The production of carbon materials by hydrothermal carbonization of cellulose

Carbon

Volumn 47, Issue 9, 2009, Pages 2281-2289

  Sevilla, M ^a   Fuertes, A B ^a  

^a INSTITUTO NACIONAL DEL CARBÓN   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

[CARBONYL; BENZENE RING; CARBON MATERIAL; CARBONACEOUS MATERIALS; CHEMICAL POINT; DEHYDRATION PROCESS; ELEMENTAL ANALYSIS; FUNCTIONALIZED; HYDROTHERMAL CARBONIZATION; HYDROTHERMAL TRANSFORMATION; INFRARED AND RAMAN SPECTROSCOPY; SEM; SMALL CLUSTERS; SOLID PRODUCTS; SPECTROSCOPIC TECHNIQUE; XPS;

AGGLOMERATION; BENZENE; CARBONIZATION; CELLULOSE; DEHYDRATION; ESTERS; ETHERS; GLUCOSE; INFRARED SPECTROSCOPY; OXYGEN; POINT GROUPS; SPECTROSCOPIC ANALYSIS; SUGAR (SUCROSE);

COKE;

AGGLOMERATION; BENZENE; CARBONIZATION; CELLULOSE; COKE; DEHYDRATION; ESTERS; ETHERS; GLUCOSE; INFRARED SPECTROSCOPY; SPECTROCHEMICAL ANALYSIS; SUCROSE;

EID: 66049158918     PISSN: 00086223     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.carbon.2009.04.026     Document Type: Article

References (58)

1. Wang Q., Li H., Chen L., and Huang X. Monodispersed hard carbon spherules with uniform nanopores. Carbon 39 14 (2001) 2211-2214
2. Wang Q., Li H., Chen L., and Huang X. Novel spherical microporous carbon as anode material for Li-ion batteries. Solid State Ionics 152-153 (2002) 43-50
3. 3 and GaN semiconductor hollow spheres. Angew Chem Int Ed Engl 43 29 (2004) 3827-3831
4. Titirici M.M., Thomas A., Yu S.-H., Müller J.-O., and Antonietti M. A direct synthesis of mesoporous carbons with bicontinuous pore morphology from crude plant material by hydrothermal carbonization. Chem Mater 19 17 (2007) 4205-4212
5. Hu J., Li H., and Huang X. Influence of micropore structure on Li-storage capacity in hard carbon spherules. Solid State Ionics 176 11-12 (2005) 1151-1159
6. Yao C., Shin Y., Wang L.-Q., Windish C.F., Samuels W.D., Arey B.W., et al. Hydrothermal dehydration of aqueous fructose solutions in a closed system. J Phys Chem C 111 42 (2007) 15141-15145
7. Bergius F., and Specht H. Die Anwendung hoher Drucke bei chemischen Vorgängen und eine Nachbildung des Entstehungsprozesses der Steinkohle (1913), Verlag Wilhelm Knapp, Halle and der Saale, Germany p. 58
8. Berl E., and Schimdt A. Die Inkohlung von cellulose und lignin in neutralem medium. Liebigs Ann Chem 493 1 (1932) 97-123
9. Schuhmacher J.P., Huntjens F.J., and Van Krevelen D.W. Chemical structure and properties of coal XXVI - studies on artificial coalification. Fuel 39 (1960) 223-234
10. Bobleter O., Niesner R., and Röhr M. The hydrothermal degradation of cellulosic matter to sugars and their fermentative conversion to protein. J Appl Polym Sci 20 (1976) 2083-2093
11. Bonn G., Cocin R., and Bobleter O. Hydrothermolysis - a new process for the utilization of biomass. Wood Sci Technol 17 3 (1983) 195-202
12. Karagöz S., Bhaskar T., Muto A., Sakata Y., Oshiki T., and Kishimoto T. Low-temperature catalytic hydrothermal treatment of wood biomass: analysis of liquid products. Chem Eng J 108 1-2 (2005) 127-137
13. Huber G.W., Iborra S., and Corma A. Synthesis of transportation fuels from biomass: chemistry, catalysts, and engineering. Chem Rev 106 9 (2006) 4044-4098
14. Sakaki T., Shibata M., Miki T., Hirosue H., and Hayashi N. Reaction model of cellulose decomposition in near-critical water and fermentation of products. Bioresour Technol 58 2 (1996) 197-202
15. 3 hollow-sphere gas sensors. Inorg Chem 43 17 (2004) 5442-5449
16. Zheng M., Cao J., Chang X., Wang J., Liu J., and Ma X. Preparation of oxide hollow spheres by colloidal carbon spheres. Mater Lett 60 24 (2006) 2991-2993
17. Titirici M.M., Antonietti M., and Thomas A. A generalized synthesis of metal oxide hollow spheres using a hydrothermal approach. Chem Mater 18 16 (2006) 3808-3812
18. Sun X., Liu J., and Li Y. Use of carbonaceous polysaccharide microspheres as templates for fabricating metal oxide hollow spheres. Chem Eur J 12 7 (2006) 2039-2047
19. 2 spheres prepared by carbon sphere template method. Sens Actuators B: Chem 120 2 (2007) 508-513
20. Sevilla M., Lota G., and Fuertes A.B. Saccharide-based graphitic carbon nanocoils as supports for PtRu nanoparticles for methanol electrooxidation. J Power Sources 171 2 (2007) 546-551
21. Sevilla M., Sanchís C., Valdés-Solís T., Morallón E., and Fuertes A.B. Highly dispersed platinum nanoparticles on carbon nanocoils and their electrocatalytic performance for fuel cell reactions. Electrochim Acta 54 8 (2008) 2234-2238
22. Ramosa M.E., Bonellia P.R., and Cukiermana A.L. Physico-chemical and electrical properties of activated carbon cloths: effect of inherent nature of the fabric precursor. Colloids Surf A: Physicochem Eng Aspects 324 1-3 (2008) 86-92
23. 4 activation. Carbon 44 8 (2006) 1464-1475
24. Guilminot E., Gavillon R., Chatenet M., Berthon-Fabryc S., Rigacci A., and Budtovab T. New nanostructured carbons based on porous cellulose: elaboration, pyrolysis and use as platinum nanoparticles substrate for oxygen reduction electrocatalysis. J Power Sources 185 2 (2008) 717-726
25. Zavadskii A.E. X-ray diffraction method of determining the degree of crystallinity of cellulose materials of different anisotropy. Fibre Chem 36 6 (2004) 425-430
26. Sevilla M, Fuertes AB. Chemical and structural properties of carbonaceous products obtained by hydrothermal carbonization of saccharides. Chem Eur J, in press. doi:10.1002/chem.200802097.
27. Sun X., and Li Y. Colloidal carbon spheres and their core/shell structures with noble-metal nanoparticles. Angew Chem Int Ed Engl 43 5 (2004) 597-601
28. Shaka S., and Ueno T. Chemical conversion of various celluloses to glucose and its derivatives in supercritical water. Cellulose 6 3 (1999) 177-191
29. Bobleter O. Hydrothermal degradation of polymers derived from plants. Prog Polym Sci 19 5 (1994) 797-841
30. Serageldin M.A., and Pan W.-P. Coal analysis using thermogravimetry. Thermochim Acta 76 1-2 (1984) 145-160
31. Van Krevelen D.W. Graphical statistical method for the study of structure and reaction processes of coal. Fuel 29 (1950) 269-284
32. Holgate H.R., Meyer J.C., and Tester J.W. Glucose hydrolysis and oxidation in supercritical water. AIChE J 41 3 (1995) 637-648
33. Karagöz S., Bhaskar T., Muto A., and Sakata Y. Comparative studies of oil compositions produced from sawdust, rice husk, lignin and cellulose by hydrothermal treatment. Fuel 84 7-8 (2005) 875-884
34. Aida T.M., Sato Y., Watanabe M., Tarima K., Nonaka T., Hattori H., et al. Dehydration of D-glucose in high temperature water at pressures up to 80 MPa. J Supercrit Fluids 40 3 (2007) 381-388
35. Kabyemela B.M., Adschiri T., Malaluan R.M., and Arai K. Glucose and fructose decomposition in subcritical and supercritical water: detailed reaction pathway, mechanisms, and kinetics. Ind Eng Chem Res 38 8 (1999) 2888-2895
36. Lua A.C., and Yang T. Effect of activation temperature on the textural and chemical properties of potassium hydroxide activated carbon prepared from pistachio-nut shell. J Colloid Interface Sci 274 2 (2004) 594-601
37. Araujo-Andrade C., Ruiz F., Martínez-Mendoza J.R., and Terrones H. Infrared and Raman spectra, conformational stability, ab initio calculations of structure, and vibrational assignment of α and β glucose. J Mol Struct: THEOCHEM 714 2-3 (2005) 143-146
38. Ibarra V., Muñoz E., and Moliner R. FTIR study of the evolution of coal structure during the coalification process. Org Geochem 24 6-7 (1996) 725-735
39. Cuesta A., Dhamelincourt P., Laureyns J., Martínez-Alonso A., and Tascón J.M.D. Raman microprobe studies on carbon materials. Carbon 32 8 (1994) 1523-1532
40. Sheng C. Char structure characterised by Raman spectroscopy and its correlations with combustion reactivity. Fuel 86 15 (2007) 2316-2324
41. Ferrari A.C., and Robertson J. Interpretation of Raman spectra of disordered and amorphous carbon. Phys Rev B 61 20 (2000) 14095-14107
42. Schwan J., Ulrico S., Batori V., and Ehrhardt H. Raman spectroscopy on amorphous carbon films. J Appl Phys 80 1 (1996) 440-447
43. Okpalugo T.I.T., Papakonstantinou P., Murphy H., McLaughlin J., and Brown N.M.D. High resolution XPS characterization of chemical functionalised MWCNTs and SWCNTs. Carbon 43 1 (2005) 153-161
44. Molina R., Espinós J.P., Yubero F., Erra P., and González Elipe A.R. XPS analysis of down stream plasma treated wool: influence of the nature of the gas on the surface modification of wool. Appl Surf Sci 252 5 (2005) 1417-1429
45. Xia W., Wang Y., Bergsträβer R., Kundu S., and Muhler M. Surface characterization of oxygen-functionalized multi-walled carbon nanotubes by high-resolution X-ray photoelectron spectroscopy and temperature-programmed desorption. Appl Surf Sci 254 1 (2007) 247-250
46. Sasaki M., Kabyemela B., Malaluan R., Hirose S., Takeda N., Adschiri T., et al. Cellulose hydrolysis in subcritical and supercritical water. J Supercrit Fluids 13 1 (1998) 261-268
47. Sasaki M., Fang Z., Fukushima Y., Adschiri T., and Arai K. Dissolution and hydrolysis of cellulose in subcritical and supercritical water. Ind Eng Chem Res 39 8 (2000) 2883-2890
48. 3). Cellulose 12 6 (2005) 595-606
49. 2O to 2273 K and 500 MPa. AIChe J 35 10 (1989) 1631-1638
50. Garrote G., Domínguez H., and Parajó J.C. Hydrothermal processing of lignocellulosic materials. Holz als Roh- und Werkstoff 57 3 (1999) 191-202
51. Nagamori M., and Funazukuri T. Glucose production by hydrolysis of starch under hydrothermal conditions. J Chem Technol Biotechnol 79 3 (2004) 229-233
52. Antal M.J., Mok W.S.L., and Richards G.N. Mechanism of formation of 5-(hydroxymethyl)-2-furaldehyde from D-fructose and sucrose. Carbohydr Res 199 1 (1990) 91-109
53. Sinag A., Kruse A., and Schwarzkopf V. Formation and degradation pathways of intermediate products formed during the hydropyrolysis of glucose as a model substance for wet biomass in a tubular reactor. Eng Life Sci 3 12 (2003) 469-473
54. Chheda J.N., Huber G.W., and Dumesic J.A. Liquid-phase catalytic processing of biomass-derived oxygenated hydrocarbons to fuels and chemicals. Angew Chem Int Ed 46 38 (2007) 7164-7183
55. Asghari F.S., and Yoshida H. Acid-catalyzed production of 5-hydroxymethyl furfural from D-fructose in subcritical water. Ind Eng Chem Res 45 7 (2006) 2163-2173
56. Luijkx G.C.A., van Rantwijk F., van Bekkum H., and Antal Jr. M.J. The role of deoxyhexonic acids in the hydrothermal decarboxylation of carbohydrates. Carbohydr Res 272 2 (1995) 191-202
57. Tang M.M., and Bacon R. Carbonization of cellulose fibers - II. Physical property study. Carbon 2 3 (1964) 221-225
58. Meyer N., et al. Fresenius J Anal Chem 370 (2001) 789-791