Methionine bound to Pd/γ-Al2O3 catalysts studied by solid-state 13C NMR

Solid State Nuclear Magnetic Resonance

Volumn 72, Issue , 2015, Pages 64-72

  Johnson, Robert L ^a   Schwartz, Thomas J ^b   Dumesic, James A ^b   Schmidt Rohr, Klaus ^a,c  

^a IOWA STATE UNIVERSITY   (United States)

^b University of Wisconsin Madison   (United States)

^c BRANDEIS UNIVERSITY   (United States)

Author keywords

Catalyst characterization postmortem; Multicp MAS; Surface NMR

Indexed keywords

ALUMINUM; AMINO ACIDS; BINS; CARBON; CATALYSTS; CHEMICAL BONDS; CHEMICAL SHIFT; COMPLEXATION; FEEDSTOCKS; MAGIC ANGLE SPINNING; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

CATALYST CHARACTERIZATION; CATALYST INHIBITION; LARGE-AMPLITUDE MOTION; MULTICP/MAS; PREFERENTIAL BINDING; REDUCING ENVIRONMENT; SOLID STATE MAGIC ANGLE SPINNING NMR; SURFACE NMR;

PALLADIUM;

ALUMINUM OXIDE; METAL NANOPARTICLE; METHIONINE; PALLADIUM; PYRONE DERIVATIVE; SULFUR; TRIACETIC ACID LACTONE;

CATALYSIS; CHEMISTRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; OXIDATION REDUCTION REACTION; SURFACE PROPERTY;

ALUMINUM OXIDE; CATALYSIS; MAGNETIC RESONANCE SPECTROSCOPY; METAL NANOPARTICLES; METHIONINE; OXIDATION-REDUCTION; PALLADIUM; PYRONES; SULFUR; SURFACE PROPERTIES;

EID: 84961309584     PISSN: 09262040     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ssnmr.2015.09.007     Document Type: Article

References (54)

1. B.J. Nikolau, M. Perera, L. Brachova, and B. Shanks Platform biochemicals for a biorenewable chemical industry Plant J. 54 4 2008 536 545
2. B.H. Shanks Unleashing biocatalysis/chemical catalysis synergies for efficient biomass conversion ACS Chem. Biol. 2 2007 533 535
3. T.J. Schwartz, B.J. O'Neill, B.H. Shanks, and J.A. Dumesic Bridging the chemical and biological catalysis gap: challenges and outlooks for producing sustainable chemicals ACS Catal. 4 2014 2060 2069
4. J. Cardenas, and N.A. Da Silva Metabolic engineering of Saccharomyces cerevisiae for the production of triacetic acid lactone Metab. Eng. 25 2014 194 203
5. M. Chia, T.J. Schwartz, B.H. Shanks, and J.A. Dumesic Triacetic acid lactone as a potential biorenewable platform chemical Green Chem. 14 7 2012 1850 1853
6. T.J. Schwartz, Z.J. Brentzel, and J.A. Dumesic Inhibition of Metal Hydrogenation Catalysts by Biogenic Impurities Catal. Lett. 145 2015 15 22
7. P. Albers, J. Pietsch, and S.F. Parker Poisoning and deactivation of palladium catalysts J. Mol. Catal. A: Chem. 173 1-2 2001 275 286
8. P. Albers, H. Angert, G. Prescher, and K. Seibold Catalyst poisoning by methyl groups Chem. Commun. 17 1999 1619 1620
9. 2 catalysts J. Phys. Chem. B 103 1999 3923 3934
10. L.J. Hoyos, M. Primet, and H. Praliaud Sulfur Piosoning and Regeneration of Palladium-based Catalysts J. Chem. Soc. Faraday Trans. 88 1 1992 113 119
11. D.S. Brands, G. U-A-Sai, E.K. Poels, and A. Bliek Sulfur deactivation of fatty ester hydrogenolysis catalysts J. Catal. 186 1999 169 180
12. 2S Deactivation and reactivation of the catalyst Appl. Catal. A 165 1997 147 157
13. T.J. Schwartz, R.L. Johnson, J. Cardenas, A. Okerlund, N.A.D. Silva, K. Schmidt-Rohr, and J.A. Dumesic Engineering catalyst microenvironments for metal-catalyzed hydrogenation of biologically-derived platform chemicals Angew. Chem. Int. Ed. 53 47 2014 12718 12722
14. 3 catalysts for olefin metathesis J. Phys. Chem. C 113 19 2009 8228 8233
15. 13C n.m.r. spectroscopy Zeolites 7 1 1987 6 8
16. A. Gutsze, J.P. Lange, H.G. Karge, and J. Allgeier Carbonization of polyethylene over acidic zeolites J. Catal. 113 2 1988 525 528
17. G.A. Somorjai, and C. Aliaga Molecular studies of model surfaces of metals from single crystals to nanoparticles under catalytic reaction conditions. Evolution from prenatal and postmortem studies of catalysts Langmuir 26 21 2010 16190 16203
18. B.M. Weckhuysen Snapshots of a working catalyst: possibilities and limitations of in situ spectroscopy in the field of heterogeneous catalysis Chem. Commun. 2 2002 97 110
19. T. Azais, G. Hartmeyer, S. Quignard, G. Laurent, and F. Babonneau Solution state NMR techniques applied to solid state samples: characterization of benzoic acid confined in MCM-41 J. Phys. Chem. C 114 19 2010 8884 8891
20. 13C and 29Si MAS NMR Langmuir 18 16 2002 6159 6163
21. V.A. Bell, R.F. Carver, C. Dybowski, and H.S. Gold Aldol condensation of butan-2-one and pentan-3-one on an activated alumina as monitored via in-situ carbon-13 nuclear magnetic resonance spectroscopy J. Chem. Soc. Faraday Trans. 1 80 4 1984 831 839
22. 13C solid-state NMR exchange experiments J. Phys. Chem. B 106 9 2002 2261 2268
23. T. Azaïs, C. Tourné-Péteilh, F. Aussenac, N. Baccile, C. Coelho, J.-M. Devoisselle, and F. Babonneau Solid-state NMR study of ibuprofen confined in MCM-41 material Chem. Mater. 18 26 2006 6382 6390
24. 15N NMR spectroscopy of pyrazole and 3,5-dimethylpyrazole adsorbed on alumina and silica J. Phys. Chem. 98 35 1994 8752 8760
25. W. Zhang, S. Xu, X. Han, and X. Bao In situ solid-state NMR for heterogeneous catalysis: a joint experimental and theoretical approach Chem. Soc. Rev. 41 1 2012 192 210
26. C.P. Slichter Probing phenomena at metal surfaces by NMR Annu. Rev. Phys. Chem. 37 1 1986 25
27. 13C chemical shifts of CO adsorbed on Pt electrocatalysts J. Phys. Chem. C 112 38 2008 14702 14705
28. P. McGrath, A.M. Fojas, B. Rush, J.A. Reimer, and E.J. Cairns Characterizing electrocatalytic surfaces: electrochemical and NMR studies of methanol and carbon monoxide on Pt/C Electrochim. Acta 53 3 2007 1365 1371
29. M. Pruski, J.C. Kelzenberg, B.C. Gerstein, and T.S. King Solid-state NMR of carbon-13 in ethylene adsorbed on silica-supported ruthenium J. Am. Chem. Soc. 112 11 1990 4232 4240
30. 13C 1-labeled octanethiol-protected Au nanoparticles: shifts, relaxations, and particle-size effect J. Am. Chem. Soc. 125 1 2002 18 19
31. 13C NMR guides rational design of nanocatalysts via chemisorption evaluation in liquid phase Science 332 6026 2011 224 228
32. C.F. Tirendi, G.A. Mills, C. Dybowski, and G. Neue Platinum-proton coupling in the NMR spectrum of benzene on an alumina-supported platinum catalyst J. Phys. Chem. 96 12 1992 5045 5048
33. C.F. Tirendi, G.A. Mills, and C. Dybowski Solid-state nuclear magnetic resonance investigations of benzene and cyclohexane adsorbed on platinum/aluminum oxide J. Phys. Chem. 88 24 1984 5765 5767
34. C.F. Tirendi, G.A. Mills, and C.R. Dybowski Solid-state NMR spectroscopy of benzene adsorbed on.eta.-alumina J. Phys. Chem. 93 8 1989 3282 3286
35. 13C chemical shift of adsorbed acetone for measuring the acid strength of solid acids: a theoretical calculation study J. Phys. Chem. C 114 29 2010 12711 12718
36. J.F. Haw, J. Zhang, K. Shimizu, T.N. Venkatraman, D.-P. Luigi, W. Song, D.H. Barich, and J.B. Nicholas NMR and theoretical study of acidity probes on sulfated zirconia catalysts J. Am. Chem. Soc. 122 50 2000 12561 12570
37. 13C chemical shift tensors of acetone complexed with Brønsted and Lewis acids J. Am. Chem. Soc. 120 47 1998 12342 12350
38. 13C solid-state NMR studies of methanol adsorbed on a series of acidic microporous zeotype materials J. Phys. Chem. 100 16 1996 6698 6707
39. Y.H. Chin, and P.D. Ellis Solid-state NMR study of acetylene adsorbed to platinum on alumina as followed by direct observation using CP MAS methods. Differentiation between acetylene adsorbed to alumina and platinum J. Am. Chem. Soc. 111 19 1989 7653 7654
40. F. Gul-E-Noor, M. Mendt, D. Michel, A. Pöppl, H. Krautscheid, J. Haase, and M. Bertmer Adsorption of small molecules on Cu3(btc)2 and Cu3-xZnx(btc)2 Metal-Organic Frameworks (MOF) as studied by solid-state NMR J. Phys. Chem. C 117 15 2013 7703 7712
41. 13C NMR and infrared evidence of a dioctyl-disulfide structure on octanethiol-protected palladium nanoparticle surfaces J. Am. Chem. Soc. 126 32 2004 10053 10058
42. E. Soederlind, and P. Stilbs Chain conformation of ionic surfactants adsorbed on solid surfaces from carbon-13 NMR chemical shifts Langmuir 9 7 1993 1678 1683
43. 13C NMR investigations of dodecyl sulfate-alumina interfacial interactions using high surface area pseudo-boehmite solids containing adsorbed surfactants Langmuir 12 8 1996 1958 1966
44. L.-Q. Wang, J. Liu, G.J. Exarhos, K.Y. Flanigan, and R. Bordia Conformation heterogeneity and mobility of surfactant molecules in intercalated clay minerals studied by solid-state NMR J. Phys. Chem. B 104 13 2000 2810 2816
45. M.S. Yahnke, B.M. Rush, J.A. Reimer, and E.J. Cairns Quantitative solid-state NMR Spectra of CO adsorbed from aqueous solution onto a commercial electrode J. Am. Chem. Soc. 118 48 1996 12250 12251
46. 13C Solid-State nuclear magnetic resonance Environ. Sci. Tech. 38 9 2004 2680 2684
47. 13C NMR with signal enhancement by multiple cross polarization J. Magn. Reson. 239 0 2014 44 49
48. J. Schaefer, and E.O. Stejskal Carbon-13 nuclear magnetic resonance of polymers spinning at the magic angle J. Am. Chem. Soc. 98 4 1976 1031 1032
49. W.L.F. Armarego, and C.L.L. Chai Purification of Laboratory Chemicals 6th ed. 2009 Waltham, Massachusetts, Elsevier, Inc. United States
50. 13C NMR signals from di-oxygenated alkyl bands by a chemical-shift-anisotropy filter Solid State Nucl. Magn. Reson. 26 1 2004 36 45
51. K.J. Fritzsching, Y. Yang, K. Schmidt-Rohr, and M. Hong Practical use of chemical shift databases for protein solid-state NMR: 2D chemical shift maps and amino-acid assignment with secondary-structure information J. Biomol. NMR 56 2 2013 155 167
52. M. Chia, M.A. Haider, G. Pollock III, G.A. Kraus, M. Neurock, and J.A. Dumesic Mechanistic insights into ring-opening and decarboxylation of 2-pyrones in liquid water and tetrahydrofuran J. Am. Chem. Soc. 135 2013 5699 5708
53. 27Al dipolar interactions in solids J. Magn. Reson. 139 2 1999 250 257
54. 3 methanol synthesis catalyst J. Am. Chem. Soc. 114 22 1992 8552 8559