elsevier, New York.
60. Mackenzie, R.C. 1981. Thermoanalytical methods in clay studies. p. 5-29. In J.J. Fripiat (ed.) Advanced techniques for clay mineral analysis. Elsevier, Amsterdam, The Netherlands.
61. McKeever, S.W.S. 1988. Thermoluminescence of solids. Cambridge Univ. Press, London.
62. Minato, H. 1988. Dehydration energy of halloysite by means of DSC methods with the relationships of its mineralogy and modes of occurrence. Thermochim. Acta 135:279-283.
63. Morgan, D.J. 1977. Simultaneous DTA-EGA of minerals and natural mineral mixtures. J. Therm. Anal. 12:245-263.
64. Morgan, D.J., S.B. Warrington, and S.J. Warne. 1988. Earth sciences applications of evolved gas analysis: A review. Thermochim. Acta 135:259-266.
65. Mullens, J. 1998. EGA-evolved gas analysis. p. 509-546. In M.E. Brown (ed.) Handbook of thermal analysis and calorimetry. Elsevier, New York.
66. Nathan, Y, G. Panzer, and S. Gross. 1988. The thermal analysis of some phosphate minerals: Strengite, lipscombite, cyrilorite, and goyazite. Thermochim. Acta 135:259-266.
67. Ovadyahu, D., S. Shoval, I. Lapides, and S. Yariv. 1996. Thermo-IR-spectroscopy study of the mechanochemical adsorption of 3,5-dichlorophenol by TOT swelling clay minerals. Thermochim. Acta 282:369-383.
68. Paulik, F. 1995. Special trends in thermal analysis. Wiley, Chichester, UK.
69. Paulik, F., and J. Paulik. 1978. Simultaneous techniques in thermal analysis. Analyst 103:417-437.
70. Paulik, J., F. Paulik, and M. Arnold. 1982. Simultaneous TG, DTG, DTA, and EG techniques for the determination of carbonate, sulfate, pyrite, and organic material in minerals, soils, and rocks. J. Therm. Anal. 25:327-340.
71. Pelovski, Y. 2000. Thermal analysis for control of the properties of mineral fertilizers. J. Therm. Anal. Calorim. 60:53-58.
72. Post, J.L., B.L. Cupp, and F.T. Madsen. 1997. Beidellite and associated clays from the Delamar Mine and Florida Mountain area, Idaho. Clays Clay Miner. 45:240-250.
73. Reading, M. 1998. Controlled rate thermal analysis and related techniques. p. 423-443. In M.E. Brown (ed.) Handbook of thermal analysis and calorimetry. Elsevier, New York.
74. Remmler, M., and F.D. Kopinke. 1995. Thermoanalytical methods for characterizing hydrocarbonsludge soil mixtures. Thermochim. Acta 263:101-122.
75. Sadek, O.M., and W.K. Mekhamer. 2000. Ca-montmorillonite clay as thermal energy storage material. Thermochim. Acta 363:47-54.
76. Schilling, M.R. 1990. Effects of sample size and packing in the thermogravimetric analysis of Camontmorillonite STx-1. Clays Clay Miner. 38:556-558.
77. Schnitzer, M., and H. Kodama. 1972. Differential thermal analysis of metal-fulvic acid salts and complexes. Geoderma 7:93-103.
78. Schomburg, J., and M. Storr. 1984. Dilatometerkurvenatlas der tonmineralrohstoffe, Akademie-Verlag, Berlin.
79. Schwertmann, U. 1984. The double dehydroxylation peak of goethite. Thermochim. Acta 78:39-46.
80. Shang, C., and L.W. Zelazny. 2008. Selective dissolution techniques for mineral analysis of soils and sediments. p. 33-80. In A.L. Ulery and L.R. Drees (ed.) Methods of soil analysis. Part 5. Mineralogical methods. SSSA Book Ser. 5. SSSA, Madison, WI.
81. Sharp, J.H., and S.A. Wentworth. 1969. Kinetic analysis of thermogravimetric data. Anal. Chem. 41:2060-2062.
82. Smalley, I.J., and G.S. Xidakis. 1979. Thermogravimetry of an expansive clay soil from Adelaide: Approximate mineralogical analysis using standard montmorillonite. Clay Sci. 5:189-193.
83. Smykatz-Kloss, W. 1974. Differential thermal analysis: Applications and results in mineralogy. Springer-Verlag, New York.
84. Smykatz-Kloss, W. 2002. Differential thermal analysis of Mg-bearing carbonates and sheet silicates. J. Therm. Anal. Calorim. 69:85-92.
85. Sobecki, T.M., and A.D. Karathanasis. 1987. Quantification and compositional characterization of pedogenic calcite and dolomite in calcic horizons of selected Aquolls. Soil Sci. Soc. Am. J. 51:683-690.
86. Soukup, D.A., B.J. Buck, and W. Harris. 2008. Preparing soils for mineralogical analyses. p. 13-32. In A.L. Ulery and L.R. Drees (ed.) Methods of soil analysis. Part 5. Mineralogical methods. SSSA Book Ser. 5. SSSA, Madison, WI.
87. Statheropoulos, M., S. Kyriakou, and N. Tzamtzis. 1998. Performance evaluation of a TG/MS system. Thermochim. Acta 322:167-173.
88. Tan, K.H. 1978. Formation of metal-humic acid complexes by titration and their characterization by differential thermal analysis and infrared spectroscopy. Soil Biol. Biochem. 10:123-129.
89. Tan, K.H., B.F. Hajek, and I. Barshad. 1986. Thermal analysis techniques. p. 151-183. In A. Klute (ed.) Methods of soil analysis. Part 1. 2nd ed. Agron. Monogr. 9. ASA and SSSA, Madison, WI.
90. Todor, D.N. 1976. Thermal analysis of minerals. Abacus Press, Kent, England.
91. Tonsuaadu, K., M. Reid, T. Leskela, R. Mannonen, L. Niinisto, and M. Veiderma. 1995. A thermoanalytical study of synthetic carbonate-containing apatites. Thermochim. Acta 256:55-65.
92. Tullock, R.J., and C.B. Roth. 1975. Stability of mixed iron and aluminum hydrous oxides on montmorillonite. Clays Clay Miner. 23:27-32.
93. Turi, E.A. (ed.) 1996. Thermal characterization of polymeric materials. 2nd ed. Academic Press, New York.
94. van Groos, A.F.K., and S. Guggenheim. 1990. High pressure differential thermal analysis: Application to clay minerals. p. 50-94. In J.W. Stucki et al. (ed.) Thermal analysis in clay science. Clay Minerals Society, Boulder, CO.
95. van Humbeeck, J. 1998. Simultaneous thermal analysis. p. 497-508. In M.E. Brown (ed.) Handbook of thermal analysis and calorimetry. Elsevier, New York.
96. Warne, S.S.J., D.J. Morgan, and A. Milodovski. 1981. Thermal analysis studies of dolomite, ferrous dolomite, ankerite series: Iron content recognition and determination by variable atmosphere DTA. Thermochim. Acta 51:105-111.
97. Weast, R.C. (ed.). 1980. Constant humidity table. In CRC handbook of chemistry and physics. 61st ed. CRC Press, Boca Raton, FL.
98. Wendlandt, W.W. 1986. Thermal analysis. 3rd ed. John Wiley and Sons, New York.
99. Wetton, R.E. 1998. Thermomechanical methods. p. 363-399. In M.E. Brown (ed.) Handbook of thermal analysis and calorimetry. Elsevier, New York.
100. Wicks, F.J., and R.A. Ramik. 1990. Vacuum thermogravimetric analysis and evolved gas analysis by mass spectroscopy. p. 160-189. In J.W. Stucki et al. (ed.) Thermal analysis in clay science. Clay Mineral Society Workshop Lectures. Clay Miner. Soc., Aurora, CO.
101. Wiedemann, H.G., and S. Felder-Casagrande. 1998. Thermomicroscopy. p. 473-496. In M.E. Brown (ed.) Handbook of thermal analysis and calorimetry. Elsevier, New York.
102. Xi, Y.F., Z. Ding, H.P. He, and R.L. Frost. 2004. Structure of organoclaysan X-ray diffraction and thermogravimetric analysis study. J. Colloid Interface Sci. 277:116-120.
103. Xie, W., and W.P. Pan. 2001. Thermal characterization of materials using evolved gas analysis. J. Therm. Anal. Calorim. 65:669-685.
104. Yariv, S. 1989. Thermal analysis of minerals. Thermochim. Acta 148:421-430.
105. Yariv, S. 1996. Thermo-IR-spectroscopy analysis of the interactions between organic pollutants and clay minerals. Thermochim. Acta 274:1-35.