Structural elucidation of hydro-products from hydrothermal carbonization of loblolly pine at different temperatures using NMR techniques

Energy

Volumn 133, Issue , 2017, Pages 171-178

  Wu, Qiong ^a   Huang, Lang ^b   Yu, Shitao ^a   Liu, Shiwei ^a   Xie, Congxia ^a   Ragauskas, Arthur J ^c,d  

^a QINGDAO UNIVERSITY OF SCIENCE AND TECHNOLOGY   (China)

^b WASHINGTON STATE UNIVERSITY   (United States)

^c University of TN   (United States)

^d OAK RIDGE NATIONAL LABORATORY   (United States)

Author keywords

Biomass energy; Carbonaceous materials; NMR techniques; Thermal conversion

Indexed keywords

AROMATIC COMPOUNDS; AROMATIZATION; CALORIFIC VALUE; CARBONIZATION; CHAINS; CONDENSATION REACTIONS; PROTONATION; SUBSTITUTION REACTIONS; THERMOCHEMISTRY;

ALIPHATIC SIDE CHAIN; BIO-MASS ENERGY; CARBONACEOUS MATERIALS; CARBONYL AND CARBOXYL GROUPS; HYDROTHERMAL CARBONIZATION; NMR TECHNIQUES; STRUCTURAL ELUCIDATION; THERMAL CONVERSION;

FORESTRY;

BIOENERGY; BIOMASS; CARBON SEQUESTRATION; CONIFEROUS TREE; HIGH TEMPERATURE; HYDROTHERMAL SYSTEM; NUCLEAR MAGNETIC RESONANCE; PHENOL; PHENOLIC COMPOUND; POLYMER;

BIOMASS; ENERGY;

PINUS TAEDA;

EID: 85019763751     PISSN: 03605442     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.energy.2017.05.040     Document Type: Article

References (37)

1. Burguete, P., Corma, A., Hitzl, M., Modrego, R., Ponce, E., Renz, M., Fuel and chemicals from wet lignocellulosic biomass waste streams by hydrothermal carbonization. Green Chem 18 (2016), 1051–1060.
2. Hu, B., Wang, K., Wu, L.H., Yu, S.H., Antonietti, M., Titirici, M.M., Engineering carbon materials from the hydrothermal carbonization process of biomass. Adv Mater 22 (2010), 813–828.
3. Jia, X.F., Li, J., Wang, E.K., One-pot green synthesis of optically pH-sensitive carbon dots with upconversion luminescence. Nanoscale 4 (2012), 5572–5575.
4. Wu, Q., Li, W., Wu, Y.J., Zong, G.G., Liu, S.X., Effect of reaction time on structure of ordered mesoporous carbon microspheres prepared from carboxymethyl cellulose by soft-template method. Ind Crops Prod 76 (2015), 866–872.
5. Zhao, L., Fan, L.Z., Zhou, M.Q., Guan, H., Qiao, S.Y., Antonietti, M., Titirici, M.M., Nitrogen-containing hydrothermal carbons with superior performance in supercapacitors. Adv Mater 22 (2010), 5202–5206.
6. Wu, Q., Li, W., Wu, Y.J., Tan, J., Liu, S.X., Hydrothermal carbonization of carboxymethylcellulose: one-pot preparation of conductive carbon microspheres and water-soluble fluorescent carbon nanodots. Chem Eng J 266 (2015), 112–120.
7. Kosa, M., Ben, H.X., Theliander, H., Ragauskas, A.J., Pyrolysis oils from CO2 precipitated kraft lignin. Green Chem 13 (2011), 3196–3202.
8. Zhang, W.P., Xu, S.T., Huan, X.W., Bao, X.H., In situ solid-state NMR for heterogeneous catalysis: a joint experimental and theoretical approach. Chem Soc Rev 41 (2012), 192–210.
9. Yang, Z.C., Zhang, Y., Kong, J.H., Wong, S., Li, X., Wang, J., Hollow carbon nanoparticles of tunable size and wall thickness by hydrothermal treatment of a-cyclodextrin templated by F127 block copolymers. Chem Mater 25 (2013), 704–710.
10. Kubo, S., White, R.J., Tauer, K., Titirici, M.M., Flexible coral-like carbon nanoarchitectures via a dual block copolymer-latex templating approach. Chem Mater 25 (2013), 4781–4790.
11. Falco, C., Caballero, F.P., Babonneau, F., Gervais, C., Laurent, G., Titirici, M.M., Baccile, N., Lamgmuir 27 (2011), 14460–14471.
12. Baccile, N., Falco, C., Titirici, M.M., Characterization of biomass and its derived char using 13 C-solid state nuclear magnetic resonance. Green Chem 16 (2014), 4839–4869.
13. Wu, Q., Li, W., Tan, J., Liu, S.X., Flexible cage-like carbon spheres with ordered mesoporous structures prepared via a soft-template/hydrothermal process from carboxymethylcellulose. RSC Adv 4 (2014), 61518–61524.
14. Pu, Y.Q., Cao, S.L., Ragauskas, A.J., Application of quantitative 31P NMR in biomass lignin and biofuel precursors characterization. Energy Environ Sci 4 (2011), 3154–3166.
15. Balakshin, M., Capanema, E., On the quantification of lignin hydroxyl groups with 31P and 13C NMR spectroscopy. J Wood Chem Technol 35 (2015), 220–237.
16. Hu, Z., Sykes, R., Davis, M.F., Charles, B.E., Ragauskas, A.J., Chemical profiles of switchgrass. Bioresour Technol 101 (2010), 3253–3257.
17. Hoekman, S.K., Broch, A., Robbins, C., Hydrothermal carbonization (HTC) of lignocellulosic biomass. Energy Fuels 25 (2011), 1802–1810.
18. Sannigrahi, P., Kim, D.H., Jung, S., Ragauskas, A.J., Pseudo-lignin and pretreatment chemistry. Energy Environ Sci 4 (2011), 1306–1310.
19. Sevilla, M., Fuertes, A.B., The production of carbon materials by hydrothermal carbonization of cellulose. Carbon, 2009, 2281–2289.
20. Cao, X.Y., Ro, K.S., Chappell, M., Li, Y., Mao, J.D., Chemical structures of Swine-Manure Chars Produced under different carbonization conditions investigated by advanced solid-state 13C nuclear magnetic resonance (NMR) spectroscopy. Energy Fuels 25 (2011), 388–397.
21. Gao, Y., Wang, X.H., Yang, H.P., Chen, H.P., Characterization of products from hydrothermal treatments of cellulose. Energy 42 (2012), 457–465.
22. Chheda, J.N., Huber, G.W., Dumesic, J.A., Liquid-phase catalytic processing of biomass-derived oxygenated hydrocarbons to fuels and chemicals. Angew Chem Int Ed 46 (2007), 7164–7183.
23. Xiao, L.P., Shi, Z.J., Xu, F., Sun, R.C., Hydrothermal carbonization of lignocellulosic biomass. Bioresour Technol 118 (2012), 619–623.
24. Ben, H.X., Ragauskas, A.J., In suit NMR characterization of pyrolysis oil during accelerated aging. Chemsuschem 5 (2012), 1687–1693.
25. Shen, D.K., Gu, S., The mechanism for thermal decomposition of cellulose and its main products. Bioresour Technol 100 (2009), 6496–6504.
26. Baccile, N., Laurent, G., Babonneau, F., Fayon, F., Titirici, M.M., Antonietti, M., Structural characterization of hydrothermal carbon spheres by advanced solid-state MAS 13C NMR investigation. J Phys Chem C 113 (2009), 9644–9654.
27. Acton, Q.A., Aromatic hydrocarbons-Advances in research and treatment. 2013, Scholarly Editions, Atlanta, Georgia ISBN:978-1-481-68525-2.
28. Foston, M., Nunnery, G.A., Meng, X.Z., Sun, Q.N., Baker, F.S., Ragauskas, A.J., NMR a critical tool to study the production of carbon fiber from lignin. Carbon 52 (2013), 65–73.
29. Binder, J.B., Gray, M.J., White, J.F., Zhang, Z.C., Holladay, J.E., Reactions of lignin model compounds in ionic liquids. Biomass Bioenergy 33 (2009), 1122–1130.
30. Kawamoto, H., Nakamura, T., Saka, S., Pyrolytic cleavage mechanisms of lignin-ether linkages: a study on p-substituted dimers and trimers. Holzforschung 62 (2008), 50–56.
31. Chaala, A., Ba, T., Garcia-Perez, M., Roy, C., Colloidal properties of bio-oils obtained by vacuum pyrolysis of softwood bark: aging and thermal stability. Energy Fuels 18 (2004), 1535–1542.
32. Aida, T.M., Sato, Y., Watanabe, M., Tarima, K., Nonaka, T., Hattori, H., Dehydration of d-glucose in high temperature water at pressures up to 80 MPa. J Supercrit Fluids 40 (2007), 381–389.
33. Chheda, J.N., Huber, G.W., Dumesic, J.A., Liquid-phase catalytic processing of biomass-derived oxygenated hydrocarbons to fuels and chemicals. Angew Chem Int Ed 46 (2007), 7164–7183.
34. Ben, H.X., Ragauskas, A.J., NMR Characterization of pyrolysis oils from kraft lignin. Energy Fuels 25 (2011), 2322–2332.
35. Titirici, M.M., Antonietti, M., Baccile, N., Hydrothermal carbon from biomass: a comparison of the local structure from poly-to monosaccharides and pentoses/hexoses. Green Chem 10 (2008), 1204–1212.
36. Pu, Y.Q., Hu, F., Huang, F., Davison, B.H., Ragauskas, A.J., Assessing the molecular structure basis for biomass recalcitrance during dilute acid and hydrothermal pretreatment. Biotechnol Biofuels 6 (2013), 15–28.
37. Yao, C.H., Shin, Y., Wang, L.Q., Windisch, C.F., Samuels, W.D., Arey, B.W., Wang, C.M., Risen, W.M., Exarhos, G.J., Hydrothermal dehydration of aqueous fructose solutions in a closed system. J Phys Chem C 111 (2007), 15141–15145.